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1. Color tuning of a nickel complex with a novel N(sub 2)S(sub 2) pyridine-containing macrocyclic ligand

Author

Tamayo, Abel, Brondino, Carlos D., Casabo, Jaume, Kivekas, Raikko, Escriche, Lluis, Sillampaa, Reijo, Lodeiro, Carlos, and Covelo, Berta

Subjects
Nickel compounds -- Structure, Nickel compounds -- Chemical properties, Pyridine -- Structure, Pyridine -- Chemical properties, Alcohol -- Structure, Alcohol -- Chemical properties, Alcohol, Denatured -- Structure, Alcohol, Denatured -- Chemical properties, Acetonitrile -- Structure, Acetonitrile -- Chemical properties, Chemistry
Abstract

The novel pyridine-containing 14 membered macrocycle 3,11-dithia-7,17-diazabicyclo[11.3.1]heptadeca-1(17),13,-15-triene (L), which contains an N(sub 2)S(sub 2) donor set was synthesized and its protonation behavior was studied. The reactions between L and NiX(sub 2).6H(sub 2)O in ethanol or acetonitrile afforded the octahedral complexes and the square -planar complex [Ni(L)]-(X)(sub 2) were obtained by heating these octahedral complexes.

Published
2006

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