1. Fabrication of Nitrogen Functionalized Carbon Nanofiber Nanocomposite Using Activated Carbon Derived from Lantana Camara for the Electrochemical Detection of Ofloxacin.
- Author
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Sahil, Bharati Jaryal, Vishal, Singh, Dilbag, and Gupta, Neeraj
- Subjects
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CARBON-based materials , *FIELD emission electron microscopy , *SCANNING transmission electron microscopy , *LANTANA camara , *FOURIER transform infrared spectroscopy , *CARBON nanofibers - Abstract
Efforts to mitigate the environmental and health risks associated with the antibiotic ofloxacin necessitate innovative methodologies for its detection. The cost of expensive carbon materials like carbon nanofibers can be reduced by making their hybrids with biomass‐derived carbon materials. In this context, a nitrogen‐functionalized carbon nanofiber‐based nanocomposite (N‐LN‐CNF), incorporating activated carbon derived from Lantana Camara, was fabricated for the detection of ofloxacin. X‐ray photoelectron spectroscopy and Fourier Transform Infrared analyses confirmed the presence of nitrogen functionalities in the N‐LN‐CNF. The surface and internal morphology were analyzed using field emission scanning electron microscopy and high‐resolution transmission electron microscopy. The material was tested as an electrochemical sensor for ofloxacin detection. A linear response for ofloxacin was observed in the range of 2 μM to 43 μM for N‐LN‐CNF/GCE via linear sweep voltammetry (LSV) with a limit of detection (LOD) of 1.92 μM. The interaction between the fabricated electrode and the analyte is a combination of diffusion and adsorption‐controlled processes. This metal‐free sensor offers a sustainable approach for detecting ofloxacin in water and pharmaceutical preparations. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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