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The effect of hydrogen on the structural change of vacancies in tungsten is analyzed by molecular dynamics in order to clarify the interaction between vacancies and hydrogen in tungsten. Simulations are performed at different temperatures (573, 773, 1073 K) and with different numbers of hydrogen in the vacancies (0, 18, 36, 54). Evaluating (1) isopotential surface for the increase of total potential energy, (2) the root mean square deviation (RMSD) of tungsten atoms, (3) the root mean square fluctuation (RMSF) of tungsten atoms and (4) density distribution in radial direction, we found that the presence of a large number of hydrogen in a vacancy at each temperature caused changes in the structure. This fact partially supports the experimental fact that in the coalescence of two tungsten vacancies, the retention of hydrogen activates them., source:https://doi.org/10.15748/jasse.10.132, identifier:0000-0002-0593-8810

A fiberform nanostructured layer is formed on a tungsten (W) surface using helium (He) plasma irradiation. The behavior of the nanostructures and He bubbles were observed during annealing via in situ transmission electron microscopy. Notable changes in the nanostructures occurred at 1223 K. A collapse of the nanostructures was observed along with a collapse of the He bubbles during annealing., source:https://doi.org/10.1585/pfr.11.1206125, identifier:0000-0002-2023-9786

We have developed a compact divertor plasma simulator (CDPS) that can produce steady-state deuterium and/or helium plasmas with densities above ∼ 1018 m−3 for Plasma-Wall Interaction (PWI) studies of neutron-irradiated materials. The maximum particle flux is about 1022 m−2s−1. The CDPS was installed and is being operated in the radiation-controlled area of the International Research Center for Nuclear Materials Science, Institute for Materials Research, Tohoku University. We are able to control sample temperature within uncertainty of 5 °C during plasma exposure by adjusting the cooling air flow rate to the sample holder. The CDPS has a sample-carrier system, which makes it possible to transfer a plasma-irradiated sample from the sample holder to an infrared heater for analysis using thermal desorption spectroscopy (TDS) without exposing it to the air. This avoids the oxidation of the sample and minimizes the time between the end of plasma exposure and TDS analysis. An ITER-like tungsten (W) sample (A.L.M.T. Corp.), which has been irradiated by neutrons to 0.06 dpa in a fission reactor, was exposed to a deuterium plasma in the CDPS. The experimental results clearly show that the total deuterium retention in the neutron-irradiated W sample increases significantly in comparison with a pristine W, as demonstrated by broadening of the TDS spectrum at high temperatures., source:https://doi.org/10.1585/pfr.12.1405040, identifier:0000-0001-7826-0046

This overview presents recent results regarding hydrogen isotope absorption and emission dynamics in neutron-irradiated tungsten (W) using our recently developed Compact Diverter Plasma Simulator (CDPS), a linear plasma device in a radiation-controlled area. Neutron irradiation to 0.016 - 0.06 displacement per atom resulted in a significant increase in deuterium (D) retention due to trapping effects of radiation-induced defects. We analyzed the dependency of D retention on the D plasma fluence by exposing neutron-irradiated pure W to D plasma at 563 K over a range of D fluence values. The total retention was revealed to be proportional to the square root of D fluence, indicating that the implanted D atoms first occupy the defects caused by neutron-irradiation near the surface and then the defects located in deeper regions. We further investigated the effects of post-plasma annealing on D emission; neutron-irradiated pure W was exposed to D plasma at 573 K and was then annealed at the same temperature for 30 hours. Approximately 10% of the absorbed D was released by annealing, suggesting that a heat treatment of the plasma-facing component of a fusion reactor at moderately elevated temperatures could contribute to the removal of accumulated hydrogen isotopes. The experimental results obtained in this study were only available by investigating neutron-irradiated specimens with the CDPS system, which will be essential for future studies of material behavior and plasma-wall interactions in the fusion reactor environment., source:https://doi.org/10.1585/pfr.15.1505081

A tungsten (W) deposition layer is formed while a sample is exposed to a helium (He) plasma at the surface temperature of 473 or 573 K. The formed He-W co-deposition layer was composed of fine grains, the size of which increased with the surface temperature. The samples with the co-deposition layer was exposed to a deuterium (D2) plasma, and the D retention was investigated using thermal desorption spectroscopy. It was found that the co-deposition layer has quite different D retention characteristics compared with bulk W., source:https://doi.org/10.1585/pfr.15.1201004

Arcing experiments were conducted in the linear plasma device Pilot-PSI, where a pulsed plasma was superimposed to a steady state plasma. The arcing was observed by a fast framing camera, and the sample was analyzed with a transmission electron microscope. Observations of glowing objects released from the sample in response to the arcing and destruction of the fuzzy layer at the edge of the arc trail without significant melting suggested that dust was formed and released from the surface in response to arcing., source:https://doi.org/10.1585/pfr.15.1205061, identifier:0000-0002-2023-9786

The Large Helical Device (LHD) started the deuterium plasma experiment on March 7, 2017. Approximately 6.4 GBq of tritium was produced in the first deuterium plasma experiment campaign and were utilized as tracers for the investigation of release behavior and the balance of tritium in the LHD vacuum vessel. To determine the tritium balance in LHD, the tritium release from the vacuum vessel was continually observed during the plasma experiment period and the vacuum vessel maintenance activities. The tritium exhaust rate was approximately 32.8% at the end of the plasma experiment. After the plasma experiment, the vacuum vessel was ventilated by room air for the maintenance activity and the tritium release from the in-vessel components was observed. The tritium release rate gradually decreased and became constant after four-month in spite of water vapor concentration. It is suggested that the tritium release mechanism from the vacuum vessel is a diffusion-limited process from the bulk. The tritium release amount during the maintenance activity for one year was approximately 5.0%. Considering the decrease of tritium decay for 1.5 years, tritium inventory in LHD was estimated to be approximately 3.66 GBq (57.2%) at the end of maintenance activity., source:https://doi.org/10.1585/pfr.15.1405062, identifier:0000-0001-9941-1958

An innovative color measurement technique is employed in the Large Helical Device (LHD). This study provides a method for obtaining in broad spatial extent and in great detail the color information of the first wall relating to the thickness of the deposition layer. The RGB (Red, Green, and Blue) value, mainly of the stainless steel plates on the helically twisted coil, is measured by a color analyzer equipped with an integrated sphere light source. On the outer torus side, the colors of almost all stainless steel plates are close to carbon black, which suggests that deposition is dominant. On the inner torus side, all plates except for those neighboring the carbon divertor plates are almost white, as in the case of the stainless steel substrate of the first wall, which suggests that erosion is dominant. The relationship between the color and the distance from the stainless steel plates to the plasma is investigated., source:https://doi.org/10.1585/pfr.10.1202074, identifier:0000-0001-5522-3082

Nanostructured tungsten formed by the exposure to helium plasma in a linear plasma device was installed in the large helical device (LHD). After the exposure in a series of experiments in the 2012 fiscal year campaign in LHD, the samples were analyzed by scanning electron microscope (SEM), transmission electron microscope (TEM), and energy dispersion x-ray spectroscopy (EDX). It was found that part of the nanostructures was totally covered with carbon based material probably from divertor, while some other parts were eroded by sputtering. On the erosion dominant region, it was revealed that the head part of nanostructures was sputtered and the surface became rounded, but the nanostructures still remained near the surface. Optical reflectance of the material was measured, and it was found that the morphology changes increased the optical reflectivity up to ∼10% from typically less than 1%. The possibility and limitation of the nanostructured tungsten as a light absorber (viewing dump) are discussed., source:https://doi.org/10.1585/pfr.10.1402083, identifier:0000-0003-0543-5241

Remaining tritium in the vacuum vessel after the first deuterium plasma experimental campaign conducted over four months was investigated in the large helical device (LHD) for the first time in stellarator/heliotron devices by using the tritium imaging plate technique. In-vessel components such as divertor tiles and first wall panels, and long-term material probes retrieved from the vacuum vessel were analyzed. The in-vessel component in which tritium remained most densely is the baffle part of divertor tiles made of graphite retrieved from the inboard-side divertor. Asymmetric tritium retention is observed on divertor tiles located at magnetically symmetric positions, and can be attributed to the toroidal field direction dependence of the asymmetric loss of energetic tritons generated by deuterium–deuterium nuclear fusion reactions. On the first wall, tritium remained in a deposited layer, which mainly consists of carbon., source:S Masuzaki et al 2020 Phys. Scr. 2020 014068, source:https://doi.org/10.1088/1402-4896/ab6d44, identifier:0000-0003-0161-0938

Distributions of deposits and hydrogen (H) on the graphite divertor target elements TM4h4 and TM3v5 in the test divertor units 3 (TDUs3) of Wendelstein 7-X (W7-X) are studied. The TM4h4 and TM3v5 are located at the magnetically symmetric positions in the upper and lower divertor. The microstructure of the deposition layer is characterized by a transmission electron microscope (TEM) combined with a focused ion beam (FIB). Metallic deposits such as iron (Fe), molybdenum (Mo), chromium (Cr) are detected in the deposition layer by energy-dispersive x-ray spectroscopy (EDS). The depth-resolved distribution patterns of boron (B) and metallic deposits on upper and lower horizontal (h) divertor target elements TDUs3-TM4h4 as well as upper and lower vertical (v) divertor target elements TDUs3-TM3v5 are clarified by glow discharge optical emission spectrometry (GDOES). Results for both TDUs3-TM4h4 and TDUs3-TM3v5 show that the B deposition regions exhibit higher H retention due to the co-deposition with deposits. On the other hand, up-down asymmetries in B deposition caused by particle drift exist on both TDUs3-TM4h4 and TDUs3-TM3v5. The B deposition amount on upper TDUs3-TM4h4 is 40% smaller than that on lower TDUs3-TM4h4. While for the vertical target elements, the B deposition amount on upper TDUs3-TM3v5 is 35% larger than that on lower TDUs3-TM3v5. Meanwhile, a shift of around 3 cm in B deposition peaks is observed on upper and lower TDUs3-TM4h4 and TDUs3-TM3v5. Results of numerical simulation of carbon deposition/erosion profiles on the target elements using ERO2.0 code and power flux measured by infrared cameras are shown and compared with the above mentioned B profiles., source:Mingzhong Zhao et al 2022 Nucl. Fusion 62 106023, source:https://doi.org/10.1088/1741-4326/ac8c56, identifier:0000-0001-5089-3642

0000-0003-0161-0938, Remaining tritium in the vacuum vessel after the first deuterium plasma experimental campaign conducted over four months was investigated in the large helical device (LHD) for the first time in stellarator/heliotron devices by using the tritium imaging plate technique. In-vessel components such as divertor tiles and first wall panels, and long-term material probes retrieved from the vacuum vessel were analyzed. The in-vessel component in which tritium remained most densely is the baffle part of divertor tiles made of graphite retrieved from the inboard-side divertor. Asymmetric tritium retention is observed on divertor tiles located at magnetically symmetric positions, and can be attributed to the toroidal field direction dependence of the asymmetric loss of energetic tritons generated by deuterium–deuterium nuclear fusion reactions. On the first wall, tritium remained in a deposited layer, which mainly consists of carbon.