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Double – Double (DD) is a new family of laminates that holds the potential to completely overhaul the design of composite structures. These laminates are not only lighter and more robust than the classical QUAD laminates, but they also accelerate manufacturing processes and reduce costs. However, the application of DD laminates as substrates in adhesive joints has not been studied so far. In this work, end-notched flexure (ENF) tests with composite substrates are performed in both QUAD and DD configurations. The main goal is to evaluate the maximum load and shear fracture energy for both laminates. Additionally, the displacement fields are measured through the digital image correlation (DIC) analysis. Experimental results showed that DD laminates can significantly improve the shear fracture energy of adhesive joints and also delay the crack propagation over the test. The findings presented herein could play a crucial role in driving significant alterations in the design procedures of adhesive joints with composite materials, highlighting the DD advantages. [ABSTRACT FROM AUTHOR]

This paper aims to examine the behavior of cracked adhesive joints experimentally and numerically when they are subjected to quasi-static and dynamic loads using the tensile and falling-wedge impact tests, respectively. Double cantilever beam (DCB) specimens were manufactured and tested under impact loading with varying impact energies to analyze the adhesive joint mode-I dynamic fracture response. To determine quasi-static and dynamic mode-I fracture energies, the compliance-based beam method (CBBM) was utilized accounting for the axial force exerted by the wedge. It was found that by changing the loading condition from quasi-static to impact, the maximum force and fracture energy of adhesively bonded joints were considerably increased by 275% and 452%, respectively. However, within the impact test conditions, increases of 10% and 22% were obtained in maximum force and fracture energy when the impact energy was tripled. The adhesive joints tested under static loading experienced a mixed interfacial/cohesive failure pattern, whereas by shifting the loading condition to impact, the failure pattern turned fully cohesive. The quasi-static and dynamic fracture responses of adhesive joints were modeled using the cohesive zone model employing a triangular traction-separation law. The numerical and experimental results exhibited reasonable correlation. [ABSTRACT FROM AUTHOR]

The resurgence of interest in hybrid joints, combining adhesive bonding with mechanical fastening in engineering applications, is driven by the recognition of unique advantages and limitations inherent in each joining method. Unlike conventional bonded joints with precise adhesive thickness control, hybrid joints involving pre-tensioned bolts depend on a process termed squeeze-flow, influenced by joint geometry, adhesive viscosity, and adhesive filler presence. A method for the precise measurements of the adhesive layer thickness, conducted at 5 mm intervals, proved its accuracy and repeatability. The results revealed the significant impact of adhesive viscosity and filler characteristics on adhesive layer thickness. Viscosity, while playing a central role, is not acting in isolation, as filler properties collectively influence adhesive layer thickness distribution and bonding performance. The complexity of this relationship underscores the interplay between adhesive layer thickness, viscosity, filler content, and load-bearing capacity. Smaller-sized fillers result in thinner layers and reduced load capacities, while adhesives with larger particles exhibit higher load capacities. This complexity emphasizes the need for a nuanced approach when selecting adhesives for specific applications, considering not only viscosity but also filler attributes to optimize bonding performance in hybrid joints. [ABSTRACT FROM AUTHOR]

In this paper, an attempt was made to determine the load-bearing capacity of a bonded joint of galvanized steel elements with carbon fiber reinforced polymer (CFRP) fabric. This issue is extremely relevant to the use of bonded carbon fiber fabric as a mean of reinforcing hot-dip galvanized steel structures. This technique is used in engineering practice for both hot-rolled and cold-formed steel elements. In order to obtain the necessary parameters for modelling bonded joints of galvanised steel thin-walled elements, laboratory tests were carried out. In the first stage, four specimens made of 50 mm diameter steel cylinders bonded to 16 mm thick hot-dip galvanised steel sheet of S350 GD were subjected to the pull-off test. In this connection the SikaWrap 230C composite fabric embedded in SikaDur 330 adhesive layer was investigated. In the second stage, the axial tensile test of the bonded butt joint using the same materials was performed. In this stage, 10 hot-dip galvanised steel sheet samples of S350 GD and 16 mm thickness were tested. The discussion on the failure mechanism in the context of the bonding capacity of the composite joint was carried out. Moreover the advanced numerical model using the commercial FE program ABAQUS/Standard and the coupled Cohesive Zone Model was developed. The significant influence of the preparation method of steel element surface and the thickness of the adhesive layer on the failure mechanism of the joint and the value of the maximum failure force was shown. [ABSTRACT FROM AUTHOR]

The purpose of the work is to present issues related to the influence of surface treatment on the strength of adhesive joints of C45 steel sheets by grinding based on experimental research. These issues were related to determining the impact of the gradation and type of abrasive material on the strength of adhesive joints of the steel sheets. The grinding was carried out manually using an angle grinder with a disc diameter of 125 mm and a rotational speed of 11.060 min-1, using abrasive materials with grains made of: ceramics, zirconium and electro-corundum with a gradation of P40, and sandpaper with grains made of electro-corundum with various grain sizes with three gradations P40, P220, P400 (according to European FEPA standards). To make the adhesive joints of steel sheets, the epoxy adhesive was used, which contains an epoxy resin based on bisphenol A and a triethyleneteramine curing agent. A profilographometer from Hommel - Etamic was used to determine selected 2D and 3D surface roughness parameters, and the strength tests of the steel sheets adhesive joints were performed on a ZWICK/ROELL Z150 testing machine. The analysis of the tests showed a significant impact of the surface treatment method on the attained shear strength of the steel sheets adhesive joints. Comparing the samples prepared with electrocorundum of the variable gradation, the tests exhibited that the samples prepared with P40 paper had the highest roughness, while samples prepared with P400 paper had the highest shear strength. Roughness analysis indicated that in the comparison group of samples prepared with abrasives of the various abrasive materials, ceramics showed the highest roughness parameters and the shear strength of the adhesive joints after this treatment. [ABSTRACT FROM AUTHOR]

This research presents a comparative analysis of the fracture surfaces of adhesively bonded dissimilar single lap joints (DSLJs) and investigates the effect of nanosilica (NS) additives on their fracture behavior and performance. The study focuses on DSLJs composed of aluminum (Al), stainless steel (SS), copper (Cu), and carbon fiber reinforced polymer (CFRP) adherends bonded with an epoxy adhesive. The fracture surface of DSLJs is further analyzed by introducing two parameters: fractional total fracture area (aT) and the surface sensitivity of each adherend (aSurface). These parameters serve as benchmarks to predict the final load capacity of the adhesive joints. It is found that a decrease in aT and an increase in the sensitivity of the adherend with a lower Young's modulus lead to higher load capacity. Tensile tests revealed that incorporating NS up to a critical weight percentage of 0.6 wt% improves the proposed surface parameters and significantly contributes to higher levels of load capacity and absorbing greater amounts of energy to failure. Furthermore, numerical simulations offer insights into stress distribution and the mechanism of plastic deformation propagation, providing additional support for the experimental findings. Highlights: NS up to 0.6 wt% enhances the mechanical properties of DSLJs.NS–epoxy interactions characterized through Fourier transform infrared and transmission electron microscopy analysis.Fracture surface patterns help to predict the final load capacity of DSLJs.Plastic propagation in epoxy verifies fracture surface pattern in DSLJs. [ABSTRACT FROM AUTHOR]

Determining adhesive failure in adhesively bonded joints is still challenging in the field. While the three-point bending test (3PBT) (ISO 14679:1997) has been helpful in identifying critical forces and displacements related to bond strength, it only allows for a qualitative assessment of the bond line. Recently, a new quantitative methodology has been developed to determine critical stress and fracture toughness using the coupled stress–energy criterion and the 3PBT. However, these assessments require a significant effort using semi-analytical or finite element (FE) analysis. Therefore, the present study proposes a reliable set of analytical equations to determine peel and shear stress distributions using a weak interface formulation and 1D Euler–Bernoulli approach. More precisely, a particular numerical method computes the integration constants from these equations. A new method has been proposed for calculating the interfacial stiffness in peel and shear mode, based on the material and geometrical parameters of the geometry. This method differs from the previous approach, where the interfacial stiffness was calibrated from the experimental behavior of the test. The whole approach has been validated through experimental and numerical analysis, including the costly 3D FE analysis. An analytical expression for interfacial energy release is suggested, developed following the works of Fraisse and Schmit on J-integral assessment of sandwich-type overlaps and depending on the applied force and a rotation, which could be experimentally measured. Therefore, this work is significant progress in determining bond strength using a simple mechanical test and equations applicable to various industries. [ABSTRACT FROM AUTHOR]

In this study, the shear strength and thermal properties of the adhesively bonded joints were investigated of adhesives reinforced with nanoparticles using carbon fiber-reinforced composite materials. The diglycidyl ether bisphenol A (DGEBA) was used as the epoxy resin. Single lap joint tests of 1% wt. Multi-walled carbon nanotubes (MWCNT) and 3, 5, and 7% wt. silicon dioxide (SiO2) nanoparticle-reinforced mixed adhesives were performed according to ASTM D5868 standards. The shear strengths of the mixed adhesives obtained by mixing at different ratios were compared with the epoxy resin. Upon conducting an analysis of the shear strengths of nanomaterials, results indicate that the incorporation of 1CNT + 3SiO2 in the nanomaterials showed the greatest improvement, with a 46% increase in shear strength. 1CNT + 5SiO2, 1CNT, and 1CNT + 7SiO2 showed increases of 32%, 14%, and 5%, respectively. The results of a tensile test indicate that pure epoxy exhibited a tensile strength of 5953 N, 1CNT, and 3SiO2, while the epoxy composite demonstrated a significantly higher tensile strength of 8738 N, along with an elongation of 0.72 mm. In addition, the morphology of fractured surfaces was examined by scanning electron microscopy (SEM). To investigate damage mechanisms, such as bridging, crack blunting, and branching of nanoparticles were observed. Characterization of epoxy resin and mixed MWCNT + SiO2 nanoparticles reinforced adhesives were also performed using Fourier infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and differential thermal analysis (DTA). Nanoparticles are settled between polymer chains, improving polymer chains' motion and thermal properties. [ABSTRACT FROM AUTHOR]

Adhesive joints GFRP/Steel bonded with epoxy adhesive were exposed to the external environment for one year, a tropical environment with temperature variations, humidity, radiation, and salt spray, due to its proximity to the sea. The shear strength of the joint was measured over the exposure time, as well as their chemical and physical changes. Tg of the adhesive was evaluated through DMA, and changes in the composite matrix were studied using FTIR. A significant reduction in joint strength was observed within the first 30 days, but this reduction quickly stabilized. High corrosion of the metal adherend was evident, which was also observed in the bonded region, significantly impacting the adhesive strength of the joints. Changes in the color of the composite were also identified due to exposure to solar radiation, which also affected the chemical bonds, as indicated by FTIR. The Tg of the adhesive decreased in the first 90 days and then gradually increased. These changes may have been related to the humidity, initially decreasing the Tg, and the exposure to higher ambient temperatures, which causes post cure effect. Therefore, the proposed external exposure conditions contain factors capable of causing significant changes in the joint and its components. [ABSTRACT FROM AUTHOR]

This paper focuses on the non-destructive evaluation of adhesive joints used in vehicles designed for transporting food products. The research and analysis were limited to the joints used in connecting elements of the cargo space. Two non-destructive methods were employed in the study: ultrasonic and thermographic techniques. Both methods confirmed the feasibility of evaluating adhesive joints in the construction of food transport vehicles, with the thermographic method proving to be much faster in identifying large areas of deadhesion in the plating. The ultrasonic method, on the other hand, allows for the inspection of sheathing and aluminum profiles. The predefined decibel drop in the height of the first two pulses on the ultrasonic defectoscope screen for areas with high-quality joints was less than 3.5 dB. In contrast, for areas with adhesion-related damage, the decibel drop in the first two pulses exceeded 4.5 dB. [ABSTRACT FROM AUTHOR]

AbstractExamining the mechanical performance of CFRP and aluminum samples subjected to environmental aging is crucial. Additionally, it is essential to develop methods to enhance their mechanical properties. This research investigates the impact of fullerene and single-walled carbon nanotubes (SWCNT) on the fatigue life and static strength of bonded and bonded/bolted joints. The study focuses on composite-to-composite (CTC) and composite-to-aluminum (CTA) substrates under three-point bending, both before and after hygrothermal aging. The samples were divided into four categories: (1) neat specimens, (2) specimens with added fullerene, (3) specimens with added SWCNT, and (4) specimens with a combination of 50% SWCNT and 50% fullerene. The experimental results indicated that the optimal nanoparticle ratio for bonded joints differs from that for bonded/bolted joints. Adding nanoparticles to the adhesive increased the fatigue life of SLJs, particularly in samples containing mixed particles and SWCNT. In some cases, nanoparticles amplified the effect of hygrothermal conditions, enhancing fatigue life further. The integration of nanoparticles into the adhesive and the use of bonded/bolted joints significantly improved joint strength, with the combination of both techniques yielding the best results. These modified joints offer a promising alternative to traditional joints in terms of strength and fatigue life. The study enhances understanding of the aging of adhesive and hybrid joints, especially dissimilar joints (composite to metal), and provides insights into their behavior under various environmental aging conditions. These methods show potential for optimizing joints and composite structures, improving durability, and reducing the likelihood of operational failures. [ABSTRACT FROM AUTHOR]

Wind turbine blades are complex structures composed of multiple bonded components. The fatigue performance of these adhesive joints is crucial for ensuring operational safety over the blade's lifespan. Traditional structural fatigue analysis methods are inadequate for evaluating the fatigue properties of these joints due to the unique characteristics of adhesive materials. Variations in material and dimensional parameters, as well as fluctuating operational loads, further complicate the fatigue analysis of adhesive joints in wind turbine blades. To tackle this issue, this study introduces a fatigue analysis and reliability assessment method for the adhesive joints of wind turbine blades, employing the Cyclic Cohesive Zone Model (CCZM) and accounting for parameter uncertainties. Specifically, a novel methodology for fatigue analysis based on the CCZM is presented. The methodology is programmatically implemented to obtain a fatigue life dataset through multiple simulations, considering uncertainties in material parameters, adhesive dimensions, and loads. Subsequently, a fatigue reliability model is formulated to evaluate the fatigue reliability of adhesive joints in wind turbine blades under different parameter conditions, and the sensitivity of fatigue reliability to each parameter is investigated. The findings offer valuable insights for improving the safety and reliability of adhesive structures in wind turbine blades. [ABSTRACT FROM AUTHOR]

The failure of bonded composite materials is accompanied by specific failure modes. These are specifically Mode I, Mode II, Mode III, and their combination (so-called mixed mode). These modes depend on the direction and type of loading. The mechanical properties describing the damage initiation and the damage evolution are unique according to the type of adhesive and present mode of failure. However, a few research studies have focused on an adhesive thicknesses greater than 0.2 mm. The main objective of this research is to investigate the mechanical properties of a bonded joint with large adhesive thickness loaded according to Modes I and II. The observed failure parameters, the cohesive and damage parameters, are identified by minimizing the difference between the force–displacement diagram obtained from the experimental data for both Mode I and Mode II. The finite element model is confronted with these parameters and is evaluated based on their agreement. Compared to other studies with a small adhesive layer thickness, the values of failure parameters are lower. The results show that the adhesive thickness has an influence on the values of cohesive and damage parameters and that these parameter values decrease significantly compared to a small adhesive thickness. The obtained parameters can be further used to predict the fracture toughness of other bonded joints loaded in any direction. [ABSTRACT FROM AUTHOR]

This study investigates the repair of damaged curved glass/epoxy composite laminates through various adhesive reinforcements and adhesively bonded external patches. The experimental procedures involve fabricating laminates, conducting four-point bending tests, quasi-static indentation tests, and optimizing damaged areas. Results demonstrate the influence of repairs on curved beam strength and interlaminar tensile strength. Adhesive repairs with chopped fiber reinforcement outperform plain epoxy and particle fiber-reinforced repairs, preserving 51.28% of curved beam strength. Adhesively bonded external patches, both single and double, with chopped fiber reinforcement exhibit significant strength recovery 72.08% and 80.78% compared to virgin samples. The study emphasizes the effectiveness of adhesively bonded external patches, particularly those with chopped glass fiber reinforcement, in enhancing curved beam strength and interlaminar tensile strength. This research provides valuable insights for repairing angled structures, such as those in airplane components, showcasing potential applications of these techniques for structural maintenance. HIGHLIGHTS: Investigated adhesive reinforcements and bonded external patches for curved composites. Laminates fabricated, tested for bending, indentation, and optimized in damaged region Chopped fiber adhesive repairs preserve significant 51.28% strength. Adhesively bonded patches exhibit 72.08% and 80.78% strength recovery. [ABSTRACT FROM AUTHOR]

Finite element (FE) simulations of adhesively bonded composite joints were conducted using the cohesive zone model (CZM). To clarify the effect of fracture criteria on the accuracy of the CZM simulation, two types of mixed-mode criteria including the -linear summation model of Modes I and II energy release rates, G I / G IC + G II / G IIC = 1 , and the nonlinear power-law, ( G I / G IC ) n + ( G II / G IIC ) n = 1 , were employed. A CZM formulation using the power-law fracture criterion was developed in this study. The load–displacement curves calculated by the two models were compared with the experimental results obtained from mixed-mode Fernlund–Spelt-type double cantilever beam tests, and the Mode II end-notched flexure (ENF) tests. Calculations using the nonlinear fracture criterion were closer to the experimental results. Consequently, it is concluded that nonlinear fracture modeling is of vital importance for accurate strength analysis of mixed-mode adhesive joints. [ABSTRACT FROM AUTHOR]

AbstractSpecifically, the conventional wood adhesive uses polyvinyl alcohol (PVA) as colloid to stabilise the polyvinyl acetate (PVAc) emulsion. Green materials are being used as a result of recent study on chemicals and alternative sources. This factor has made the substitution of sustainable biopolymers for petrochemicals considerably more important. An emulsifier, sodium lauryl sulphate (SLS), was used during the addition polymerization process to produce a hydroxyethyl cellulose-grafted-poly (vinyl acetate) (HEC-g-P(VAc)) emulsion from HEC and VAc. The purpose of the study was to increase the content of renewable materials in the emulsion. The adhesive films glass transition temperatures (Tg) have been identified via Differential Scanning Calorimetry (DSC). The performance of the PVAc emulsion-based adhesive in accordance with EN 204 and EN 205 standards was evaluated by measuring the tensile shear strength of wood joints under both dry and wet conditions. The viscosity of the adhesives significantly increased along with the addition of HEC. The application of HEC led to an increase in PVAc film hardness, which was confirmed by the film’s glass transition temperature. In an environment that was wet, after 24 h, the tensile strength of the sample containing HEC increased by 54% compared to a pristine sample, as per EN 204 and EN 205. Water resistance significantly increased in sample with HEC, as was found by measuring the water contact angle which is in line with wet strength. The overall study conclusion emphasises the superior water resistance and increased adhesion capabilities of PVAc emulsion-based wood adhesives stabilised by HEC. [ABSTRACT FROM AUTHOR]

To estimate the fatigue life of lightweight automotive structures in compliance with top-down design principles, there is a need for an accurate adhesive joint fatigue life prediction method that is compatible with industrial finite element modeling practices. This paper proposes a method to split the analytical J-integral solution based on the fracture mode of joints. The split mode I and II J-integrals correspond to the opening mode and sliding mode of the bonded joint, respectively. By splitting the J-integral and introducing the concept of the mixed mode ratio, an improved approach for estimating adhesive joint fatigue life is presented, considering the influence of loading modes. The proposed fatigue life prediction method is validated through fatigue tests on a sub-component level bonded structure. The results of the validation demonstrate that the split J-integral analytical solution method, considering the mixed mode ratio, provides better predictions compared to its predecessor approach. [ABSTRACT FROM AUTHOR]

Additive manufacturing (AM) has gained popularity due to reduced production times of low-cost and geometrically complex structures. Due to technological constraints such as print volume, time, and thermal stability of large AM parts, adhesive joints are commonly used in assembling smaller components in large-scale polymeric structures. This work investigates the feasibility of using embedded optical fibers to monitor strain distributions within AM composite (carbon fiber/nylon) single-lap shear (SLS) joints. Internal strain distributions within the adhesive and surface strain fields of the SLS joints with AM adherends under tensile loads were obtained using optical fibers and digital image correlation, respectively. Results indicate negligible influence of optical fibers on the failure strength and axial stiffness of 3D-printed SLS joints under quasi-static loading. Higher strains were observed at the bond edges within the adhesive (using optical fiber) and the surface (using DIC) of the joints due to the rotation of the bond under loading. All specimens failed in the adherends beyond the bonded region due to their low interlaminar strength. [ABSTRACT FROM AUTHOR]

Background: This paper investigates the mechanical properties and failure behaviours of rivet-bonded hybrid joints composed of aluminium adherends and steel rivets under quasi-static tensile loading. Objective: The damage law of hybrid joints is studied to provide a reference for the design and manufacture of hybrid joints. Methods: Tensile tests were conducted on aluminium and steel specimens at various triaxial stress levels. The corresponding finite element model (FEM) was developed to verify the Johnson–Cook damage parameters of the studied metals. The hybrid joint considering the rivet forming process was constructed through FE modelling using the Johnson–Cook failure criterion and Cohesive Zone Model (CZM), which was then validated with the experimental results. Results: Experimental results of the hybrid joint showed that a typical two-stage failure: 1) the adhesive layer bears the majority of the load during the initial loading stage, and 2) the adhesive layer completely fails after reaching the peak load and the rivet solely bears the load subsequently. Conclusions: The riveting process did not cause damage to the adhesive layer, which ensured the reliability of the manufacturing techniques of the hybrid joint. And the yielding of rivets may buffer the immediate failure of hybrid joints. [ABSTRACT FROM AUTHOR]

AbstractComposite materials have long been used in various industries due to their superior properties such as high strength, light weight and corrosive resistance. Bonded composite joints are finding increasing applications, as they provide extensive structural benefits and design flexibility. On the other hand, the failure mechanism of composite adhesive joints is not fully understood. A model that bridges manufacturing parameters and final quality measures is highly desired for the design and optimization of the manufacturing process of composite adhesive joints. In this study, a novel framework of Physics-Informed Neural Ordinary Differential Equation (ODE) with Heterogeneous Control Input (PINOHI) is proposed, which links the heterogeneous manufacturing parameters to the final bonding quality of composite joints. The proposed model structure is heavily motivated by engineering knowledge, incorporating a calibrated mathematical physics model into the Neural ODE framework, which can significantly reduce the number of data samples required from costly experiments while maintaining high prediction accuracy. The proposed PINOHI model is implemented in the quality prediction of composite adhesive joints bonding problem. A set of experiments and associated data analytics are conducted to demonstrate the superior property of the PINOHI model by using both the leave-one-batch-out cross-validation and sensitivity analysis. [ABSTRACT FROM AUTHOR]

This study investigates the impact of exposure to aggressive environments, specifically saline conditions per ASTM B117 standard, on the shear strength of adhesive‐bonded joints, crucial for ensuring structural integrity in various industrial applications like automotive, aerospace, and construction. Using an epoxy‐based adhesive to bond AISI304 steel, specimens undergo 14‐ and 28‐day salt spray treatments to simulate harsh working conditions. Torsional shear strength assessment of steel‐to‐steel adhesive joints is conducted using a torsion test methodology, with an analytical approach used to extrapolate adhesive joint shear strength. This research contributes to understanding adhesively bonded joint performance in challenging environmental conditions, and how the shear strength of the bonded joints changes in relatively small amount of time, offering valuable insights for robust structural designs across industrial sectors. [ABSTRACT FROM AUTHOR]

Highlights To enhance the mechanical properties of the adhesive layer in joints, a thin–structural open–cell porous Ni–foam was embedded into the adhesive interface through ultrasonics (US) assisted. The porous metal foam is effective in interlocking itself with adhesive. After the ultrasonic vibration was applied for 0.17 s, the adhesive penetrated Ni–foam, generating enough residue. This technique effectively improves the energy absorption and shear strength of the CFRP/Al single lap joint by more than 250.33% and 118.4% with a 0.5 mm thick Ni–foam insert, respectively. The fatigue resistance increased by 154% with a 0.3 mm thick Ni–foam insert based on the fatigue testing results and the Weibull distribution method. The S–N curves were established at different reliabilities for engineering applications. With the Ni–Foam insert, the failure modes were changed through crack deflexion, Ni–Foam degumming, and crack blocking. Ultrasonic vibration assisting Ni‐foam inserts CFRP/Al adhesive joints. The shear strength of joints with Ni‐foam was maximally increased by 118.4%. The fracture forms of joints with Ni‐foam were changed. The fatigue life of the joints with Ni‐foam was maximally increased by 154%. S–N curve of joint with Ni–foam of different reliability levels was got. [ABSTRACT FROM AUTHOR]

Highlights Adhesively bonded joints play a vital role in improving the structural performance of 3D‐printed components. This research aims to examine the effect of graphene inclusion on the failure load and vibrational behavior of polylactic acid flat‐joggle‐flat (FJF) joints prepared using fused deposition modeling. The present research focused on the effect of print directions (0°, 45°, 90°) and the inclusion of graphene nanofiller (0.25, 0.50, 0.75, and 1.00 wt%) on the performance of FJF joints. The effect of raster direction on mechanical properties was examined by tensile testing of dog‐bone samples. Results showed that 0° print orientation had higher tensile strength compared to other printing directions. Shear testing of FJF joints indicated that the inclusion of graphene has enhanced the strength of 3D‐printed FJF joints by 61.18%. Fractography results showed that the formation of the shear band with the inclusion of 0.50 wt% graphene helps to distribute the stress more evenly and prevent catastrophic failure of the FJF joint. The free vibrational test revealed that the inclusion of 0.50 wt% graphene had improved the natural frequencies, as the presence of graphene‐enhanced the interfacial bonding between FJF adherend and adhesive. 0° print orientation had higher tensile strength than other printing directions. Inclusion of graphene‐enhanced the shear strength of flat‐joggle‐flat (FJF) joints by 61.18%. Shear band formation delayed the failure of graphene‐reinforced FJF joints. FJF reinforced with 0.50 wt% graphene had adherend failure. FJF joint added with 1.0 wt% graphene had lower natural frequencies. [ABSTRACT FROM AUTHOR]

AbstractAdhesive bonding is a versatile joining method gaining popularity due to its ability to join variety of metals, nonmetals, and composite materials to achieve lightweight, high-strength structures. Unlike mechanical fasteners that require holes, adhesive bonding creates a continuous bond, resulting in a more uniform stress distribution. It also allows bonding thin materials and dissimilar materials, and creates airtight seals. However, even with these advantages, adhesive joints lack structural redundancy and sometimes strength compared to their mechanical counterparts. This has driven extensive research and development efforts to improve their strength, reliability, and overall performance. The present paper aims to explore both historical and recent advancements in techniques for enhancing the strength of adhesively bonded joints, organizing them in a coherent and systematic manner that can be easily quantified. The paper also presents a comprehensive comparison of the techniques, their dependency on various factors, and guidelines for the optimal choice. This examination could pave the way for novel optimization techniques and data-driven approaches for achieving superior joint performance. [ABSTRACT FROM AUTHOR]

In this research, the free vibration analysis of lap joint laminated conical shell connected to laminated conical shell with adhesive layer for various boundary conditions are investigated. Based on the first-order shear deformation theory (FSDT), the main field equations of the analytical model are derived and the governing differential equations of laminated conical shell to laminated conical shell adherends lap joint are obtained for homogeneous and elasticity adhesive layers by using Hamilton principle method. Then, based on the generalized differential quadrature method (GDQM), the equilibrium equations of the structure adherends are investigated. The influence of the boundary conditions, the type of the composite materials and adhesive layer, the circumferential wave number, the length to radius ratio of the shell, and the length of overlap to length of shell ratio are studied. Furthermore, the thickness to radius ratio and the thickness of adhesive to thickness of shell ratio, as well as the various cone angles of conical shell on the natural frequency of laminated conical adherends shells connected to the conical shells with adhesive layer are investigated. For validation of the numerical results, the results are compared with the previous research and the comparisons show very good agreement. The numerical results show that with the increase of the internal shell and external shell of semi-angle, the non-dimensional frequency of lap joint connection of two laminated conical shells with adhesive layer decreased and increased, respectively. Furthermore, with the increase of the adhesive thickness to conical shell thickness ratio and lap joint length to length of conical shell ratio, the dimensionless natural frequency of the structure increased. [ABSTRACT FROM AUTHOR]

A new crack-tip finite element able to improve the accuracy of Finite Element Method (FEM) solutions for cracks growing along the Winkler-type spring interfaces between linear elastic adherents is proposed. The spring model for interface fracture, sometimes called Linear-Elastic (perfectly) Brittle Interface Model (LEBIM), can be used, e.g., to analyse fracture of adhesive joints with a thin adhesive layer. Recently an analytical expression for the asymptotic elastic solution with logarithmic stress-singularity at the interface crack tip considering spring-like interface behaviour under fracture Mode III was deduced by some of the authors. Based on this asymptotic solution, a special 5-node triangular crack-tip finite element is developed. The generated special singular shape functions reproduce the radial behaviour of the first main term and shadow terms of the asymptotic solution. This special element implemented in a FEM code written in Matlab has successfully passed various patch tests with spring boundary conditions. The new element allows to model cracks in spring interfaces without the need of using excessively refined FEM meshes, which is one of the current disadvantages in the use of LEBIM when stiff spring interfaces are considered. Numerical tests carried out by h-refinement of uniform meshes show that the new singular element consistently provides significantly more accurate results than the standard finite elements, especially for stiff interfaces, which could be relevant for practical applications minimizing computational costs. The new element can also be used to solve other problems with logarithmic stress-singularities. [ABSTRACT FROM AUTHOR]

In response to heightened environmental awareness, various industries, including the civil and automotive sector, are contemplating a shift towards the utilization of more sustainable materials. For adhesive bonding, this necessitates the exploration of materials derived from renewable sources, commonly denoted as bio-adhesives. This study focuses on a bio-adhesive L-joint, which is a commonly employed configuration in the automotive sector for creating bonded structural components with significant bending stiffness. In this investigation, the behavior of joints composed of pine wood and bio-based adhesives was studied. Two distinct configurations were studied, differing solely in the fiber orientation of the wood. The research combined experimental testing and finite element modeling to analyze the strength of the joints and determine their failure mode when subjected to tensile loading conditions. The findings indicate that the configuration of the joint plays a crucial role in its overall performance, with one of the solutions demonstrating higher strength. Additionally, a good degree of agreement was observed between the experimental and numerical analyses for one of the configurations, while the consideration of the maximum principal stress failure predictor (MPSFP) proved to accurately predict the location for crack propagation in both configurations. [ABSTRACT FROM AUTHOR]

The fracture resistance of adhesive joints depends on the bondline thickness, especially in the toughest systems. While increasing the adhesive thickness to operate at peak fracture toughness is anticipated to be attractive, it leads to a mass increase and to a decrease of the effective shear stiffness and strength, calling for a trade-off. Here, we follow a rational materials selection approach for mechanical design to address different sets of objectives and constraints representative of different classes of applications. The approach is applied to select the best conventional adhesive based on a novel database. Mechanical analysis with two different degrees of complexity is considered. The elementary level only accounts for the influence of thickness on toughness, while more advanced models introduce the dependence of shear strength on thickness as well as the stiffness mismatch with the adherends. The best adhesive choice strongly depends on the objectives, constraints, and loading configuration. However, the ranking is not drastically affected by the adherends' stiffness. Gaps found for stiff/strong and tough adhesives motivate the development of architected joints. Inserting stop holes improves damage tolerance and density but reduces the shear strength and stiffness, requiring an optimum design. [ABSTRACT FROM AUTHOR]

In all areas of application, adhesive joints are exposed to environmental conditions, which can weaken the joint. To verify the functionality of the joints for a certain service life, accelerated ageing tests are used. To assess the mechanical performance of aged joints, single lap joints (SLJ) are often used. The influence of various geometries of SLJ on the strength and stress behaviour is known. The various ageing processes in bonded joints are not yet sufficiently known. Thus, the influence of the specimen geometry on the ageing behaviour cannot be reliably estimated and is therefore investigated in this work. SLJ with different geometries made of an AlMgSi alloy and a one-component epoxy-hybrid adhesive were artificially aged. T dimensions of the SLJ were varied in width, overlap length, adhesive thickness or joint design. Similar ageing results were seen in a significant shorter time with narrower samples or shorter overlap length. A SLJ with a bonding area of 6.3 mm x 6.3 mm was derived from these results. After 4–5 weeks of ageing, this shows comparable results to the standard test SLJ after 8 weeks. This allows to speed up industrial ageing tests nearly by factor two without changing ageing mechanisms. [ABSTRACT FROM AUTHOR]

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Epoxy adhesives become very brittle after curing due to their high‐crosslinking degree. For increasing the toughness of epoxy adhesives, the addition of different toughening agents has been proposed. In this study the diglycidyl ether of bisphenol A (DGEBA)/dicyandiamide epoxy network has been modified by adding an emulsion latex containing core–shell rubber particles (CSPs) prepared by means of seeded emulsion polymerization. The CSPs consist of poly (butyl acrylate) (PBA) as core and methyl methacrylate (MMA) copolymerized with glycidyl methacrylate (GMA) as shell. The effects of adding various amounts of the emulsion latex on the mechanical properties, thermal stability, adhesion, and microstructure of the cured epoxy resin were investigated. The CSPs were analyzed by transmission electron microscopy (TEM), Fourier‐transform infrared spectroscopy (FTIR), and differential scanning calorimetry (DSC). The mechanical properties, thermal stability, adhesion to aluminum plates, and microstructure of the cured epoxy resin were investigated by stress–strain, thermal gravimetric analysis (TGA), single lap shear test, and field emission scanning electron microscopy (FESEM), respectively. The addition of 7 wt.% emulsion latex to epoxy enhanced the tensile strength and the toughness of the dumbbell‐shaped samples by 421% and 4388% with respect to neat epoxy, respectively. Furthermore, the single lap shear strength increased in 33% and an increase of 71°C in the initial decomposition temperature of the epoxy was obtained by adding 7 wt.% CSP, without affecting the maximum decomposition temperature. The FESEM micrographs of the fractured surfaces indicated that the major toughening mechanisms were CSP de‐bonding, plastic void growth, and shear bond yielding. [ABSTRACT FROM AUTHOR]

The fatigue of adhesive joints in offshore wind turbine blades is a critical and widespread challenge, necessitating an urgent focus on adhesive bond reliability. Given the constraints of full-scale testing, this research explores the fatigue endurance of carbon fiber–epoxy adhesive composites, integral to blade construction. Recognizing the fatigue characteristics' sensitivity to environmental factors and joint dimensions, an innovative approach to fatigue modelling and evaluation is introduced. This method incorporates the influence of different environmental stresses and size effects. Specifically, a degradation coefficient and size impact factor (SIF) are introduced into the cyclic cohesive zone model, and a simulation-based analytic approach is proposed for analyzing adhesive fatigue. Furthermore, we introduce a reliability modelling procedure that integrates performance degradation theory to address the deteriorative characteristics inherent in adhesive fatigue. Subsequently, the specimens' damage accumulation increased by 75% because of the stresses and escalated to 85% with adhesive joint size effects, causing carbon fiber Reinforced Polymer/epoxy adhesive joints to fail interfacially rather than in a mixed-mode manner. This study provides valuable insights for the safety analysis and assessment of adhesive joint performance in offshore wind turbine blades. [ABSTRACT FROM AUTHOR]

Adhesive joints are widespread in the aerospace, aeronautics, and automotive industries. When compared to conventional mechanical joints, adhesive joints involve a smaller number of components, reduce the final weight of the structure, enable joining dissimilar materials, and resist the applied loadings with a more uniform stress state distribution compared to conventional joining methods. Hydroformed tubular adhesive joints are a suitable solution to join tubes with identical cross-sections, i.e., tubes with the same dimensions, although this solution is seldom addressed in the literature regarding implementation feasibility. This work aims to numerically analyze, by cohesive zone modelling (CZM), hydroformed tubular adhesive joints between aluminum adherends subjected to tensile loads, considering the variation of material parameters (type of adhesive) and geometrical parameters. Initially, a validation of the proposed CZM approach is carried out against experimental data. Next, the aim is to numerically evaluate the tensile characteristics of the joints, measured by the maximum load (Pm) and energy of rupture (ER), considering the main geometrical parameters (outer tube diameter of the non-hydroformed adherend or dENHA, overlap length or LO, tube thickness or tAd, and joggle angle or q). CZM validation was successfully performed. The numerical study determined that the optimal geometry uses the adhesive Araldite® AV138, higher dENHA and LO highly benefit the joint behavior, tAd has a moderate effect, and q has negligible influence on the results. [ABSTRACT FROM AUTHOR]

The Plasma Electrolytic Oxidation (PEO) process was investigated to enhance the adhesion of AA2024-O aluminum alloy with a polyetherimide (PEI) matrix composite, using oxy-fuel welding (OFW). A Central Composite Design (CCD) statistical model was used to optimize three independent parameters in PEO: immersion time (s), duty cycle (%), and electrolyte concentration (Na2B4O7·10H2O), aiming to achieve a maximum value of shear strength of the hybrid joint (in MPa). The hybrid joint without PEO treatment presented a resistance of 2.2 MPa while the best condition presented a resistance of 9.5 MPa, resulting in a value 4× higher than the untreated material, due to the characteristics of the coating, which presented a more hydrophilic surface, allowing better mechanical interlocking with the polymer matrix and resulting in mixed-mode failure (adhesive, cohesive, and light fiber). In addition to improving adhesion, the PEO treatment provided better corrosion resistance to the alloy, forming an inert aluminum oxide (Al2O3) coating, with an improvement of approximately 99.84% compared to the untreated alloy. The statistical design covers about 77.15% of the total variability of the PEO + welding process, with independent factors influencing around 48.4% of the variability. [ABSTRACT FROM AUTHOR]

The composite blade is integral to megawatt-class wind turbines and frequently incurs interlaminar damages such as adhesive failures, cracks, and fractures, which may originate from manufacturing flaws or sustained external fatigue loads. Notably, adhesive joint failure in the spar–web and trailing edge (TE) represents a predominant damage mode. This study systematically explores the failure mechanism in these regions, using mode I fracture toughness tests for an in-depth, quantitative analysis of the adhesive joint's fatigue crack growth characteristics. Additionally, we conducted extensive material and technical evaluations on specimen units, aiming to validate the reliability of techniques employed for wind blade damage modeling. A damage model, inspired by the NREL 5 MW wind generator's composite blade structure, meticulously considers the interactions between the TE and spar–web. Utilizing the virtual crack closure technique (VCCT), this model effectively simulates crack growth dynamics in wind blade adhesive joints, while the extended finite element method (XFEM) aids in analyzing crack propagation trajectories under repetitive fatigue loading. By applying this integrated methodology, we successfully determined the lifespan of the spar–web adhesive joint under constant load amplitudes, providing crucial insights into the resilience and longevity of critical wind turbine components. [ABSTRACT FROM AUTHOR]

This review paper provides an exploration of various facets of creep behaviour in adhesives and adhesive joints, encompassing experimental procedures, prediction models, influential parameters and strategies to enhance resistance. The discussion extends to the interplay between fatigue and creep, emphasising recent advances over the last two decades. While avoiding redundancy with prior work on temperature and moisture degradation, the paper articulates connections between topics for a better understanding. A critical examination of load levels reveals that small variations significantly impact the creep life of adhesive joints, particularly prominent with epoxy adhesives. The adhesive type, joint geometry and substrate material are scrutinised, revealing distinct impacts on creep behaviour. The study underscores the critical role of adhesive thickness and overlap length, emphasising their relevance in determining the time to failure in bonded joints under creep conditions. Notably, the substrate material's role is highlighted. As the review delves into unexplored dimensions, it calls for further research to bridge existing gaps and refine our understanding of tertiary creep and time until failure. [ABSTRACT FROM AUTHOR]

To examine the viability of combining pine needle fiber-reinforced polylactic acid composites, galvanized iron sheet and aluminum sheet via the use of mechanical fastening and adhesive bonding methods was investigated. The study included the preparation of three distinct kinds of joints, namely, adhesive, nut-bolt, and rivet joints, with the purpose of assessing their tensile and flexural strength. The findings indicated that the use of both mechanical fastening and adhesive bonding methods yielded successful outcomes in the bonding of these materials, with the strength of the joints changing based on the approach employed. The adhesive bonding approach exhibited superior tensile and flexural strength in comparison to the mechanical fastening technique. The microstructural examination demonstrated that the adhesive bonding approach yielded a consistent and uninterrupted contact between the materials, while the mechanical fastening technique exhibited some surface imperfections and deformations. The results indicated that both approaches were effective in producing robust and long-lasting joints. [ABSTRACT FROM AUTHOR]

In this paper, an attempt was made to determine the load-bearing capacity of a bonded joint of galvanized steel elements with CFRP fabric. This issue is extremely relevant to the use of bonded carbon fiber fabric as a mean of reinforcing hot-dip galvanized steel structures. This technique is used in engineering practice for both hot-rolled and cold-formed steel elements. In order to obtain the necessary parameters for modelling bonded joints of galvanised steel thin-walled elements, laboratory tests were carried out. In the first stage, four specimens made of 50 mm diameter steel cylinders bonded to 16 mm thick hot-dip galvanised steel sheet of S350 GD were subjected to the pull-off test. In this connection the SikaWrap 230C composite fabric embedded in SikaDur 330 adhesive layer was investigated. In the second stage, the axial tensile test of the bonded butt joint using the same materials was performed. In this stage, 10 hot-dip galvanised steel sheet samples of S350 GD and 16 mm thickness were tested. The discussion on the failure mechanism in the context of the bonding capacity of the composite joint was carried out. Moreover the advanced numerical model using the commercial FE program ABAQUS/Standard and the coupled Cohesive Zone Model was developed. The significant influence of the preparation method of steel element surface and the thickness of the adhesive layer on the failure mechanism of the joint and the value of the maximum failure force was shown.

Fiber-reinforced polymers (FRP) for structural elements' strengthening and rehabilitation are increasingly gaining popularity because of their proven efficiency and ease of application. The response of the adhesive joint formed between the FRP and concrete is a crucial factor influencing the overall behavior of FRP structures. The analysis of the interface crack propagation is a complex task involving the consideration of multiple interacting mechanisms. This work aims to provide a background to a recently proposed model that analyzes the behavior of the adhesive joint formed at the interface between the FRP and concrete, by creating its counterpart. The study presented herein discusses a model based on fracture mechanics to obtain a reference point needed to assess the output provided by an algorithm utilizing a damage-based model for concrete and an empirical-based procedure for the loss of bond action. Typically, model validation is performed via a comparison against experimental data. However, additional insights into the interacting phenomena can be provided by comparing the results of various applicable models. [ABSTRACT FROM AUTHOR]

The adhesive bonding approach is widely used in assembling of spars, stringers, ailerons, flaps, and rudders in aircraft. The present research investigated the impact of silicon carbide (SiC) nanoparticle inclusion on the shear and free vibrational behaviour of adhesively bonded single lap joints (SLJ). The shear test results showed that the inclusion of 1.5 wt.% SiC in the epoxy resin enhanced the shear behaviour of adhesively bonded SLJ. Furthermore, the failure surfaces of adhesively bonded SiC-reinforced SLJ were examined using a field emission scanning electron microscope (FESEM). The microstructural investigation of the failure surface demonstrated that the development of rougher surfaces, plastic void enlargement, and formation of shear bands in the joint region had improved adhesion among GFRP adherends. Thus, the SiC-incorporated adhesively bonded SLJ had predominant cohesive failures. Meanwhile, the SiC-free lap joint had an adhesive failure due to lower adhesion. The vibrational results avowed that 1.5 wt.% SiC-incorporated adhesively bonded SLJ has higher natural frequencies. Results also affirmed that higher wt.% SiC-incorporated joint had better modal damping values due to nanoparticle accumulation, which increased the interaction between glass fiber reinforced polymer (GFRP) adherends. [ABSTRACT FROM AUTHOR]

Combining steel with wood has been practised for many years. The issue is related to two main areas, i.e., bonding steel elements with wood so that they serve as connectors facilitating the assembly of wood elements and bonding steel elements to wood beams to improve their load-bearing capacity. In the first case, the adhesives used may be relatively expensive and more difficult to apply, whereas in the second one, especially when steel elements are glued inside the glulam (GL) beams, it is better if the adhesives used are more accessible to apply and cheaper. As it seems rational to reinforce wood with high-modulus ties, research has been carried out to compare the connection quality of commercially available adhesives that can be used for this purpose. Moreover, thermosetting adhesives have been applied as an alternative and cheaper solution. Thermostat adhesives also have a high pH of the bond, which prevents the steel from rusting. The research shows that the load-bearing capacity of the bond depends on whether the bars are ribbed or sheet metal. Moreover, among thermosetting adhesives, the most favourable load-bearing values were obtained using a mixture of PF/pMDI (phenol formaldehyde resin/polymeric diphenylmethane diisocyanate) and powder from recycled tyres. The shear strength of these joints was 1.63 N/mm2 and 3.14 N/mm2 for flat specimens and specimens with ribbed bars, respectively. [ABSTRACT FROM AUTHOR]

The widely used adhesive joining technique suffers from the drawback of being unable to be dismantled to examine for degradation. To counteract this weakness, several structural health monitoring (SHM) methods have been proposed to reveal the joint integrity status. Among these, doping the adhesive with carbon nanotubes to make the joint conductive and monitoring its electrical resistance change is a promising candidate as it is of relatively low cost and easy to implement. In this work, resistance change to monitor fatigue debonding of composite single-lap adhesive joints has been attempted. The debonded area, recorded with a liquid penetrant technique, related linearly to the fatigue life expended. However, it correlates with the resistance change in two different trends. Scanning electron microscopy on the fracture surface reveals that the two trends are associated with distinct failure micromechanisms. Implications of these observations on the practical use of the resistance change for SHM are discussed. [ABSTRACT FROM AUTHOR]

Adhesive joints are some of the oldest inseparable connections, and were used much earlier than other non-separable connections (e.g., welded, soldered). Adhesives are widely used in the manufacture of vehicles, household appliances, aircraft, and medicine. One disadvantage of adhesive joints is their long bonding time (amounting, for example, to 72 h for polyurethane adhesives used in bus roof bonding), and another is their production of harmful waste. Tapes that are adhesive coated on both sides are increasingly being used to join parts during production. Such tapes have lower strength than traditional adhesives, but their bonding time is much shorter. In addition, the amount of waste remaining after production is minimized. Tapes, like adhesives, dampen vibrations well and seal the materials being joined. The purpose of this study was to evaluate the influence of selected factors on the quality of tape–steel sheet joints and to assess the possibility of testing acrylic tape–steel sheet joints using ultrasonic methods. It was found that the preparation of a surface for bonding has a significant effect on the quality of the joint, and it was confirmed that non-destructive evaluation of the quality of the tested joints by the ultrasonic method is possible. The decibel drop in the height of the first and fifth pulses obtained on the screen of the ultrasonic defectoscope was proposed as an ultrasonic measure. The highest-quality joints were characterized by a measure in the range of 12 dB, lower-quality areas of about 8 dB, and tape-free areas of about 5 dB. At the same time, it was noted that in the case of proper surface preparation, there was cohesive failure of the joint during breakage. [ABSTRACT FROM AUTHOR]

AbstractAdditive manufacturing (AM) processes, also known as 3D printing, are experiencing growth and more industries are seeking solutions in these types of processes due to their advantages, including reducing the manufacturing time, sustainability, and the freedom to execute complex geometries. However, the dimensions of components are still quite small. Thus, it is necessary to find solutions for cases where assembly and joining of manufactured components are necessary. This work studies the tensile performance of adhesively bonded single-lap joints (SLJ) between AM adherends of polylactic acid (PLA), Polyethylene Terephthalate Glycol-modified (PETG), and Acrylonitrile Butadiene Styrene (ABS), bonded with the adhesives Araldite® 2015 and Sikaforce® 7752. The adherends’ mechanical elastic, plastic and fracture properties are determined prior to the assessment of the adhesive performance in SLJ. Failure modes, joint strength, assembly stiffness, and failure energy are obtained experimentally and compared to Cohesive Zone Model (CZM) predictions, aiming to provide the best material/adhesive combination that maximises the joint performance. In terms of strength and stiffness, PLA joints bonded with the Araldite® 2015 provided the best results, although the behaviour was different for the dissipated energy. The CZM approach showed to be a reliable design approach for bonded AM joints. [ABSTRACT FROM AUTHOR]

AbstractThis study introduces a novel approach to reinforcing notched aluminum plates using functionally graded composites (FGCs). By integrating volume fraction principles of Functionally Graded Materials (FGMs) into fiber-matrix mixture laws, we propose an advanced patch reinforcement strategy. The research employs the Cohesive Zone Model (CZM) and Extended Finite Element Method (XFEM) in ABAQUS to simulate patch debonding, crack initiation, and propagation. We compare linearly graded and FGM patches against non-graded counterparts, demonstrating superior load distribution and damage tolerance of graded composites. Three gradation concepts are explored: C-1 (peak fiber density at mid-thickness), C-2 (increased fiber density near patch edge), and C-3 (highest fiber density adjacent to the adhesive joint). Results reveal a critical interplay between adhesive debonding and crack propagation in the aluminum substrate. The study highlights the efficacy of graded composite patches in mitigating damage and offers significant insights into advanced reinforcement techniques for enhanced structural durability and reliability in engineering applications. [ABSTRACT FROM AUTHOR]

This paper outlines an experimental investigation into the durability of large-scale adhesively bonded joints with a thick layer of methyl methacrylate adhesive (MMA). Ageing has been performed by immersion in a 3.5 wt% NaCl solution for 10 weeks at 50°C. Two aged and one unaged specimen were subjected to tensile testing, and three aged and one unaged specimen were loaded up to ~ 3.5 million fatigue cycles followed by a residual tensile test. The ductility of the adhesive is affected by ageing and fatigue testing. Despite a decrease in ductility, the plastic zone development was adequate for the required strain redistribution without compromising the joint performance (strength and stiffness) demonstrating the fatigue tolerance of the joint. The shear, longitudinal, and peel strain values in the adhesive bulk are evaluated by digital image correlation. The shear strength values are significantly higher than the requirements following from the design. All specimens failed by sudden delamination of the composite plate. Post-mortem analysis showed no corrosion travel at the interface of steel and adhesive. [ABSTRACT FROM AUTHOR]

Adhesive bonding has become increasingly popular in the aeronautic and automobile sectors due to its ability to reduce weight, create strong bonds, and join dissimilar materials. The primary aim of the study is to conduct experimental analysis on Single-Lap Joints (SLJs), specifically focusing on varying ambient temperatures from (25°C to 65°C) while keeping the loading rate constant at 1.3 mm/min. This study used SAE 1020 steel, AA2024-T3, and BK-9 adhesive to manufacture SLJs. The adhesive-bonded SLJs were developed using dissimilar and similar adherends. The thermal behavior of the BK-9 adhesive was examined by conducting Digital Scanning Calorimetry (DSC) and Thermal Gravimetry Analysis (TGA) before and after subjecting it to elevated temperatures. The bonding quality has been examined using ultrasonic testing. The failure strength of the adhesive bond on SLJs was performed at the Universal Testing Machine (UTM) using tensile testing equipment, and a Field Emission Scanning Electron Microscope (FESEM) was utilized to determine the failure patterns. The result indicate that the SAE 1020-SAE 1020 steel joints exhibited superior mechanical behaviour, showing the highest failure load of 5.120 kN at 25°C room temperature, respectively. [ABSTRACT FROM AUTHOR]