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A double-periodic multilayer method was proposed to test KBA system of 4.75keV using 8keV source. Alignment of angle is the key for most of grazing incidence systems in x-ray range. But for soft x-ray, strong absorption makes the alignment have to be operated in vacuum, which is difficult enough. A double-periodic multilayer was used to experiment at 8keV in air replacing 4.75keV in vacuum. This multilayer includes two parts, the top and the bottom. The top is W/B 4 C multilayer with four bilayers and 6.93nm periods. The bottom is W/B 4 C multilayer with 10 bilayers and 3.95nm periods. For 8keV energy, x-ray will penetrate through the top and reflected by the bottom. While for 4.75keV, x-ray will be reflected by the top directly. The full width of half maximum is 0.1° at 8keV and 0.3° at 4.75keV, so it is accurate enough for 4.75keV to experiment at 8keV, which was also verified by the 1-D KBA experiment. This double-periodic multilayer provides a valid solution for alignment in soft x-ray range.

Compound refractive x-ray lens is a unique device to form image of opaque object which is illuminated by x-rays. It is consisted of a lot number of placed in-line concave microlenses and works like ordinary refractive lens for visual light. In contrast to other x-ray optical devices, it could achieve satisfying resolution without complicated equipment. The spherical compound refractive x-ray lens used in this experiment is composed of 123 biconcave microlenses of 200 μm diameter. Each microlens was formed by the epoxy between two bubbles which were injected into an epoxy-filled glass capillary. There are three advantages ensuring good image quality of the lens for using in hard x-rays: (1) The epoxy (C100H200O20N, 1.08 g/cc) is composed of carbon, hydrogen and nitrogen, each of them is characterized by a low absorption coefficient for 5-30 keV x-rays. (2) Because of the nature of physics forming the bubble, the lens surface quality is extremely good. (3) The capillary makes sure that the series of unit lenses are well aligned coaxially. The lens focal length is 114 mm at 8.05 keV which is adjusted according to thick-lens analysis. X-ray images of grid mesh are compared between using a copper anode x-ray tube without filter and a synchrotron radiation source with monochromator. It could be found that the resolution and contrast are improved a lot by using monochromatic x-rays. The field of view and geometrical distortion around the edges of the field of view are reduced because of using a synchrotron radiation source. For x-ray tube as source the lens achieved a spatial resolution of 5 μm and field of view of about 700 μm. For a synchrotron radiation source, that is 3.8 μm by 2.3 μm resolution and field of view of about 316 μm by 128 μm.

Hard X-ray imaging by a spherical compound refractive lens is presented. The lens is composed of 123 biconcave microlenses with a size of 200 μm in diameter. Each microlens was formed by the epoxy between two bubbles, which were injected into an epoxy-filled glass capillary. The focal length of the lens is 114 mm at 8.05 keV. The light source was obtained by using a copper anode X-ray tube without a filter. The lens can be achieved a spatial resolution of 5 μm with field of view of about 700 μm, and 1–3 μm resolution may be obtainable by using monochromator and diaphragm.

Multilayer coatings are key optical components in the EUV, soft X-ray and X-ray range. At Institute of Precision Optical Engineering (IPOE), the development of multilayer optics has been impelled for their wide applications in X-ray laser, plasma diagnostics, astronomical observation and synchrotron radiation. The paper presents our recent results of periodic multilayers of Mo/Si, Cr/C, Cr/Sc, La/B4C, Mo/B4C, Si/C, Si/SiC, Mg/SiC Mo/Y and Ru/Y. To improve the reflectivity of Ru/Y multilayer mirrors, Mo layers were inserted between Ru and Y layer. The Mo barrier layers suppress intermixing between Ru and Y, thereby increasing the reflectivity of Ru/Y multilayer. We also discuss the application of Mo/Si, Mo/Y, Mo/B4C, La/B4C non-periodic multilayers in EUV broadband polarization measurement.

Three kinds of multilayer mirrors were developed for solar observation and earth’s magnetosphere observation at Extreme Ultraviolet (EUV) wavelength region. The first one is Mo/Si multilayer mirror, designed for solar Fe-XII emission line at wavelength of 19.5nm. The reflectivities are in the range of 38.7~42.9%, measured at National Synchrotron Radiation Laboratory (NSRL), Hefei, China. Th e second high-reflective multilayer is designed for solar He-II radiation at 30.4 nm. At this wavelength, SiC/Mg multilayers were investigated, and as high as 50.0% measured reflectivity was obtained at incident angle of 10u. Aperiodic SiC/Mg multilayers were also designed for wide angular ranges of 15-22u and 12-21u. The third multilayer mirror was a dual-function mirror used for earth’s magnetosphere observation, which requires high-reflective for He-II emission line at wavelength of 30.4nm but low-reflectance at 58.4nm from ionosphere He-I emission. Using aperiodic SiC/Mg multilayer stack, the dual-function multilayer mirror was designed by genetic algorithm. Compared to periodic multilayer, the dual-function multilayer suppresses the reflectivity for He-I at 58.4nm from 2.2% to 0.1%, without loss of the reflection for He-II at 30.4nm, significantly. These multilayer mirrors were all prepared by magnetron sputte ring system in IPOE, and measured at NSRL, China. Keywords: EUV astronomical observation; multilayer; magnetron sputtering; synchrotron radiation

To investigate the levels of stromal cell-derived factor-1 (SDF-1) and vascular endothelial growth factor (VEGF) in the vitreous of patients with proliferative diabetic retinopathy.The levels of SDF-1 and VEGF in the vitreous of 30 eyes of 30 patients with proliferative diabetic retinopathy (PDR) and 12 eyes of 12 patients with idiopathic macular hole (MH) were measured by enzyme-linked immunosorbent assay. Vitreous fluid samples were obtained by vitrectomy.The vitreous concentration of VEGF was significantly higher in eyes with PDR (2,865.87 +/- 387.85 pg/ml) than in eyes with idiopathic macular hole (142.42 +/- 21.03 pg/ml, P0.0001). The vitreous level of SDF-1 was also significantly higher in eyes with PDR (298.40 +/- 24.57 pg/ml) than in eyes with idiopathic macular hole (86.91 +/- 15.89 pg/ml, P0.0001). The vitreous concentration of SDF-1 correlated significantly with that of VEGF in eyes with PDR ([correlation coefficient] r = 0.62, P0.001).Vitreous levels of both SDF-1 and VEGF in patients with PDR are significantly higher than those of nondiabetic patients. SDF-1 may be correlated with VEGF in angiogenesis in PDR.

Vitreous amyloidosis is a rare condition that mainly occurs in Familial Amyloidotic Polyneuropathy (FAP). In some cases, it may be the only symptom without systemic disorders. One case of familial vitreous amyloidosis was reported here, with white, wispy opacities in vitreous cavity in both eyes. Pars plana vitrectomy and histopathological examination of the vitreous specimens were performed. The vitreous specimens showed typical microscopic features of amyloidosis with Congo red stain and non-branching fibrils on a transmission electron microscope. Transthyretin (TTR) gene was amplified with DNA isolated from the peripheral blood cells. Bi-directional sequencing of exon 3 showed a single base-pair substitution, which results in an amino acid substitution at position83, glycine to arginine (TTR Arg-83). TTR Arg-83 may be a new pathologic mutation in vitreous amyloidosis.

SiC/Mg and B(4)C/Mo/Si multilayers were designed for He-II radiation at 30.4 nm. These multilayers were prepared by use of a direct current magnetron sputtering system and measured at the National Synchrotron Radiation Laboratory, China. The measured reflectivities were 38.0% for the SiC/Mg multilayer at an incident angle of 12 deg and 32.5% for the B(4)C/Mo/Si multilayer at 5 deg, respectively. A dual-function multilayer mirror was also designed by use of the aperiodic SiC/Mg multilayer. Annealing experiments were performed to investigate the thermal stability of the SiC/Mg multilayer. The interface of the SiC/Mg multilayer before and after annealing was studied by electron-induced x-ray emission spectra, which evidences the absence of thermal reaction products at the interfaces after annealing.

Multilayer mirrors are the important optical elements for astronomical observation at extreme ultraviolet region. In this article, three kinds of multilayer mirrors were introduced for solar observation and magnetosphere observation. Mo/Si multilayer mirror was fabricated for solar Fe-XII emission line at wavelength of 19.5nm. For solar He-II radiation at 30.4 nm, Mo/Si, Si/SiC, Si/C, Si/B4C and Mg/SiC multilayers were investigated, and the measurements results shows that Mg/SiC multilayer provides the highest reflectivity of 43.8% at incidence angle of 5 degree. The third multilayer mirror was a dual-function mirror used for earth's magnetosphere observation, which requires high-reflective for He-II emission line at wavelength of 30.4nm but anti-reflectance at 58.4nm from ionosphere He-I emission. Using aperiodic Mg/SiC multilayer, the dual-function multilayer mirror was designed. Compared to periodic multilayer, the dual-function multilayer suppresses the reflectivity for He-I at 58.4nm from 2.2% to 0.1%, without loss of the reflection for He-II at 30.4nm, significantly.

The SiC/Mg and B4C/Mo/Si multilayers were fabricated for He-II radiation at 30.4nm. The measured reflectivitier were 38.0% for SiC/Mg multilayer at incident angle 12 degree, and 32.5% for B4C/Mo/Si multilayer at 5 degree, respectively.

200μg/cm2 free-standing Zr filters of 20mm in diameter were prepared .Results show that the transmittance is 19% at 13.9nm, Carbon, Oxygen and Nitrogen are the major impurities that affect transmittance in the soft X-ray region.

Multiple heterostructures inserted with defects are presented. Single and double layer guided-mode resonance (GMR) Brewster filters with multiple channels are introduced. Single and double chamber integrated optical filter arrays are fabricated.

The present status of studies on EUV, soft x-ray and x-ray multilayer in the Institute of Precision Optical Engineering (IPOE) is briefly reviewed. With the aim of realizing a Mach-Zender interferometer working at 13.9nm, we have developed a semitransparent beam splitter with multilayer deposited on the back side of a silicon nitride membrane. On the basis of the experimental optical properties of the beam splitter, design has been performed to define the multilayer structure that provides the highest product of reflectivity and transmission. Optimized Mo/Si multilayer has been successfully deposited on the back side of a silicon nitride membrane by use of the magnetron sputtering. Measurements by means of a reflectometer in Beijing Synchrotron Radiation Facility at 13.9nm and at an angle of 7.2° provide a reflectivity of 20% and a transmission of 22%. Such a beam splitter has been used for X-ray Mach-Zender interferometer at 13.9nm. The broadband multilayer analyzer in the range between 12.4nm and 20nm is designed, and made which can deviate the Quasi-Brewster's angle several degree and show very high polarization. The main feature of our design approach is the use of an analytical solution as a starting point for direct computer search, and the desired results can be given in a reasonable time. The method can be applied in different spectral range for suitable material combination. Supermirrors with broad angular band working at different wavelength such as Cu Kα line are designed, manufactured and measured. The results show that the performance of the supermirrors is in agreement with designed data.

The periodic mulitlayer with high reflectivity and small full width at half maximum (FWHM) in hard x-ray range, while the reflectivity of non-periodic multilayer decreases and FWHM increase. Therefore, the optimum coating design must be found out as a compromise between the requirements for the reflectivity and the FWHM. We have used purely numerical techniques to design broad angular multilayer mirror in angle intervals (2.9°-3.1°), which is starting from an appropriate periodic multilayer structure. In our method, the risk of local minimization of the merit function disappears, because we refined the desired depth-distribution of the period using a direct numerical algorithm and the analytical solution as a starting point for computer calculation. The plateau reflectivity can be obtained in a few minutes. The main feature of our approach is the use of an analytical solution as a starting point for direct computer search, and the desired results can be given in a reasonable time. This technique is able to design almost any given reflectivity spectrum both energy- and angle-dependent and in a reasonable amount of time. The periodic and non-periodic W/Si multilayer for grazing incidence multilayer mirrors at the K-edge of Ti (0.275 nm) were both designed and fabricated by high vacuum DC magnetron sputtering coater model JGP560C6, and the multilayer films were characterized by X-ray reflectivity measurements on a laboratory x-ray diffractometer(XRD) and the atomic force microscope (AFM). We find good agreement of the changing trend of surface roughness between the simulation of XRD and measurement of AFM.

We designed two kinds of supermirrors composed of Carbon and Tungsten in current paper. Using Simplex Optimization method, we designed C/W supermirror with broad incident angular range (0.5°~0.9°) at Cu Kα line (λ=0.154nm). Connecting the analytical method, based on oversimplified analytical and semi-empirical formulas, with the Simplex Optimization method, we designed C/W supermirror with broad photon energy range (16~25keV), at θ=0.5°. The negative effect, due to the interfacial roughness and diffusion between the adjacent sublayers in multilayer, also emerges in simulating the practice performance of the both supermirrors. The supermirrors with broad incident angular range were fabricated by DC magnetron sputtering, because such supermirror is easy to be measured at our lab, using X-ray diffractormeter. The measured reflectivity near the first order Bragg peak is about 30% at Cu Kα line. The roughness factor is about 0.84nm by the fitting data.

The broadband x-ray supermirrors have been designed, fabricated and studied experimentally. They are intended for operating in the photon energy range from 12.4 to 20keV at the fixed grazing incident angle of 0.5°. The choice of material pairs composing a non-periodic multilayer structure is considered from the maximum achievable reflectivity and the layer structure stability. Tungsten and silicon are selected, which have the great index contrast in this energy range and are suitable for fabrication with the use of the vested coating system. The interface width determined by transmission electron microscopy (TEM) lies in the range of 0.4~0.6nm. Following a theoretical approach including analytical and numerical techniques, the designed multilayer mirrors have a practically constant reflectivity of about 24% in the desired photon energy range. The multilayers were deposited onto polished silicon substrates by a high vacuum DC magnetron sputtering system and were characterized by x-ray diffractormeter (XRD) at 8.0keV. The experiments show that the sample has about 10% reflectivity in a wide angular range; The roughness of the interface for both tungsten on silicon layer and silicon on tungsten layer was estimated to be about 0.5nm. Oscillations in the reflectivity curve proved to be larger than the expected ones. They may be caused by the random variation of the layer thickness, as well as the interdiffusion between two materials. Possibilities for further improvements of wideband multilayer mirrors are analysed as well.

The status of polarizing optical elements for the soft x-ray range is reviewed. The criteria for optimum polarization of soft x-ray reflective analyzers, transmission polarizers and phase retarders based on multilayer interference structures are presented. Following these principles, soft x-ray polarizing optical elements have been designed. Designs of broad angular and wavelength range reflective analyzers based on a combination of analytical and numerical methods are also discussed.

K-B microscope intended for the use in inertial confinement fusion experiments was designed. The microscope operates at the 8keV x-ray energy and provides the 8X magnification. The parameters of the microscope are decided by requirements of ICF experiments. Ray tracing software (Zemax) is used to simulate optical system performance. Grazing angle range on the surface of mirrors and the assembly tolerance of centre grazing incident angle were both calculated. For the working energy is 8 keV, in order to obtain sufficient reflectivity at about 1° grazing angle on each mirror, multilayer should be coated on the mirrors. Two kinds of multilayer, periodic multilayer and non-periodic multilayer (supermirror), are discussed in the paper. Take into account the grazing angle ranges on the mirrors and the grazing angle tolerance, it is necessary to have a fairly constant reflectivity over a wide angular domain. Periodic multilayer has narrow bandpass, which cannot fulfill the requirement of such wide angular domain. The non-periodic structure multilayer was designed and fabricated. The results show this kind of non-periodic multilayer can be used in K-B microscope.

To evaluate short-term effects of single photodynamic therapy (PDT) for age-related macular degeneration (AMD) accompanied with choroidal neovascularization (CNV).We analyzed retrospectively the effects of single PDT for 20 patients (20 eyes) with CNV caused by AMD. Corrected visual acuity, fluorescein angiography (FA) and optic coherence tomography (OCT) were examined before and after PDT. All patients were followed up at least 3 months.At the end of 3-month follow-up, 5 eyes had vision progress, 15 eyes had vision stable and no eye had vision deterioration. Fluorescein angiography one week post PDT showed cessation of fluorescein leakage in 8 eyes with predominant classic CNV, and reduction of fluorescein leakage in 12 eyes with minimal classic CNV or occult CNV without classic component. At the 3-month following PDT fluorescein angiography showed fluorescein leakage reappeared in 4 of 8 eyes with predominant classic CNV. Among 12 eyes with minimal classic CNV or occult CNV without classic component, 9 eyes showed decreased or unchanged fluorescein leakage, 3 eyes had a progression of fluorescein leakage. Optic coherence tomography showed obvious recovery of serous sensory retinal detachment after PDT.PDT may occlude or inhibit CNV caused by AMD in short-term. No obvious side effects were noticed.

e13533 Background: Some studies postulated that the plasma concentration of gefitinib may have great influence on its efficacy; meanwhile, it is well-known that polymorphisms in metabolic enzymes a...

A remarkable magnetostriction λ111 as large as 6700 ppm was found at 70 K in PrFe1.9 alloy. This value is even larger than the theoretical maximum of 5600 ppm estimated by the Steven's equivalent operator method. The temperature dependence of λ111 for PrFe1.9 and TbFe2 alloys follows well with the single-ion theory rule, which yields giant estimated λ111 values of about 8000 and 4200 ppm for PrFe1.9 and TbFe2 alloys, respectively, at 0 K. The easy magnetization direction of PrFe1.9 changes from [111] to [100] as temperature decreases, which leads to the abnormal decrease of the magnetostriction λ. The rare earth sublattice moment increases sharply in PrFe1.9 alloy with decreasing temperature, resulting in the remarkably largest estimated value of λ111 at 0 K according to the single-ion theory.

ZrO 2 thin films were prepared by sol-gel technology from suitable zirconia aqueous colloidal suspensions containing nano-crystalline ZrO 2 at room temperature synthesized by hydrothermal process from inorganic precursor (ZrOCl 2 (DOT) 8 H 2 O). By adding a soluble organic binder PVP to the suspension prior to application, it substantially increased the coating refractive index and the abrasion- resistance as well as the laser damage threshold. The features of the coatings and the colloidal suspensions were investigated. Multilayer highly reflective dielectric coatings were also elaborated by laying down quarterwave- thick alternating coatings of the binder-aided zirconia and silica, which was prepared with the sol-gel process from TEOS. Laser damage thresholds of 20 and 18 J/cm 2 (1064 nm, 1 ns) were achieved for single ZrO 2 -PVP coating and ZrO 2 -PVP/SiO 2 multilayers respectively.

Oxide growth on rare-earth erbium film at room temperature was quantitatively followed by means of quartz oscillation technique. Structure and chemistry of the oxide layer were characterized by x-ray diffraction and x-ray photoelectron spectroscopy. The humidity in oxidizing environment is found to be the key factor leading to the increase of oxidation rate of the erbium film. The oxide layer is composed of crystallites of erbium and erbium oxide. The O 1s photoelectron spectra are characterized by two components that are assigned to oxide and hydroxide species respectively. The oxide layer shows a layered structure with an oxide layer covered by a hydroxide overlayer.© (2000) COPYRIGHT SPIE--The International Society for Optical Engineering. Downloading of the abstract is permitted for personal use only.

TiO2 nanoparticle thin films are fabricated via sol-gel process followed by dip and spin coating technique, using Ti(OC4H9)4 as raw material. A complexing agent is used in order to form a stable sol. Experiments show that the colloidal particles in the sols are relatively large under basic catalyst conditions, while under acidic conditions, the colloidal particles are only about several nanometers. The properties and structures of the films are studied. The films are normally homogenous and crack-free. TEM shows that the films are composed of nanoparticles with a certain porosity. Under the thermal treatment of 80 degrees Celsius, the porosity and thickness of the film decrease while the refractive index increases from the original 1.70 to the final 1.89. When the temperature of the thermal treatment goes up, the size of the nanoparticles increases and crystallization occurs.© (1998) COPYRIGHT SPIE--The International Society for Optical Engineering. Downloading of the abstract is permitted for personal use only.

Theoretically, the spectral resolution of a multilayer can be improved through a combination of utilizing high reflectance orders and by decreasing the thickness of the scattering layer. We fabricate Mo/Si multilayers in the first, second, third, fourth and fifth reflectance orders with Mo layer thicknesses of 3.0 nm and 2.0 nm, respectively, using direct current magnetron sputtering. The structure of the multilayers is characterized with a grazing angle x-ray diffractometer (XRD). Then the reflectivity of the multilayers is measured in a synchrotron radiation facility. The results show that the spectral resolution increases with the increasing reflectance order and with the decreasing Mo layer thickness. The highest spectral resolution is improved to 117.5 in the 5th order for dMo = 2 nm, where the reflectivity is 18%.

We propose and demonstrate three approaches to achieve narrowband multichannel filters. These are multiple heterostructures with defects, guided-mode resonance (GMR) Brewster filters with multiple channels, and integrated narrow bandpass filter arrays. Transmission studies for multiple heterostructures with defects are presented. We show that the enlargement of the forbidden band and multiple-channel filtering can be reached simultaneously with these configurations. GMR Brewster filters with multiple channels can be obtained with a single-layer grating. The same properties can be obtained by use of double-layer structures that consist of a homogeneous layer and a grating with equal refractive index. We developed a combinatorial etching technique that has 32 elements on a single substrate with which to fabricate integrated narrow bandpass filters. Single- and double-chamber integrated optical filter arrays were fabricated by use of this etching technique. These narrowband multichannel filters and narrow bandpass filter arrays show good filtering features and can be utilized in many optical applications.

The polarization state of the BESSY UE56/1-PGM beamline radiation in the broad wavelength range of 12.7–15.5nm was measured using a molybdenum/silicon transmission phase retarder and a reflection analyzer with aperiodic multilayer interference structures, which can broaden the spectral response of these optical elements. The characteristics of the circular polarized undulator radiation, as well as the polarization properties of the two polarizing elements, were determined by a complete polarization analysis. Furthermore, the polarization of the radiation as a function of the undulator shift setting was also measured at the wavelength of 13.1nm by use of the broadband phase retarder-analyzer pair.

Experimental results on aperiodic broadband transmission molybdenum/silicon multilayer phase retarders for the extreme ultraviolet range are presented. The broadband phase retarders were designed using a numerical method and made using direct current magnetron sputtering on silicon nitride membrane. The polarization properties of these aperiodic transmission phase retarders have been investigated using the soft x-ray polarimeter at BESSY-II. The measured phase shift was about 42° in the wavelength range of 13.8–15.5nm, and the corresponding s-component transmission (Ts) decreased from 6% to 2% with increasing wavelength.

In this paper, double-layer surface-relief resonant Brewster filters consisting of a homogenous layer and a grating with equal refractive index are obtained by adjusting the grating filling factor, and linewidth properties of these types of filters are investigated. It is shown etch depth error does not change the filter linewidth, but the grating filling factor and the substrate refractive index can significantly change the filter linewidth. Moreover, the coupling strength can be appreciately affected by the homogeneous layer thickness, and one can obtain different linewidths at the same operating wavelength by selecting different homogeneous layer thickness with other physical parameters maintained.

In this letter, the double-layer resonant Brewster filters and their properties were presented, which consist of a homogenous layer with a refractive index equal to that of the grating. By tuning the thickness of the homogeneous layer, a multichannel resonant Brewster filter with thin grating thickness can be obtained. For this type of filters, the variety of the grating thickness almost did not change the resonance location, but had a distinct effect on the filter linewidth. By changing grating period or tuning incident angle, different linewidths can be obtained at the same resonance wavelength without losing the low-reflection sideband feature.

Broadband extreme ultraviolet molybdenum/yttrium aperiodic multilayer analyzers were designed for polarization experiments in 8.5–11.7nm wavelength range. The multilayer analyzers were made using direct current magnetron sputtering and characterized using the soft x-ray polarimeter at BESSY-II facility. Measured s reflectivities at the Brewster angle are 5.5% for a multilayer designed for 8.5–10.1nm wavelength range and 6.1% for one designed for 9.1–11.7nm. The multilayers also exhibit high polarization degree up to 98.79%. In addition, the multilayer was also measured over 38°–52° angular range at the fixed wavelength of 10.2nm and the mean s reflectivity is 6.2%.

In this letter, a type of guided-mode resonance (GMR) reflection filter incorporating multimode resonance and the Brewster effect is presented. Long-range, low sidebands, and multiple channels are found to be obtainable for a single-layer GMR reflection filter with a TM-polarized plane wave incident at the Brewster angle. Detailed characteristics are calculated using rigorous coupled-wave analysis. In our calculation, for TM-polarized incident wave, we find it sufficiently accurate to calculate the effect index by using the zero-order permittivity e0,TM of the effective media theory, and narrowband multichannel reflectance can be achieved at the Brewster angle by tuning the grating depth.

Nonperiodic molybdenum/silicon broadband multilayer polarizers have been designed using numerical optimization algorithm and fabricated using direct current magnetron sputtering. Their performances have been characterized using the high precision eight-axis soft x-ray polarimeter at the BESSY facility. Different multilayers have measured s-polarized reflectivities of 27% at 13.1nm and higher than 15% over the wavelength range of 13–19nm. Nearly constant s reflectivity, up to 37%, is observed over the 15–17nm wavelength range, where the degree of polarization is more than 98%. Furthermore, these multilayer polarizers also show high s reflectivity and polarization over a broad angular range at fixed wavelength.

The design, fabrication and characterization of the X-ray supermirrors are discussed in this paper. Using the local optimization method of simplex algorithm and the global one of simulated annealing algorithm with different initial multilayer structures, we designed the broad angular band supermirrors with different grazing incidence angle intervals at the energy of 8.0 keV (the Kα line of Cu) and the broad energetic band supermirrors with different energy intervals at fixed grazing incidence angles. The fabricating techniques for depositing non-periodic multilayers are also studed. The W/C and W/Si supermirrors are deposited on silicon substrates and characterized by a high resolution X-ray D1 diffractometer from Bede Company, UK. Choosing the interface roughness and the densities of the materials as independent variables, some measured reflectivity curves are fitted using the Debye-Waller factor with interface roughness. The experimental results show that the optical performances of the fabricated supermirrors are in agreement with the designed ones.

One-dimensional metallodielectric heterostructural photonic band gap (PBG) material is designed to reach high transmittance band in short wavelength, broad and deep forbidden band in long wavelength, especially sharp cutoff edge between the transmission and forbidden bands. The designed PBG material is applied to modify the emission spectrum of a BaF2 scintillator and is proved to be adequate to suppress the slow component of the scintillation light. The suppression ratio of the slow to the fast component reaches 28dB with a tolerable attenuation of the fast component.