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Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition.
- Source :
-
Journal of Organic Chemistry . 4/4/2008, Vol. 73 Issue 7, p2890-2893. 4p. 1 Chart. - Publication Year :
- 2008
-
Abstract
- A novel thionation protocol for carbonyl compounds, with the system PSCI3IH2OIEt3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation. [ABSTRACT FROM AUTHOR]
- Subjects :
- *CARBONYL compounds
*SULFURATION
*ORGANIC synthesis
*MICROWAVES
*IRRADIATION
Subjects
Details
- Language :
- English
- ISSN :
- 00223263
- Volume :
- 73
- Issue :
- 7
- Database :
- Academic Search Index
- Journal :
- Journal of Organic Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 31830624
- Full Text :
- https://doi.org/10.1021/jo7022069