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International audience; Surface integrity directly affects the mechanical behavior of the workpiece, which is especially relevant on fatigue behavior. To characterize the quality of the machined surface, aspects such as material damage, roughness or residual stress are considered. Measurement of the material damage of the surface is characterized in some cases as surface drag, depth of the affected machining zone, a phenomenon which takes place due to plastic strain in the surface layer caused by machining stress which could have an influence on residual stress. Surface drag measurement done with optical microscopes has relevant uncertainty. In this paper, a methodology to measure the surface drag with lower uncertainty is proposed. The method consists of measuring the deformation of a grid as a result of the machining process. The grid was created with micromilling. The method was applied to analyze the effect of feed on the surface integrity after orthogonal cutting of Ti-6Al-4V. The depth of the affected layer was measured using a 3D optical measuring device (Alicona Infinite Focus IFG4) and compared with numerical simulations and a good agreement was achieved. In comparison with optical microscope results, it can be concluded that traditional method underestimates surface drag

International audience; Finite Element Modelling used to predict machining outcomes needs to be supplied with the appropriate material thermomechanical properties which are obtained by specific testing devices and methodologies. However, these tests are usually not representative of the extreme conditions achieved in machining processes and the obtained material law may not be suitable enough. Inverse identification could address this problem by obtaining material thermomechanical properties directly from machining outcomes such as cutting forces, temperatures, strain or strain rates. Nevertheless, this technique needs to be supplied with accurate machining outcomes. However, some of them such as strain or strain rate are difficult to be properly measured. The aim of this paper is to present a methodology to measure plastic strain and strain rate during orthogonal machining under plane strain conditions. The main idea is to create a physical microgrid in a workpiece and to analyze the distortion suffered by this grid. The novelty of the method consists on its capability of measuring strain and strain rate fields in a very localized area (primary shear zone) using a single image. The methodology was applied in orthogonal cutting of Ti-6Al-4V under cutting conditions that are representative of the broaching process. Experimental results were compared with DIC measurements, analytical results based on unequal division shear zone model, literature results and with numerical fields obtained from an AdvantEdge-2D model.

International audience; One of the biggest issues of the mechanical cylindrical joints is related to premature wear appearing. This application of bioinspiration principles in an engineering context taking advantage of smart solutions offered by nature in terms of kinematic joints could be a way of solving those problems. This work is focused on joints of one DOF in rotation (revolute or ginglymus joints in biological terms), as this is one of the most common type of mechanical joints. This type of joints can be found in the elbow of some quadrupedal mammals. The articular morphology of the elbow of these animals differs in the presence/absence of a trochlear sulcus. In this study, bio-inspired mechanical joints based on these morphologies (with/without trochlear sulcus) were designed and numerically tested. Their load bearing performance was numerically analysed. This was done through contact simulations using the finite element method under different external loading conditions (axial load, radial load and turnover moment). Results showed that the tested morphologies behave differently in transmission of external mechanical loads. It was found that bio-inspired joints without trochlea sulcus showed to be more specialized in the bearing of turnover moments. Bioinspired joints with trochlea sulcus are more suitable for supporting combined loads (axial and radial load and turnover moments). Learning about the natural rules of mechanical design can provide new insights to improve the design of current mechanical joints.

Thermodiffusion, which leads to a component separation in a mixture due to the thermal gradient, still does not have an unambiguous microscopic picture. Therefore, experimental studies, especially in convection free environment, are important. As part of the 4th campaign on the DCMIX project, thermodiffusion experiments on three compositions of the toluene-methanol-cyclohexane ternary mixture, on a mixture of fullerene-tetralin-toluene and on a mixture of polystyrene-toluene-cyclohexane have been performed in microgravity conditions on board the International Space Station. A binary mixture of polystyrene-toluene has been filled into the companion cell for the campaign. The Selectable Optical Diagnostics Instrument (SODI), wich is a two-wavelength Mach-Zehnder interferometer for the ternary mixtures, plus a monochromatic Mach-Zehnder interferometer for the binary mixture, has been used in order to obtain the temperature and the concentration fields in the cells. Precisely, it is a 5-steps phase-shifting interferometry technique which is implemented with SODI, producing by means of laser illumination a set of 5 phase-shifted images of π/2 between them as function of the time. A total of 58 runs of various durations and at different mean temperatures have been conducted. Here, we evaluate the contrast of the interferograms, the quality in the phase stepping, the stability of the thermal regulation of the experiments and the level of environmental disturbances on board the space station during the campaign., SCOPUS: ar.j, info:eu-repo/semantics/published

International audience; Superconductor/Ferromagnet (S/F) hybrid systems show interesting magneto-transport behaviors that result from the transfer of properties between both constituents. For instance, magnetic memory can be transferred from the F into the S through the pinning of superconducting vortices by the ferromagnetic textures. The ability to tailor this type of induced behavior is important to broaden its range of application. Here we show that engineering the F magnetization reversal allows tuning the strength of the vortex pinning (and memory) effects, as well as the field range in which they appear. This is done by using magnetic multilayers in which Co thin films are combined with different heavy metals (Ru, Ir, Pt). By choosing the materials, thicknesses, and stacking order of the layers, we can design the characteristic domain size and morphology, from out-of-plane magnetized stripe domains to much smaller magnetic skyrmions. These changes strongly affect the magneto-transport properties. The underlying mechanisms are identified by comparing the experimental results to a magnetic pinning model. * javier.villegas@cnrs-thales.fr 2

International audience; Surface integrity induced by machining process affects strongly the performance of functional products, for instance, the fatigue life as well as the resistance to stress corrosion cracking. Consequently, it is relevant to evaluate the induced properties on and beneath the machined surfaceto ensure the good performance of the mechanical components while operating under either static or cyclic loads. Furthermore, this is even more important when designing critical components that withstand high loads at high temperatures. In this context, many studies have been carried out in order to characterize the surface integrity (residual stresses, surface roughness, micro-hardness of the affected layer) when machining Inconel 718. However, so far, the cryogenic effect on surface integrity of Inconel 718 is not well established although some preliminary works have already been developed. Therefore, this work aimed to point out the performance of cryogenic machining using the carbon dioxide CO2 as a cryogenic cutting fluid, considering as a reference the conventional lubrication. A comparative study has been carried out during turning operations of Inconel 718 using the same cutting parameters and the same tool geometry. Microhardness measurements showed that the CO2 condition induced higher strain hardening near the surface while conventional condition did not generate notable difference compared to the bulk material microhardness. With respect to residual stresses, results showed that conventional lubrication generated higher tensile residual stress near the surface along the cutting direction when using new tools. As for CO2 cryogenic condition, lower tensile residual stresses have been obtained near the surface. In addition, CO2 condition induced the largest compressive peak when using new and semi−worn tools in comparison with conventional lubrication.

Safety issues related to lithium-ion batteries are a driving force in the search for new energy storage systems. Lithium-ion capacitors are becoming recognised as promising devices to address the question of safety. These products are a combination of lithium-ion batteries and electric double-layer capacitors in terms of energy and power density. The aim of this work is to assess lithium-ion capacitor safety under over-charge and under-discharge processes for pouch and prismatic cells. In the course of performing abuse tests, no evidence was found of severe hazard (explosion, fire or flame, rupture or major leakage). Quantitative external parameters (thickness, resistance and mass) and electro-thermal measurements showed an increase of swelling and internal resistance, which caused a decrease of capacity and energy efficiency in all cases. The ultrasound characterization technique confirmed that there were irreversible physical modifications of the materials under abuse conditions on prismatic cells, which could not be seen with the commonly used magnitudes (U, I, T). This technique was also used for the identification of the start of cell degradation. In post-mortem analysis, were observed different degradation phenomena such as melting of the separator and delamination in the electrodes.

International audience; Nickel-based superalloys are widely exploited in turbojets components which are subjected to intense thermal and mechanical loadings during their operation. In fact, they exhibit excellent mechanical properties over a wide range of temperature and high corrosion and creep resistance. However, these materials induce several problems related to the shaping by machining due to essentially high heat resistance, high hardening tendency, high chemical affinity with tool material and low thermal conductivity leading to very high temperature in the cutting zone. In this context, assisted machining processes aim to improve the productivity of certain materials that are difficult to cut. Indeed, in order to keep the tool cold, it has been proposed to use cryogenic fluids (liquid nitrogen LN2 and carbon dioxide CO2 as coolant for effectively reducing temperatures since their vaporization temperatures are equal to -196°C and -75°C respectively. In this context, previous researches have focused on the study of the efficiency of this technique with respect to the machinability of several materials such as titanium alloys and nickel-based alloys. It has been shown that the tool life is improved when machining titanium alloys, unlike nickel-based alloys. For this reason, this paper is devoted to a comparison between two cryogenic fluids (LN2 and CO2) with regard to their effects on tool life when machining Inconel 718 considering as a reference the conventional lubrication. Results showed that tool life is the longest in conventional lubrication. However, under cryogenic conditions, tool life is the shortest in the case of LN2 condition whereas CO2 condition exhibits lower value compared to the traditional lubrication.

This paper describes the European Space Agency (ESA) experiments devoted to study thermodiffusion of fluid mixtures in microgravity environment, where sedimentation and convection do not affect the mass flow induced by the Soret effect. First, the experiments performed on binary mixtures in the IVIDIL and GRADFLEX experiments are described. Then, further experiments on ternary mixtures and complex fluids performed in DCMIX and planned to be performed in the context of the NEUF-DIX project are presented. Finally, multi-component mixtures studied in the SCCO project are detailed. Graphical abstract: [Figure not available: see fulltext.]., 0, SCOPUS: re.j, info:eu-repo/semantics/published

International audience; The most important challenges when machining difficult-to-cut alloys used in critical applications consist mainly in increasing tool life as well as improving the component surface integrity. In particular, the nickel based alloys exhibit very low thermal conductivity inducing higher cutting temperature and thereby rapid tool wear. In this context, cryogenic machining is a promising approach that enhances cooling efficiency either when using the liquid nitrogen LN2 or the carbon dioxide LCO2. According to previous works, cryogenic machining has been carried out on several work materials such as titanium alloys and nickel based alloys. Their findings figured out that longer tool life and better surface integrity were obtained when machining titanium alloys, unlike nickel based alloys. In this work, a comparative study has been carried out in order to investigate the cryogenic machining performance during turning operation of Inconel 718 with respect to tool wear behavior and surface integrity of the machined part. In fact, two cryogenic fluids were employed namely LN2 and LCO2 considering as a reference the conventional lubrication. This study illustrates that conventional lubrication and LCO2 cryogenic cooling allowed to obtain similar machining time, tool wear and surface finish. Nevertheless, LN2 cryogenic machining resulted in the lowest tool life as well as the poorest surface finish. Moreover, residual stresses have been measured beneath the machined surfaces when machining using new tools and tools with different levels of tool flank wear. It was observed that compared to conventional lubrication, both cryogenic conditions showed better results with respect to residual stress profiles along the machined surfaces

International audience; The storage modulus variation of anisotropic magnetorheological elastomers (MREs) induced by an external magnetic field was modelled in the frequency domain. This involves synthesising five anisotropic MREs with different particle content and measuring its dynamic and magnetic properties. Dynamic properties were measured using a rheometer equipped with a magnetorheological cell and the magnetic permeability of each sample was measured with a vibrating sample magnetometer. Scanning Electron Microscope images were used to determine particle distribution. A four parameter fractional derivative model was used to describe MRE viscoelasticity in the absence of magnetic field and the fitting error was not larger than 1%. Magneto-induced modulus was also studied and two different models were analysed, the one of Jolly et al. (Smart Mater Struct;5:607 (1999)) and the other one of López-López et al. (J Rheol. 56:1209 (2012)). The first model underestimated the influence of the magnetic field for low particle contents while at high ones it overestimated the magnetic field effect, up to 13%. However, in the second model magnetic permeability values were used, and the error between the model prediction and experimental data did not exceed 7%. Hence, a new linear magneto-viscoelastic model was proposed in frequency domain for anisotropic MREs based on López-López et al. model, which predicts the effect of magnetic field on the dynamic shear modulus in function of particle content and frequency.

International audience; Nickel based alloys are extensively used in the aerospace industry due to the excellent corrosion resistance and high mechanical properties that are maintained up to elevated temperatures (600–800 °C). However, these superalloys are classified as difficult-to-cut and therefore modelling and simulation of the machining processes has become a key in the machinability assessment of nickel based alloys. The reliability of Finite Element Models (FEM) largely depends on the quality of input parameters, one of the most relevant being the constitutive material model representing work material behavior under high strain, strain rate and temperatures. In order to develop a reliable material model, the present work deals with a complete characterization of Inconel 718. Uniaxial compression tests at testing temperatures close to those found in machining (21–1050 °C) and high strain rates (10°−10 2 s −1 ) were performed on the Gleeble 3500 testing machine. Moreover, the microstructural analysis and microhardness measurements of the testing samples were performed, in order to correlate the microstructural state with the mechanical properties of the Inconel 718. Based on this experimental work, a new coupled empirical model is proposed to describe the particular behaviour of nickel based alloys at elevated temperatures and high strain rates. This material behaviour model introduces softening phenomena as well as the coupling between the temperature and the strain rate known to occur experimentally, for machining FEM simulations with Inconel 718 superalloy.

International audience; Near-beta titanium alloys like Ti555.3 are increasingly being used in aeronautics replacing in some critical applications the most common Ti6Al4V. However, these near-beta titanium alloys have a poor machinability rating which needs to be overcome so as to maintain at least the same productivity levels as in Ti6Al4V.This paper presents the machinability results carried out for Ti555.3 compared with the commonly used Ti6Al4V. The aim of this research work is to understand tool wear mechanisms when machining Ti555.3. Analysis of variables such as cutting forces, chip geometry and tool wear shows that: (I) greater difficulty is encounterd when machining Ti555.3 alloy compared with Ti6Al4V alloy which can be machined at higher speeds up to 90 m min(-1); (II) there was a correlation between the mechanical properties of work material, tool wear, and component forces; (III) the occurrence of the diffusion process leads to the formation of a layer of adhered material composed of Ti and TiC on the tool's rake face for both Ti alloys.

This paper deals with the analysis of thestrain path's influence on the elastic behaviour of TRIP700 steel; it aims to validate the cyclic testing method to characterise inelastic behaviour of advanced high strength steels (AHSS). Different cyclic tests are done, where the strain path is changed from test to test. Large deformation strain gages are used to determine the inelastic behaviour of the specimens at macro-level. At a lower scale, stress measurements are carried out using the XRD technique during anin-situ tensile test: ferrite and austenite phases’stresses are measured before unloading and after loading again to study the strain path's influence.By means of this work it is confirmed that the elastic strain path has no influence on the unloading–loading of this TRIP steel. These results prove that conventional loading–unloading cyclic testing is a valid methodology for a detailed characterisation of the elastic modulus and reliable numerical modelling of springback.; International audience; This paper deals with the analysis of thestrain path's influence on the elastic behaviour of TRIP700 steel; it aims to validate the cyclic testing method to characterise inelastic behaviour of advanced high strength steels (AHSS). Different cyclic tests are done, where the strain path is changed from test to test. Large deformation strain gages are used to determine the inelastic behaviour of the specimens at macro-level. At a lower scale, stress measurements are carried out using the XRD technique during anin-situ tensile test: ferrite and austenite phases’stresses are measured before unloading and after loading again to study the strain path's influence.By means of this work it is confirmed that the elastic strain path has no influence on the unloading–loading of this TRIP steel. These results prove that conventional loading–unloading cyclic testing is a valid methodology for a detailed characterisation of the elastic modulus and reliable numerical modelling of springback.

International audience; After translation, the first stages traditionally involved in the materials selection are filtration and classification, which require formulation of criteria (constraints or objectives) deduced from information written in the set Of material requirements. These criteria, which are representative of the behavior of the material and the studied structure, must be formulated analytically in order to be used during selection stage. However, for complex behavior, analytical processing of models is no longer possible and it can be replaced by a combination of numerical resolution methods and an optimization method which make it possible to obtain approximate formal expressions of the criteria. In this paper, a complete selection method is proposed. The method is applied to the constraints as well as the objectives, in order to carry out the filtration and classification stages at the same time. The study of the thermomechanical behavior of a machine tool frame has been used to demonstrate the validity of the proposed method.