1. Effects of immersion in 4-methacryloyloxyethyl trimellitate anhydride/methyl methacrylate-tri-n-butyl borane resin-activated liquid on microtensile bond strength of root canal dentin
- Author
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Taisuke Ozaki, Shiho Otake, Wataru Komada, Shinya Oishi, and Kenji Fueki
- Subjects
4-Methacryloxyethyltrimellitic acid anhydride ,Adhesives ,Dentin ,Methylmethacrylate-tributylborane resin ,Microscopy ,Confocal ,Dentistry ,RK1-715 - Abstract
Background/purpose: 4-methacryloyloxyethyl trimellitate anhydride/methyl methacrylate-tri-n-butyl borane (4-META/MMA-TBB) resin is used for indirect restorations. We aimed to evaluate effects of immersion in 4-META/MMA-TBB-activated liquid on the bond strength of root canal dentin. Materials and methods: We used freshly extracted single-rooted human teeth. After decoronation, each root was vertically sectioned into halves; their dentin walls were polished and flattened. The control group underwent dentin treatment with Green Activator. The immersion group was treated with Green Activator and Teeth Primer and immersed in 4-META/MMA-TBB-activated liquid. After bonding the resin blocks with Super-Bond, microtensile bond strength (μTBS) tests were performed (n = 6), and fracture surfaces were analyzed. Before surface treatment, dentin was immersed in a sodium fluorescein solution for 3 h, and resin blocks were bonded with Super-Bond with rhodamine B as in the bond strength test. The bonded cross section was observed using confocal laser scanning microscopy (CLSM). Results: μTBS was significantly higher in the immersion group than in the control group (61.5 [51.3–66.7] vs. 33.0 [20.4–57.8] MPa; P
- Published
- 2024
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