1. An Investigation on the Flexural and Thermo-mechanical Properties of CaCO3/Epoxy Composites.
- Author
-
Baştürk, S. Bahar
- Subjects
EPOXY compounds ,CANTILEVER roofs ,TENSION loads ,SCANNING electron microscopes ,BENDING moment - Abstract
Present work focused on the flexural and thermo-mechanical characteristics of epoxy based composites filled with 3 different calcium carbonate (CaCO
3 ) concentrations: 1.5, 3 and 5 wt.%. Composite specimens were fabricated through conventional casting method and subjected to flexural test via 3 point bending fixture. Additionally, dynamic-mechanical analyzer (DMA) with single cantilever mode was used to reval the thermo-mechanical responses of samples. The findings showed that the filler concentration increase led to the increase of storage modulus (E') for all specimens while the glass transition temperature (Tg ) slightly decreased for 1.5 wt. % CaCO3 filled epoxy composite. The 5 wt.% CaCO3 loaded composite showed maximum E' and Tg values with 10% and 1.5% improvement, respectively. Based on flexural test results it was surprisingly found that, 1.5% wt. CaCO3 addition attained the highest strength with ~30% improvement among all samples. However, 5 wt.% CaCO3 introduced composites displayed the lowest mechanical performance due to the presence of agglomerates/tactoids, which was verified from SEM images as well. [ABSTRACT FROM AUTHOR]- Published
- 2022
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