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Partial discharges (PDs) are believed to be one of the key factors accelerating high voltage (HV) equipment ageing. The chemical by-products of PDs actively contribute to the modification of insulations surface quality, especially in air medium due to the diversity of its constituents. Although nonthermal plasmas in air have been widely studied, their adaptation to HV systems is still highly complex and prone to controversies. In this work, a typical simulation of a fault leading to PD in air, through a Dielectric Barrier Discharge (DBD) point-to-plane configuration, is performed in order to measure ozone (O 3 ), nitrogen oxide (NO) and dioxide (NO 2 ) by-products gases. The evolution of these species regarding PD duration, PD power and humidity is analyzed. Ozone production rate and dynamics are found to predominate over NO 2 and NO ones. The effect of humidity on gases evolution is found to be indirect, as it mainly affects PD power.

This paper presents partial discharges and streamers characterizations on 3 dielectric liquids under variation of wide temperature range, i.e.: aromatic hydrocarbon dibenzyltoluene, synthetic ester and halogenic perfluoropolyether liquids. Results indicate distinct behaviors among these liquids under highly divergent AC sinusoidal and impulse electric field. Dibenzyltoluene demonstrates excellent feature in suppressing discharges even at elevated temperature. In synthetic ester, positive discharges appeared to be less numerous but extremely high up to several nC in amplitude are strongly related to the further breakdown. Streamers inception voltage which denotes the initial discharges properties and streamer propagation velocity varies from several m/s up to order of km/s, show less dependency to temperature instead of the intrinsic characteristic of liquid itself. These prebreakdowns phenomena constitute interesting information in planning and selecting insulation liquids and analyzing fundamental mechanism during the operation and maintenance for HV utility applications.

The conduction current recorded when a high voltage impulse is applied to a rod-plane gap containing water is modelled. The electro/thermal model considers the coupling between electric field, Joule dissipation, temperature rise, and variation of liquid resistivity with temperature. A fairly good agreement between current measurements and calculations are obtained. The model also shows the evolution of temperature and field distributions in the gap versus time. The calculated average temperatures appear insufficient to explain liquid boiling. Boiling can be explained by considering the influence of local surface defects. Values of the bubble pressure at discharge ignition are evaluated, with the hypothesis that discharges occur in vapor following Paschen's law.

The generation of vapor bubbles in water under high voltage impulses of long duration (500 μs) is investigated experimentally. In most cases, the appearance of bubbles is followed by the inception of discharges occurring within the vapor, eventually transforming the bubble into a propagating streamer. Time delays to bubble and discharge inception are measured versus conductivity and voltage, using fast visualization and optical detection of bubbles. Before bubble inception, the liquid heating and the onset of an electro-hydro-dynamic (EHD) motion can be observed by Schlieren visualization. Electrical measurements show a decrease of the gap resistance versus time, attributable to the heating of water. When conductivity and voltage are changed, the onset of bubble inception is correlated to a nearly constant resistance drop, suggesting that a constant temperature is present when bubbles appear. At short times, the energy dissipation required to observing bubbles is independent of conductivity and applied voltage. Experiments show that vapor bubble generation results from a competition between liquid heating by Joule dissipation, and forced cooling induced by the EHD motion.

The characterization of pre-breakdown streamers in liquids is carried out under high temperature up to 200°C. Measurements are obtained either in a high temperature non-polar liquid (dibenzyltoluene, DBT), or in a synthetic ester (Midel®7131) for comparison. Streamer inception voltages are measured in both polarities, as well as propagation velocities. The results obtained show that only minor modifications are recorded when temperature is raised up to 200°C. Due to its stability at high temperature, DBT constitutes an interesting solution in the perspective of using liquids for the insulation of high temperature power electronics.

Partial discharges characterization on ceramic substrates and dielectric liquids under high temperature up to $350^{\circ}\mathrm{C}$ is investigated. Aluminum nitride (AlN) and alumina (Al 2 O 3 substrates, and a high temperature non-polar dibenzyltoluene (DBT) liquid are used. Several complementary measurements are also done in a synthetic ester liquid. PD measurements on AlN substrates embedded in DBT show a good behavior up to $300^{\circ}\mathrm{C}$, and up to $350^{\circ}\mathrm{C}$ with Alumina. This shows that high temperature insulating liquid may constitute a good alternative to silicone gels for the encapsulation of power electronics circuits at high temperature and high voltage. The comparison between PD characteristics in the liquid alone and with substrates show that PDs mostly occur within the ceramic material at temperatures up to $300^{\circ}\mathrm{C}$.

An experimental study of breakdown and pre-breakdown phenomena in liquid nitrogen (LN 2 ) is performed in this work, aiming to provide useful knowledge for the design of high voltage superconducting systems. A metallic tape subjected to pulsed heating is used as ground electrode to properly simulate the operating conditions of a quenching superconducting apparatus. Measurements of breakdown voltages between the tape and a plane electrode tied to high voltage show the strong influence of tape polarity, LN 2 temperature, and delay between heating and voltage application. Various measurements obtained with either a highspeed camera or an intensified camera allow to characterize the sequence of pre-breakdown events (i.e. liquid boiling, vapor bubble development, and streamer propagation) leading to breakdown.

Electrical breakdown properties of Dibenzyltoluene (DBT) are investigated over wide temperature range (from room temperature up to 350°C), and under pressure variation « 1 kPa to 200 kPa). The purpose is to investigate the suitability of DBT as potential insulating material for high temperature applications, such as encapsulant in high temperature power electronics modules. Measurements were carried out using a special high temperature test cell, under nitrogen atmosphere. Sphere-sphere electrodes and voltage ramp were used. Results show some reduction of breakdown voltage at high temperature, down to 58.2% at 350°C. A similar effect is observed when pressure is reduced. This reduction occurs when the liquid approaches boiling conditions, hence facilitating the appearance of vapor bubbles.

This paper deals with physical processes involved during inception of positive streamers in liquid cyclohexane. The inception of streamers is detected with a high temporal resolution by measurements of charge, visualization, and detection of phase change by scattered laser light. These techniques allow us to obtain measurements of inception voltages and inception delay time in various conditions of impulse voltage with different slew rates, and pressure. In positive polarity, a minimum "formative time" close to 40 ns is observed, as well as a large influence of both pressure and slew rate. The hypothesis of cavitation induced by the EHD motion, and liquid boiling due to heat dissipation are considered to explain positive streamer inception.

An experimental study of discharges in air at atmospheric pressure under impulse voltage, creeping on insulating solid surface is presented. The objective is to get a better understanding of creeping discharge by studying streamer initiation and propagation, and by looking at the influence of the nature of the insulating solid. Several solid materials, of different chemical natures and permittivity are investigated. Pre-breakdown streamers are investigated by high speed visualization and transient current measurements. In the presence of insulating solids such as epoxy resin, PPA/glass fibers and polycarbonate, surface streamers appear during the voltage rise, and the time delay to appearance is correspondingly rather short. With two materials of polyolefin and fluorine modified polyolefin families, characterized by lower permittivity, the first creeping streamer appears at the maximum voltage after a much longer statistical time delay, very close to that obtained in air without solid.

Breakdown, at least in point-plane geometry, is the result of inception and propagation of pre-breakdown phenomena called "streamers". The purpose of the present investigation is a spectroscopic measurement of the essential plasma parameters, i.e. the gas temperature and the neutral particle and electron densities. In this paper we focus our spectroscopic investigation on fast positive filamentary streamers obtained at large gap distance under high impulse voltage in LN 2 .

Dielectric properties of synthetic ester oil are investigated in wide frequency range (10 mHz–1 MHz) and temperature (−60°C −200°C) ranges. The aim is to determine the ability of liquid insulation, to be used as encapsulating materials for high temperature power electronics modules. As far as the ester remains in liquid state (above approximately −16°C), a typical frequency spectrum of the dissipation factor tan δ with two parts is observed. At low frequency, dielectric losses (tan δ > 0.10) are due to ionic conduction, and at high frequency losses are mainly due to dipolar relaxation. When temperature is increased, losses increase at low frequency, and decrease at high frequency. Results show that the liquid conductivity increases by more than 3 orders of magnitude between room temperature and 200°C. A slight decrease of permittivity is also observed, correlated to the lowering of density at high temperature. This behavior totally changes when the ester becomes a gel at low temperature. Dielectric relaxations reminiscent of solid materials then appear.

Gas Insulated Substation (GIS) under High Voltage Direct Current (HVDC) are becoming widely investigated with the development of DC networks. Under DC voltage, mechanism of charge accumulation on the insulation surface is of major importance since it may distort the electric field distribution. The latter directly depends on material's conduction and so, on its volume and surface conductivities. Previous work has evidenced that those properties are influenced by the temperature, the electric field and the surrounding relative humidity [1-3]. The insulation characteristics must be clarified to allow a better estimation of the electric field distribution, as well as a better insulation design.

International audience; Surface resistivity of solid insulators is usuallydetermined by measuring the current induced when an electricfield tangential to the surface is applied. This classical methodcan become questionable when the electric field is raised. In fact,a current may also flow above the interface through the humidgas, in addition to currents flowing at the interface and below theinterface within the solid bulk. This paper presents anexperimental study of the variation of the surface resistivityversus electric field and relative humidity RH of the surroundinggas. The results show that in dry gas (RH < 1%) and for anelectric field up 8 kV/mm, the surface gets no specific propertiescompared to the volume. However, in humid gas (1% < RH

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This work reports on the relationship between structure and dielectric properties of biaxially oriented polypropylene. The morphology of semicrystalline bioriented isotactic polypropylene films is investigated using wide angle X-ray diffraction and Polarized Optical Microscopy. A b-orthorhombic structure, with a crystallinity ratio of about 46%, and “Crater” morphology of the b-form is identified. Dielectric properties are measured by Broadband Dielectric Spectroscopy over a wide temperature range (2150 to 1258C). Since the dissipation factor of the PP is very low, special care was taken to obtain valid data. Two main relaxation processes are observed: a a-relaxation peak associated to the glass transition temperature (Tg) at temperature about 278C, and a broad b*-relaxation at about 2608C, partly attributed to CH orientation. The variation of the dissipation factor versus sample thickness (from 3.8 to 11.8 mm) is correlated and partly explained by the increase of crystallinity ratio and lamella size at larger thicknesses. It comes out that the thinnest film seems perfectly meet the application requesting, namely lowest dissipation factor and highest permittivity.

The dielectric properties of two grades of bi-oriented isotactic polypropylene were studied with a variety of techniques: breakdown field measurements, dielectric spectroscopy, thermally stimulated depolarization currents (Is), and direct-current (dc) conduction I values. Standard polypropylene (STPP) and high-crystallinity polypropylene (HCPP) films were investigated. Measurements were carried out over a wide temperature range (2150C/1125C). The breakdown fields in both materials showed a very small difference. On the other hand, the dielectric losses and dc conduction I values were significantly lower in HCPP. Both materials showed a decrease in the dielectric loss versus temperature in the range 20–90C; this is favorable for application in alternating-current power capacitors. The analysis of the dc I value allowed us to find evidence of two main conduction mechanisms: (1) below 80C in both materials, a hopping mechanism due to the motion of electrons occurred in the amorphous phase, and (2) above 80C, ionic conduction occurred in HCPP, and hopping conduction occurred in STPP.

This paper presents a study of prebreakdown phenomena (usually called streamers) occurring at high voltage in liquid nitrogen. A special cryostat has been constructed to allow dielectric measurements in liquid nitrogen up to 200 kV, and 0.5 MPa hydrostatic pressure. Streamers are detected and studied with various techniques: high speed visualization, streak camera, and recording of transient currents and emitted light. The propagation of positive and negative streamers is investigated at gap distances up to 80 mm. Streamers are then compared to similar phenomena observed in mineral oil. In liquid nitrogen, streamers are different compared to mineral oil. A transition from slow to fast positive streamers (velocity about 10 km/s) is observed at a threshold voltage below the breakdown voltage. The hydrostatic pressure has almost no influence on this phenomenon. Some experiments carried out with a solid barrier perpendicular to the gap axis are also presented. The practical consequences for the design of HV insulation in superconducting systems are then discussed.

Presents a study of streamer inception in mineral transformer oil, in point-plane and rod-plane geometry under impulse voltage. The measurements performed with points and rods over a wide range of tip radii show a marked decrease of initiation fields when the electrode radius is increased. The initiation field is divided by 30 over the investigated range (from 1 /spl mu/m points up to 2 cm rods). This effect compares fairly well with the "surface effect" known for breakdown voltages under uniform field with large electrodes. Plotting these results together shows the decrease of streamer initiation fields over a very wide electrode surface range (12 decades), proportional to S/sup -0.17/ (S: electrode surface area, cm/sup 2/). These results suggest the influence of electrode surface defects on streamer initiation under impulse voltage.

This paper presents a study of prebreakdown and breakdown phenomena under ac voltage in mineral oil in very large gaps (/spl les/80 cm). The investigations presented concern the measurement of breakdown voltages together with the recording of streamers in rod-plane and sphere-plane electrode systems, at different gap sizes. A breakdown mode specific to ac voltage is found, in which 'bursts' composed of streamers initiated at each half cycle appear. This mode leads to the lowest breakdown fields recorded under ac. Values of the average stress required for burst or direct breakdown modes are deduced from the experiments. Positive streamers are responsible for breakdown in large gaps: their propagation is easy and does not depend on the gap geometry and on the presence of particles. On the other hand, the propagation of negative streamers is quenched when not very divergent fields are used.

For over a decade, our group has been working on the development of distributed electron cyclotron resonance (DECR) plasma sources. The uniform distributed plasma (UDP) is the latest outgrowth of DECR, which has proved to be a flexible concept, leading to task-adapted plasma sources. Our plasma-based ion implantation (PBII) reactor is a 60 cm diameter, 70 cm high cylinder. The inside of the cylinder wall is covered with an array of 24 tubular magnets, 2.45 GHz microwave power feeds, and wave propagators. This peripheral plasma source of a good square meter produces a uniform distributed plasma (UDP), suitable for the treatment of wafers, pipes or objects of arbitrary form. Initial PBII plans concern the nitridation of silicon wafers. At 1 mTorr pressure and 1.3 kW input power, the N 2 plasma has a density of 2 × 10 10 ions cm −3 and an electron temperature of 1.2 eV. The N + /N 2 + ratio of 7/3 in the N 2 UDP plasma, determined by quadrupole mass spectrometry, is favorable for PBII applications. A 45 kV pulsed power supply is available for initial tests, but should be supplanted by a more powerful source for meaningful experiments.

This paper presents an experimental study of Partial Discharges and light emission with ceramic substrates embedded in silicone oil, under ac and square high voltage. Two types of ceramic materials used in power electronics modules are considered: Aluminum Nitrite (AlN) and Alumina (Al2O3). With AlN, a large light emission due to the electroluminescence of the ceramics occurs during the negative dV/dt. This phenomenon is not observed with Al2O3. With Al2O3 and silicon oil, the light emitted is only due to PDs, and recording under square voltage wave shows that PDs are more numerous and/or more intense compared to ac. Square voltage is more relevant to actual working conditions within power electronics modules than ac.

Surface resistance measurements on insulating solids are usually performed by measuring the current induced when an electric field tangential to the surface is applied. The measured current results from the addition of currents flowing along the surface, and also partly in the volume. In this paper, surface current measurements on an alumina-filled epoxy resin are performed under varying conditions of temperature (40-60°C), relative humidity (0-80 %), gas nature (SF6, N2, air), pressure (0.1-0.8 MPa). In dry conditions, measured currents do not depend on the gas nature and pressure. In air, when the relative humidity (RH) is varied, a large influence is measured, and the recorded variation of surface currents includes two phases: a rapid one attributed to the immediate change of surface resistance, followed by a much slower variation attributed to the progressive impregnation of the material by water. Numerical simulation shows the dominant influence of surface properties on measured currents, and evidences the existence of a surface layer with a higher conductivity compared to the material volume, even in dry conditions.

This work reports on the relationship between structure and dielectric properties of biaxially oriented polypropylene. The morphology of semi-crystalline bioriented isotactic polypropylene (BOiPP) films is investigated using Wide Angle X-ray Diffraction (WAXD) and Polarized Optical Microscopy (POM). A β-orthorhombic structure, with a crystallinity ratio of about 46%, and a “Crater” morphology of the β-form is identified. Dielectric properties are measured by Broadband Dielectric Spectroscopy (BDS) over a wide temperature range (-150°C to 125°C). Since the dissipation factor of the PP is very low, special care was taken to obtain valid data. Two main relaxation processes are observed: a α-relaxation peak associated to the glass transition temperature (Tg) at low frequency and temperature about -7°C, and a broad β*-relaxation at high frequency at about -60°C, attributed to CH orientation. The variation of the dissipation factor versus sample thickness (from 3.8 μm to 11.8 μm) is correlated and explained by the increase of crystallinity ratio at larger thicknesses.

The dielectric properties of two grades of Bi-oriented isotactic polypropylene (BOiPP) are studied, using a variety of techniques: breakdown field measurements, dielectric spectroscopy, thermally stimulated depolarization currents, dc conduction currents. Standard (STPP) and high-crystallinity (HCPP) polypropylene films are investigated. Measurements are carried out over a wide temperature range, up to (-150°C/ +125°C). Breakdown field in both materials show a very small difference. On the other hand, dielectric losses and dc conduction currents are significantly lower in HCPP. Both materials show a decrease of dielectric losses versus temperature in the range (20-90°C), favorable for the application to ac power capacitors. The analysis of dc currents allows to evidence two main conduction mechanisms: (i) below 80°C in both materials, a hopping mechanism due to motion of electrons occurring in the amorphous phase; (ii) above 80°C, an ionic conduction in HCPP and a hopping conduction in STPP.

In Insulated gate Bipolar Transistor (IGBT) modules, ceramic substrates are used as insulation between semiconductor chips and the ground potential. The substrate, semiconductor chips and connections are covered with silicone gel to prevent partial discharges (PDs) from occurring. In this work, partial discharges are investigated on laboratory samples made of metalized substrates embedded in silicone gel and various liquids. Substrates are made of aluminum nitride (AlN), alumina (Al2O3), or glass/epoxy composite. The objective is to determine the actual origin of PDs, by changing the nature of encapsulating material and substrate. The various liquids used are first characterized using a point-plane geometry. Experiments show that a rather large discrepancy on the PD behavior can be due to the ceramic substrate itself. "Good" and "bad" substrates can be identified on the basis of PD measurements. The influence of the sample preparation (degassing procedure) is also evidenced. The main conclusion obtained in this paper shows that partial discharges do not occur within the encapsulating material, contrary to most previous hypotheses, but within pores existing in sintered ceramic materials. Changing the substrate nature has a large influence on PD behavior, whereas a modification of the encapsulating material has almost no effect.

Metalized polypropylene films are used to build power capacitors for ac voltage. The objective of this paper is to study the de-metallization processes that may occur under high electric field. A laboratory model of capacitor is first described. It allows us to visualize the de-metallization and record the corresponding capacitance loss, under various conditions of applied voltage, frequency, mechanical pressure, and gas nature. Four different de-metallization processes can be observed. The residual gas layer existing between films has a primary importance. Replacing air by nitrogen shows that the de-metallization is basically due to the oxidation of the metal.

The reliability of electrical contacts is now the major challenge to improve the lifetime of Micro Electro Mechanical Switches. This paper investigates contact failure due to material transfer in real MEMS devices. The mechanisms of degradation observed on components have been reproduced with a good correlation on an AFM-based setup. Therefore, the importance of the closure phase and the voltage applied across the contact on the material transfer phenomenon has been highlighted with a fine quantitative analysis of the transferred volume.

This paper describes an experimental study of streamer inception in mineral oil under ac voltage, with rod and point electrodes. Positive and negative streamer inception frequencies versus voltage are investigated in gaps up to 40 cm with different electrode shapes and different conditioning of the oil (filtered oil, addition of cellulose particles, water). Streamer inception probability increases exponentially versus field, and it is not possible to simply define an “inception voltage”. A voltage (or field) value correlated to an inception probability must be used to properly compare different experiments (comparison between liquids, influence of pollution, etc.). Under ac, several effects are superposed to reduce dielectric strength: “scale effects”, influence of pollution, long time duration. With sharp points, injected space charges considerably influence experiments, and the results obtained cannot be extrapolated to practical applications in which the effect of space charge is mostly absent.

Aluminium nitrite (AlN) or alumina (Al 2 O 3 ) substrates are widely used in power electronics modules, due to their ability to provide both electrical insulation, and heat conduction properties. A silicon gel usually covers the substrate, semiconductor chips, and bondings to prevent partial discharges (PD) from occurring within the module. However, at high voltage PDs can be observed in high electric field regions, mainly at the sharp edges of copper tracks on the substrate. In this study, we try to determine the origin of these PDs. Phase resolved PD recordings (PRPD) and optical visualization at very high sensitivity are carried out on substrates embedded in gel or insulating liquids. PD features are very different from those obtained in needle-plane geometry in gel or liquid, and do not depend on the nature of the liquid or gel. The main conclusion is that PDs recorded with substrates originate from the ceramic material itself, due to the presence of numerous μm-sized pores in sintered materials.

International audience; An integrated solution for the galvanic isolation between power transistors and their control unit is presented in this paper. This solution is based on a monolithic integration of a photodetector within a power MOSFET without any modification of its fabrication process. This photoreceiver can be associated with a monolithic driver to drive high side switches. Exhaustive characteristics for several integrated photodetectors are presented and discussed: quantum efficiency, step response, small signal analysis and sensitivity to the High Voltage MOSFET's Drain. The results of this analysis are photoreceivers with a Full Width at Half Maximum above 300MHz and a responsivity above 0.15A/W at a wavelength of 500nm. This leads to an integrated low power and high bandwidth optical isolation.

Ester-based insulating liquids are considered today for electrical insulation in medium and high voltage transformers. The main advantages expected are their non-toxicity, excellent biodegradability, and fire resistance. Esters can be either of natural origin or synthetic. In this work, we present a study of prebreakdown and breakdown properties at high voltage and large gaps in several natural and synthetic esters, and a comparison with the well-know mineral transformer oil. This study is focused on the study of streamer propagation in large gaps up to 10cm. Compared to mineral oil, the transition to fast streamers in esters occurs at much lower voltage. Measurements also show no difference between esters, whatever their origin, viscosity, etc. From these results, it appears that the properties of esters are less favorable for very high voltage insulation than in mineral oil: once triggered, streamers are able to propagate very quickly to breakdown at lower voltage. In consequence, esters show a lower resistance to fast transients such as the standard lightning impulse.

Aluminium nitrite (AlN) or alumina (Al 2 O 3 ) substrates are widely used in power electronics modules, due to their ability to provide both electrical insulation, and heat conduction properties. A gel layer usually covers the substrate, semiconductor chips, and bondings to prevent partial discharges (PD) from occurring within the module. However, at high voltage PDs can be observed in high electric field regions, mainly at the sharp edges of copper tracks on the substrate. In this study, we try to determine the origin of these PDs. Phase resolved PD recordings (PRPD) and optical visualisation at very high sensitivity are carried out on substrates embedded in gel or insulating liquids. PD features are very different from those obtained in needle-plane geometry in gel or liquid. The main conclusion is that PDs of low amplitudes probably originate from the ceramic itself, due to the presence of numerous µm-sized pores in sintered materials.

In gas insulated switchgears (GIS), high voltage electrodes are supported by solid insulators. A "triple junction" (TJ) exists at the interface between metal, insulating solid, and gas. This area constitutes a preferential zone were partial discharges (PDs) can appear. A further degradation of insulation performance can occur if solid particles accumulate at that place. This paper presents experiments carried out to obtain a quantitative account of the influence of a metallic particle located close to a triple junction area, both in dry air and SF6. PDs are detected and measured by conventional electrical measurements, and observed optically with a high-sensitivity intensified camera. Measurements under AC voltage show the influence of the particle on PD inception and flash-over voltage, in comparison with the same geometry without particle. In SF6, the particle induces a large decrease of PD inception and breakdown voltages, which become nearly independent of the gas pressure.

This paper reports an experimental investigation about streamer propagation and breakdown in natural esters (rape-seed oils). Experiments are carried out over a large range of gap distances (from 2 to 20 cm) and voltage (up to 460 kV), in order to determine the properties of natural esters for high voltage insulation. A detailed description of positive and negative streamers is obtained by the measurement of propagation velocity, stopping length, transient currents, charge, streak photographs of the emitted light. As in previous studies carried out in mineral transformer oil, several propagation "modes" can be observed in rape-seed oil. They show the transition from "slow" streamers (velocity about 1 km/s), to fast streamers (velocity up to 200 km/s). Fast positive streamers propagate at much lower voltage in rape-seed oil compared to mineral oil. In turn, this induces lower breakdown voltages and shorter time to breakdown in this liquid. Measurements of currents and streak photographs bring the evidence of the stepped character of fast positive streamers and show the constancy of their velocity under very high voltage.

Water absorption in an epoxy composite used for insulation of stator bars in large generators is investigated in order to study both diffusion kinetics and effects on dielectric properties. Water absorption can be described by the superposition of two Fickian mechanisms, the first occurring within epoxy and the other at interfaces between epoxy and fillers. A large decrease of breakdown strength versus water uptake is observed. It points to the large deleterious effect of water on insulation reliability. Dielectric spectroscopy is performed under various conditions of water impregnation, electric field and temperature. A very large increase of permittivity and losses is recorded in the presence of water, especially at low frequency. At power frequency, dielectric properties do not show a non-linearity when the field is increased up to service values. At very low frequency, a decrease of losses when the field is increased is observed. It is due to the Garton effect. Most of results show that the wet material behaves as a low frequency dispersion system (LFD).

In this paper, the water concentration profile within the insulation of a stator bar in the presence of a water leak is calculated by resolving the Fick's equation. The temperature strongly activates diffusion processes, but the shapes of concentration profiles remain similar. From the measured dielectric properties versus water content, an electrical model is developed in order to calculate the field and potential distribution within the insulation. The field is reduced in wet zones due to the high local permittivity and conductivity compared to dry zones. This effect is favorable since the breakdown field is lowered in wet zones. On the other hand, the field in dry zones is reinforced, but the value attained remains lower than the short-term breakdown strength. This explains why stator bars in the presence of waters leaks may survive for long times, in spite of high local water concentrations in excess of 1%. The high sensitivity of dielectric properties at low frequency to the presence of water suggests non-destructive methods to detect wet bars in a real power generator.

This paper presents an experimental study of streamer inception in a silicone gel. Many parameters are able to influence the inception of discharges in a gel: voltage wave shape, electrode geometry, temperature, etc. In this work, streamer inception is studied in various conditions of electrode shapes (from sharp points up to quasi-uniform field), voltage (ac, dc, impulse voltage) and temperature. Streamer inception is detected by the measurement of breakdown voltages in selected conditions. The results obtained show that streamer inception field varies when the electrode shape is changed, in a similar way as in liquids: the inception field decreases when the electrode surface increases. On the other hand, temperature and voltage wave shape have almost no influence on the inception field. Results are discussed in comparison with data already obtained in liquids in similar conditions.

This paper discuss the relations between laboratory studies of breakdown precursors in liquids (usually called "streamers"), and practical applications such as high voltage insulation of power transformers and testing of liquids. The conditions existing within high voltage power transformers (ac voltage, moderately divergent electric field, presence of insulating solids, particles in the oil, etc.) are rather different from those frequently used in the laboratory to study streamers (very divergent field -point-plane geometry-, and impulse voltage). Parameters such as field geometry, voltage waveform, liquid conditioning, can influence either streamer inception or propagation. After a short presentation of streamer phenomena in liquids, the most important effects of these parameters are recalled in this paper. Many features previously observed empirically by the measurement of breakdown voltage can be explained by the behaviour of streamers in conditions close to those actually present in transformers. It remains rather difficult today to model and predict streamer properties (initiation fields, propagation length, velocity, ...) when the liquid nature is changed. The large variety of physical processes involved during initiation and propagation, and the non-linearity of many processes make the study of breakdown in liquids complex. However, knowledge about streamers is helpful to define and measure parameters of practical importance (initiation and propagation conditions), providing a more scientific basis to test and compare the properties of liquids.

The purpose of this work is to evaluate the chemical stability of a bio-degradable insulating oil composed by a mixture of esters based on rape-seed oil. The measurements are done in comparison with a commercial mineral oil. Both oils are subjected to accelerated ageing conditions at 120degC under air (open beaker method). Dielectric properties (dissipation factor, permittivity, conductivity, AC breakdown voltage) and chemical parameters (acidity, water content) are monitored during the ageing process. In the rape-seed based oil, ageing has a negligible influence on the breakdown voltage, whereas conductivity and acid content show a large increase.

Silicone gels are widely used to encapsulate power electronics modules. The objective of this paper is to study the partial discharge (PD) mechanism in a silicone gel, using electrical measurements and fast visualization. Experiments are carried out in a pointplane geometry, using either impulse voltage or ac. Under impulse voltage, the visualization shows that the first discharges recorded in a new sample are due to the initiation and propagation of "streamers", with features close to those previously reported in viscous liquids. Under ac, a stable PD regime rapidly establishes: a streamer creates a cavity with a long lifetime, and PDs occur in this cavity during the subsequent ac waves. Since slow streamers develop during long times (some ms), classical PD measurements do not provide an adequate evaluation of the actual discharge magnitude: very small PDs (1 pC) are recorded, whereas large cavities with a total charge in excess of 10 pC are actually present in the gel. When PDs are repeated permanent degradations of the gel rapidly occur, showing the limited self-healing capabilities of silicone gels.

In this paper, we have investigated the dielectric properties (losses, conductivity) of a modified rape-seed oil (RS50). Dielectric spectroscopy has been done over a wide frequency range (10-2-106Hz) and conductivity measurements according to CEI 61620 standard. The parameters investigated are temperature (-20degC to 120degC) and water content. Frequency spectra of the dissipation factor tgzeta at different temperatures are typical of losses by conduction (in the low frequency range) and of losses by dipole relaxation (in the high frequency range). The influence of temperature is well explained by conduction and relaxation theories taking into account viscosity change. The increase of conductivity with temperature is rather large: a factor of 103 from -20degC to 120degC. Up to about 200% of relative humidity, no significant influence of moisture on the dielectric properties (permittivity, losses, conductivity) has been observed. These results are then discussed in correlation with potential applications of this oil in electrical systems.

Rape-seed oil is considered for electrical insulation at high voltage. In this work, breakdown and streamer propagation in rape seed oil are studied in point-plane gaps up to 20cm, under impulse voltage of both polarities. In both polarities, two main streamer types are observed: "slow" streamers with a velocity of about 2km/s, and much faster streamers up to 150km/s. Compared to mineral oil in the same conditions, fast streamers in rape-seed oil appear at much lower voltage. They are able to propagate over large distances within a short time at moderate voltage. From these results, it is concluded that the properties of streamers in rape-seed oil are less favorable for high voltage insulation than in mineral oil.

In order to increase the knowledge of the processes involved during the degradation of insulating silicone gels under ac stress, recordings of the activity of partial discharges (PD) are performed. Silicone gels are commonly used for the insulation and packaging of high voltage semiconductors such as IGBT modules. We worked on a commercially available dielectric silicone gel. Electrical and optical apparatus allows the measurement of PD's and their location, either on actual power module substrates, or in a point-plane gap. The temperature dependence of PD inception voltage is moderate, while the number of PD's and their charge steeply increases versus temperature. We show that the formation of cavities constitutes the main factor responsible for the degradation under ac conditions. The actual self-healing capabilities of silicone gels are also studied and discussed.

We studied the effects of water absorption (up to 1 wt%) on the dielectric properties of mica/glass/epoxy laminated composites used for high-voltage insulation. The DC resistivity, the dielectric constant and the dielectric loss were studied in the 10 −2 –10 6 Hz range, as a function of water uptake. The dielectric characteristics are strongly affected by water ingress. Upon water sorption the resistivity decreases by several orders of magnitude. Its variation is well described by a percolation law. The low-frequency permittivity rises to very large values. The large increase in the permittivity is related to an electrode polarisation mechanism.

This paper describes experimental measurements carried out to study the dielectric properties of composite dielectric materials (glass cloth/mica/epoxy) used for the insulation of stator bars in high power generators. Due to the structure of the material, composed of a stack of layers, its dielectric properties are nonisotropic. If the material is polluted by water, water diffusion is much faster in the direction parallel to the layers. Dielectric measurements also show that the degradation of properties due to water (increase of DC conductivity, of dielectric losses) is more marked when the electric field direction is parallel to the layers.

This paper describes the effect of water on dielectric properties at high field of composite insulation, based on epoxy reinforced by fibre glass and mica flakes. Samples with controlled water content are prepared by immersion. Breakdown measurements under ac voltage show a marked decrease of breakdown field, when large amounts of water (up to 1.5%) are present in the material. High voltage dielectric spectroscopy measurements were carried out from 0.001 Hz to 1 kHz with various water content and applied fields (up to 5 kV/mm). At low frequency, a very large increase of dielectric losses versus water content, due to the increase of material conductivity is reported. At 50 Hz, tan /spl delta/ higher than 1% are recorded with water content above 0.5%.

This paper presents a study of breakdown and prebreakdown phenomena (streamers) in liquid nitrogen and mineral oil under quasi uniform electric field, under ac and impulse voltage. Streamers preceding breakdown are studied up to 0.5 MPa by high-speed visualization and recording of emitted light. In these conditions, breakdown in LN/sub 2/ is mainly due to negative streamers, initiated at lower voltage than the corresponding positive voltage. Hydrostatic pressure has a limited effect on breakdown voltage, such as in mineral oil. It is shown that the ratio of impulse to ac breakdown voltage in LN/sub 2/ is surprisingly low (close to 1), whereas in the same conditions ac breakdown voltage in mineral oil is lower than impulse breakdown voltage. Practical consequences for the design of HV insulation in superconducting systems are discussed.