1. Cellulose nanocrystal extraction from tissue paper wastes using different extraction methods and cellulose acetate production.
- Author
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Saleh, M., M’barek, I., and Dizge, N.
- Subjects
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ENERGY dispersive X-ray spectroscopy , *WASTE paper , *CELLULOSE synthase , *SCANNING electron microscopy , *INFRARED spectroscopy , *CELLULOSE acetate - Abstract
This paper examines the feasibility of extracting cellulose from tissue paper wastes (TPW’s) using several methods: sonication (SC), subcritical (SU), microwave (MC), and microwave with diluted acid (MA). The chemical characterisation and morphological properties of nanocrystal cellulose were investigated using Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and scanning electron microscopy with energy dispersive X-Ray analysis (SEM-EDX). TPW’s have a relatively high crystallinity index (CrI = 61.02%). It was found to be lower than that for cellulose extracted using SU and SC MC, MA methods, where CrI to 65.65%, 68.07%, 69.21% and 73.42%, respectively. The MA method yielded cellulose with the highest CrI and altered surface morphology. This cellulose was selected for cellulose acetate synthesis. After acetylation, the CrI decreased to 61.45%, and the morphological aspect was changed. In conclusion, nanocrystal cellulose was successfully extracted from TPW’s and effectively changed to its esterified form. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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