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1. Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition.

Author

Pathak, Uma, Kumar Pandey, Lokesh, and Tank, Rekha

Subjects
*CARBONYL compounds, *SULFURATION, *ORGANIC synthesis, *MICROWAVES, *IRRADIATION
Abstract

A novel thionation protocol for carbonyl compounds, with the system PSCI3IH2OIEt3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation. [ABSTRACT FROM AUTHOR]

Published
2008
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