48 results on '"Thickness uniformity"'
Search Results
2. Control of Meniscus Formation Using an Electrohydrodynamics Module in Roll-to-Roll Systems for the Stable Coating of Functional Layers.
- Author
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Kim, Minjae, Jo, Minho, Noh, Jaehyun, Lee, Sangbin, Yun, Junyoung, Cho, Gyoujin, and Lee, Changwoo
- Subjects
- *
ELECTROHYDRODYNAMICS , *SURFACE tension , *SURFACE coatings , *HIGH voltages - Abstract
In fabricating functional layers, including thin-film transistors and conductive electrodes, using roll-to-roll (R2R) processing on polymer-based PET film, the instability of the slot-die coating meniscus under a high-speed web impedes functional layer formation with the desired thickness and width. The thickness profiles of the functional layers significantly impact the performance of the final products. In this study, we introduce an electrohydrodynamic (EHD)-based voltage application module to a slot-die coater to ensure the uniformity of the cross-machine direction (CMD) thickness profile within the functional layer and enable a stable, high-speed R2R process. The module can effectively control the spreadability of the meniscus by utilizing variations in the surface tension of the ink. The effectiveness of the EHD module was experimentally verified by applying a high voltage to a slot-die coater while keeping other process variables constant. As the applied voltage increases, the CMD thickness deviation reduces by 64.5%, and the production rate significantly increases (up to 300%), owing to the formation of a stable coated layer. The introduction of the EHD-based application module to the slot-die coater effectively controlled the spreadability of the meniscus, producing large-area functional layers. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
3. An Effect of Layered Auxiliary Cathode on Thickness Uniformity in Micro Electroforming Process.
- Author
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Wang, Huan, Xing, Jianpeng, Fan, Tao, Liu, Jinhu, Xie, Jing, and Li, Chaobo
- Subjects
ELECTROFORMING ,UNIFORMITY ,CATHODES - Abstract
Thickness nonuniformity is a bottleneck in the micro electroforming process of micro-metal devices. In this paper, a new method of fabricating a layered auxiliary cathode is proposed to improve the thickness uniformity of a micro-electroforming layer. In order to analyze the general applicability of the proposed method, four basic microstructures, namely circular, square, regular triangular, and regular hexagonal were used to study the effect of a layered auxiliary cathode on thickness uniformity through simulation and experimentation. The simulation results showed that with the help of the proposed auxiliary cathode, the thickness nonuniformity of four microstructures should decrease due to the reduced edge effect of the current density. The experimental results showed that the thickness uniformity of four microstructures fabricated via the proposed method was improved by 190.63%, 116.74%, 80.43%, and 164.30% compared to that fabricated via the traditional method, respectively. Meanwhile, the micro-gear was fabricated and the nonuniformity was reduced by 101.15% using the proposed method. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
4. Concurrently Fabricating Precision Meso- and Microscale Cross-Scale Arrayed Metal Features and Components by Using Wire-Anode Scanning Electroforming Technique.
- Author
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Li, Shicheng, Ming, Pingmei, Zhang, Junzhong, Zhang, Yunyan, and Yan, Liang
- Subjects
ELECTROFORMING ,FLUID flow ,MASS transfer ,METALS ,ELECTRIC fields - Abstract
In order to improve the thickness uniformity of the electroformed metal layer and components, a new electroforming technique is proposed—wire-anode scanning electroforming (WAS-EF). WAS-EF uses an ultrafine inert anode so that the interelectrode voltage/current is superimposed upon a very narrow ribbon-shaped area at the cathode, thus ensuring better localization of the electric field. The anode of WAS-EF is in constant motion, which reduces the effect of the current edge effect. The stirring paddle of WAS-EF can affect the fluid flow in the microstructure, and improve the mass transfer effect inside the structure. The simulation results show that, when the depth-to-width ratio decreases from 1 to 0.23, the depth of fluid flow in the microstructure can increase from 30% to 100%. Experimental results show that. Compared with the traditional electroforming method, the single metal feature and arrayed metal components prepared by WAS-EF are respectively improved by 15.5% and 11.4%. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
5. Improving the Thickness Uniformity of Micro Gear by Multi-Step, Self-Aligned Lithography and Electroforming.
- Author
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Wang, Huan, Xie, Jing, Fan, Tao, Sun, Dapeng, and Li, Chaobo
- Subjects
ELECTROFORMING ,LITHOGRAPHY ,UNIFORMITY ,PHOTORESISTS - Abstract
The thickness nonuniformity of an electroformed layer is a bottleneck problem for electroformed micro metal devices. In this paper, a new fabrication method is proposed to improve the thickness uniformity of micro gear, which is the key element of various microdevices. The effect of the thickness of the photoresist on the uniformity was studied by simulation analysis, which showed that as the thickness of the photoresist increased, the thickness nonuniformity of the electroformed gear should decrease due to the reduced edge effect of the current density. Differently from the traditional method performed by one-step front lithography and electroforming, multi-step, self-aligned lithography and electroforming are used to fabricate micro gear structures in proposed method, which intermittently keeps the thickness of photoresist from decreasing during processes of alternate lithography and electroforming. The experimental results show that the thickness uniformity of micro gear fabricated by the proposed method was improved by 45.7% compared with that fabricated by the traditional method. Meanwhile, the roughness of the middle region of the gear structure was reduced by 17.4%. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
6. Wall Thickness Uniformity in ISF of Hydraulic Support: System Design, Finite Element Analysis and Experimental Verification.
- Author
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Shang, Miao, Li, Yan, Yang, Mingshun, Chen, Yunshuai, Bai, Lang, and Li, Pengyang
- Subjects
FINITE element method ,SYSTEMS design ,UNIFORMITY - Abstract
Uniform wall thickness plays an essential role in avoiding forming failure in incremental sheet forming. However, it is challenging to promote the uniform distribution of wall thickness in single-pass forming of high wall angle and complex three-dimensional thin-walled parts using flexible dieless incremental sheet forming technology. In this article, based on the hydraulic support single-point incremental sheet forming technology, the finite element software is used to simulate and analyze the influence of different support pressure on the wall thickness distribution and the uniform critical angle of single-pass incremental sheet forming truncated pyramid parts. The results show that the hydraulic support can effectively improve the thickness uniformity and critical forming angle. In addition, a single-point increment experiment system of hydraulic support is designed, and the uniform critical angle of wall thickness corresponding to different support pressure is obtained. The experimental results are consistent with the finite element simulation results. Therefore, this article provides guidance for manufacturing high wall angles and complex parts with uniform wall thickness in single-pass incremental sheet forming. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
7. An optional surgical technique for obtaining lamellar donor grafts: a pilot study
- Author
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Xin Liu, Chunyu Liu, Hui Lin, Yuting Shao, Li Zhang, and Yanlong Bi
- Subjects
Reversed manual dissection ,Conventional manual dissection ,Keratoplasty ,Lamellar donor tissue ,Surface quality ,Thickness uniformity ,Ophthalmology ,RE1-994 - Abstract
Abstract Background To evaluate the surface quality and thickness uniformity of lamellar donor grafts using an optional surgical technique called reversed manual dissection (RMD) in porcine corneas. Methods Twenty-four paired porcine corneas (48 eyes) were numbered 1 to 24 and divided into 6 groups. All left corneas were assigned to conventional manual dissection (CMD), and all right corneas were assigned to RMD. Each group contained 8 corneas. For Groups I, II, and III, 30, 50, and 70% of the entire corneal thickness was dissected using CMD. For groups IV, V, and VI, 70, 50, and 30% of the entire corneal thickness was dissected using RMD. The residual stromal thickness was examined by anterior segment optical coherence tomography (ASOCT) to assess the thickness uniformity and scanning electron microscopy (SEM) to assess the surface quality. Results The thickness uniformity of the lamellar grafts between each paired group was not significantly different (p > 0.05). The qualitative surface roughness grading (QiSR) evaluated by masked observers through SEM was significantly higher in the RMD groups (p
- Published
- 2022
- Full Text
- View/download PDF
8. An Effect of Layered Auxiliary Cathode on Thickness Uniformity in Micro Electroforming Process
- Author
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Huan Wang, Jianpeng Xing, Tao Fan, Jinhu Liu, Jing Xie, and Chaobo Li
- Subjects
micro-electroforming ,thickness uniformity ,auxiliary electrode ,edge effect ,Mechanical engineering and machinery ,TJ1-1570 - Abstract
Thickness nonuniformity is a bottleneck in the micro electroforming process of micro-metal devices. In this paper, a new method of fabricating a layered auxiliary cathode is proposed to improve the thickness uniformity of a micro-electroforming layer. In order to analyze the general applicability of the proposed method, four basic microstructures, namely circular, square, regular triangular, and regular hexagonal were used to study the effect of a layered auxiliary cathode on thickness uniformity through simulation and experimentation. The simulation results showed that with the help of the proposed auxiliary cathode, the thickness nonuniformity of four microstructures should decrease due to the reduced edge effect of the current density. The experimental results showed that the thickness uniformity of four microstructures fabricated via the proposed method was improved by 190.63%, 116.74%, 80.43%, and 164.30% compared to that fabricated via the traditional method, respectively. Meanwhile, the micro-gear was fabricated and the nonuniformity was reduced by 101.15% using the proposed method.
- Published
- 2023
- Full Text
- View/download PDF
9. Synthesis and Characterization of Boron Thin Films Using Chemical and Physical Vapor Depositions.
- Author
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Schurink, Bart, van den Beld, Wesley T. E., Tiggelaar, Roald M., van de Kruijs, Robbert W. E., and Bijkerk, Fred
- Subjects
PHYSICAL vapor deposition ,CHEMICAL vapor deposition ,THIN films ,MAGNETRON sputtering ,PLASMA-enhanced chemical vapor deposition ,BORON - Abstract
Boron as thin film material is of relevance for use in modern micro- and nano-fabrication technology. In this research boron thin films are realized by a number of physical and chemical deposition methods, including magnetron sputtering, electron-beam evaporation, plasma enhanced chemical vapor deposition (CVD), thermal/non-plasma CVD, remote plasma CVD and atmospheric pressure CVD. Various physical, mechanical and chemical characteristics of these boron thin films are investigated, i.e., deposition rate, uniformity, roughness, stress, composition, defectivity and chemical resistance. Boron films realized by plasma enhanced chemical vapor deposition (PECVD) are found to be inert for conventional wet chemical etchants and have the lowest amount of defects, which makes this the best candidate to be integrated into the micro-fabrication processes. By varying the deposition parameters in the PECVD process, the influences of plasma power, pressure and precursor inflow on the deposition rate and intrinsic stress are further explored. Utilization of PECVD boron films as hard mask for wet etching is demonstrated by means of patterning followed by selective structuring of the silicon substrate, which shows that PECVD boron thin films can be successfully applied for micro-fabrication. [ABSTRACT FROM AUTHOR]
- Published
- 2022
- Full Text
- View/download PDF
10. An optional surgical technique for obtaining lamellar donor grafts: a pilot study.
- Author
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Liu, Xin, Liu, Chunyu, Lin, Hui, Shao, Yuting, Zhang, Li, and Bi, Yanlong
- Subjects
CORNEAL transplantation ,OPERATIVE surgery ,OPTICAL coherence tomography ,PILOT projects ,SCANNING electron microscopy ,SURFACE roughness - Abstract
Background: To evaluate the surface quality and thickness uniformity of lamellar donor grafts using an optional surgical technique called reversed manual dissection (RMD) in porcine corneas.Methods: Twenty-four paired porcine corneas (48 eyes) were numbered 1 to 24 and divided into 6 groups. All left corneas were assigned to conventional manual dissection (CMD), and all right corneas were assigned to RMD. Each group contained 8 corneas. For Groups I, II, and III, 30, 50, and 70% of the entire corneal thickness was dissected using CMD. For groups IV, V, and VI, 70, 50, and 30% of the entire corneal thickness was dissected using RMD. The residual stromal thickness was examined by anterior segment optical coherence tomography (ASOCT) to assess the thickness uniformity and scanning electron microscopy (SEM) to assess the surface quality.Results: The thickness uniformity of the lamellar grafts between each paired group was not significantly different (p > 0.05). The qualitative surface roughness grading (QiSR) evaluated by masked observers through SEM was significantly higher in the RMD groups (p < 0.001). The quantitative surface roughness grading (QnSR) acquired from the Mountains software was significantly lower in the RMD groups (p < 0.001).Conclusions: RMD is an optional surgical technique for obtaining porcine lamellar grafts. The thickness uniformity of RMD is comparable to that of CMD, and a smoother surface with fewer ridges and roughness is achieved compared to CMD. [ABSTRACT FROM AUTHOR]- Published
- 2022
- Full Text
- View/download PDF
11. Concurrently Fabricating Precision Meso- and Microscale Cross-Scale Arrayed Metal Features and Components by Using Wire-Anode Scanning Electroforming Technique
- Author
-
Shicheng Li, Pingmei Ming, Junzhong Zhang, Yunyan Zhang, and Liang Yan
- Subjects
cross-scale arrayed metal ,thickness uniformity ,wire-anode scanning electroforming ,Mechanical engineering and machinery ,TJ1-1570 - Abstract
In order to improve the thickness uniformity of the electroformed metal layer and components, a new electroforming technique is proposed—wire-anode scanning electroforming (WAS-EF). WAS-EF uses an ultrafine inert anode so that the interelectrode voltage/current is superimposed upon a very narrow ribbon-shaped area at the cathode, thus ensuring better localization of the electric field. The anode of WAS-EF is in constant motion, which reduces the effect of the current edge effect. The stirring paddle of WAS-EF can affect the fluid flow in the microstructure, and improve the mass transfer effect inside the structure. The simulation results show that, when the depth-to-width ratio decreases from 1 to 0.23, the depth of fluid flow in the microstructure can increase from 30% to 100%. Experimental results show that. Compared with the traditional electroforming method, the single metal feature and arrayed metal components prepared by WAS-EF are respectively improved by 15.5% and 11.4%.
- Published
- 2023
- Full Text
- View/download PDF
12. Wall Thickness Uniformity in ISF of Hydraulic Support: System Design, Finite Element Analysis and Experimental Verification
- Author
-
Miao Shang, Yan Li, Mingshun Yang, Yunshuai Chen, Lang Bai, and Pengyang Li
- Subjects
incremental sheet forming ,single point incremental forming ,thickness distribution ,thickness uniformity ,Mechanical engineering and machinery ,TJ1-1570 - Abstract
Uniform wall thickness plays an essential role in avoiding forming failure in incremental sheet forming. However, it is challenging to promote the uniform distribution of wall thickness in single-pass forming of high wall angle and complex three-dimensional thin-walled parts using flexible dieless incremental sheet forming technology. In this article, based on the hydraulic support single-point incremental sheet forming technology, the finite element software is used to simulate and analyze the influence of different support pressure on the wall thickness distribution and the uniform critical angle of single-pass incremental sheet forming truncated pyramid parts. The results show that the hydraulic support can effectively improve the thickness uniformity and critical forming angle. In addition, a single-point increment experiment system of hydraulic support is designed, and the uniform critical angle of wall thickness corresponding to different support pressure is obtained. The experimental results are consistent with the finite element simulation results. Therefore, this article provides guidance for manufacturing high wall angles and complex parts with uniform wall thickness in single-pass incremental sheet forming.
- Published
- 2023
- Full Text
- View/download PDF
13. Improving the Thickness Uniformity of Micro Gear by Multi-Step, Self-Aligned Lithography and Electroforming
- Author
-
Huan Wang, Jing Xie, Tao Fan, Dapeng Sun, and Chaobo Li
- Subjects
micro-electroforming ,thickness uniformity ,self-aligned lithography ,roughness ,Mechanical engineering and machinery ,TJ1-1570 - Abstract
The thickness nonuniformity of an electroformed layer is a bottleneck problem for electroformed micro metal devices. In this paper, a new fabrication method is proposed to improve the thickness uniformity of micro gear, which is the key element of various microdevices. The effect of the thickness of the photoresist on the uniformity was studied by simulation analysis, which showed that as the thickness of the photoresist increased, the thickness nonuniformity of the electroformed gear should decrease due to the reduced edge effect of the current density. Differently from the traditional method performed by one-step front lithography and electroforming, multi-step, self-aligned lithography and electroforming are used to fabricate micro gear structures in proposed method, which intermittently keeps the thickness of photoresist from decreasing during processes of alternate lithography and electroforming. The experimental results show that the thickness uniformity of micro gear fabricated by the proposed method was improved by 45.7% compared with that fabricated by the traditional method. Meanwhile, the roughness of the middle region of the gear structure was reduced by 17.4%.
- Published
- 2023
- Full Text
- View/download PDF
14. Enhanced thickness uniformity of large-scale α-Ga2O3 epilayers grown by vertical hot-wall mist chemical vapor deposition.
- Author
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Park, Sun-Young, Ha, Minh-Tan, Kim, Kyoung-Ho, Van Lich, Le, Shin, Yun-Ji, Jeong, Seong-Min, Kwon, Se-Hun, and Bae, Si-Young
- Subjects
- *
CHEMICAL vapor deposition , *AEROSOLS , *SAPPHIRES , *UNIFORMITY , *THIN films , *EPITAXY , *GALLIUM nitride films , *EPITAXIAL layers - Abstract
Smooth surface morphology and high thickness uniformity heteroepitaxy of corundum-structured (α-) gallium oxide (Ga 2 O 3) crystalline thin films on 100-mm diameter c -plane sapphire substrates were successfully demonstrated using vertical hot-wall mist chemical vapor deposition (CVD). The growth rate and surface morphology of the epitaxial layers were numerically and experimentally found to be dependent on the diameter of the precursor-diluted microdroplets approaching the substrate surface. Since the microdroplet is gradually evaporated while traveling through the furnace, the growth variables such as temperature, mist-flow velocity, and substrate position were tuned to obtain a suitable diameter of microdroplets approaching the substrate. In this study, the diameter of the approaching microdroplet was ≈2 μm, which was optimal for the smooth surface (root mean square roughness ≈1 nm) of α -Ga 2 O 3 epitaxial layers with a growth rate of ≈230 nm/h. Due to the even flow of mist in the vertical furnace, high thickness uniformity of the α -Ga 2 O 3 epitaxial layer is guaranteed on large-scale substrates, with a standard deviation of thickness as small as 28 nm, paving the way for highly reliable Ga 2 O 3 -based electric and optoelectronic devices. [ABSTRACT FROM AUTHOR]
- Published
- 2022
- Full Text
- View/download PDF
15. Incremental forming based on a virtual auxiliary body: analysis of thickness uniformity.
- Author
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Zhu, Hu, Liu, Luteng, and Liu, Yibo
- Subjects
- *
UNIFORMITY , *STANDARD deviations , *SHEET metal , *FACTORIAL experiment designs , *SHEET metal work - Abstract
To improve the thickness uniformity of sheet metal parts in incremental forming method based on a virtual auxiliary body, the effect of relevant parameters on the thickness uniformity was studied from both overall and local perspectives. Finite element (FE) method was used to carry out the single-factor and two-level factorial experiments, in which standard deviation of the thickness of section nodes was used as a response to analyzing the effect of factors on the thickness uniformity. First, the mean effects of each factor were obtained and the factor levels of factorial experiments were determined through a single-factor experiment. Then, the interaction effect between factors was analyzed and the optimal combination of parameters was determined through factorial experiments. From the FE analysis, it was found that the desired forming angle and the gap at the bottom have obvious mean effects and interactional effects on the thickness uniformity. Finally, the initial and optimal parameters were used for forming experiments. In the forming experiments, the overall and local thickness standard deviations of section nodes were reduced from 0.194 to 0.088 mm and from 0.149 to 0.081 mm, respectively, which means that the optimized parameters can effectively improve the thickness uniformity of sheet metal parts. [ABSTRACT FROM AUTHOR]
- Published
- 2021
- Full Text
- View/download PDF
16. Strain State in Metal Sheet Axisymmetric Stretching with Variable Initial Thickness: Numerical and Experimental Results.
- Author
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Giuliano, Gillo and Polini, Wilma
- Subjects
SHEET metal ,ALUMINUM sheets ,ALUMINUM alloys ,MOUTH protectors - Abstract
Featured Application: This paper presents a stretching process of a metal sheet with a variable thickness. It gives products with better performances than that with constant thickness. This work presents a finite element model to analyze the distribution of the strains due to an axisymmetric stretching of a metal sheet. The sheet is characterized by a variable initial thickness. The resulting strain state is compared with that of a sheet with a constant initial thickness. The results of the present study allow asserting that the distribution of strains in the sheet can be controlled by setting opportunely the trend of the sheet initial thickness. In this way, it is possible to see that, starting from a sheet with variable initial thickness, a lighter final product is obtained, whose final thickness distribution is more uniform than that of the product obtained from a classic stretching process that requires a sheet with constant initial thickness. Encouraging results from an experimental activity carried out on an AA6060 aluminum alloy sheet, whose trend of initial thicknesses was prepared by removing material from a commercial sheet with a constant thickness, allow us to note the good agreement with what was theoretically highlighted. [ABSTRACT FROM AUTHOR]
- Published
- 2021
- Full Text
- View/download PDF
17. The Pamir Yaks of North Tajikistan: Specifics of Hide Formation
- Author
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Muhiddinov A., Popov A., Bobohojaev R., Sharipov I., and Sorochkin M.
- Subjects
skin ,hide ,yaks ,cattle ,weight ,area ,thickness of skin ,thickness uniformity ,chemical composition ,Food processing and manufacture ,TP368-456 - Abstract
In all animals, the hide mass increases together with live body weight. At the age of 6 months and 3 years, the total weight of yak hide is almost two times higher than in other cattle. At 6 months, the thickness of yak hide in all topographical points exceeds that of cowhide by almost two times. By one and three years, the difference in the reference point disappears. However, the neck and the bellous hides of yak remain 25–40% thicker, and the skin area of other breeds of cattle exceeds that of yak at all ages by 35–40%. For the yaks of the Aininks Region, the optimal hide removal period is from birth to 3–4 years. For the animals over 4 years old, the hide yield by weight becomes relatively low. As far as thickness uniformity is concerned, the best skins for leather processing are those obtained from yaks under 3 years old, since they have the lowest degree of slackness. As for the chemical composition, the moisture of yak hide is 2.0–2.5% higher and the hide substance is 7.0–18.5% lower than in cowhide. This is, probably, connected with a certain reserve of water, or the so-called «depot moisture», in the skin of the animal. For all age periods, the moisture of the bellous yak hides is lower and fat content is by 1.5–2.2% higher than in other topographical areas. Apparently, this is due to the thermal adaptation of animals to the habitat conditions.
- Published
- 2018
- Full Text
- View/download PDF
18. Thickness Uniformity Dependence on Polymer Viscosity in Silver-Nanowire-Embedded Flexible and Transparent Electrodes.
- Author
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Chae, Moonsoo, Ko, Dongwook, Ma, Yoohan, Jo, Sungjin, Hyun, Dong Choon, Oh, Hyeon-Ju, and Kim, Jongbok
- Subjects
ELECTRODES ,VISCOSITY ,SPIN coating ,VISCOSITY solutions ,OPTOELECTRONIC devices ,SEMICONDUCTOR nanowires - Abstract
We herein report the effect of the viscosity of a prepolymer solution on the thickness uniformity of silver-nanowire-embedded flexible transparent electrodes. We adopted a model system with all the prepolymer solutions possessing identical physical properties except for the viscosity and then explored the most common prepolymer solutions for silver-nanowire-embedded flexible electrodes. In all experiments, single-step spin coating was conducted to coat the prepolymer solution on silver nanowires. We found that the electrodes were thinner for lower viscosity. However, the thickness ratio between the center and edge was comparable (50–60%) and independent of the prepolymer solution viscosity. This indicates that the viscosity does not determine the thickness uniformity, and that the coating method itself is vital to obtain films with uniform thickness. The flexible electrodes were introduced into organic solar cells. Their device performance was comparable regardless of the position of the electrodes and their thickness. This is because the thickness difference of the flexible electrodes did not affect their transmittance significantly. Thus, we conclude that although different coating approaches are needed to obtain flexible electrodes with high uniformity, the performance of optoelectronic devices on silver-nanowire-embedded flexible electrodes is independent of them. [ABSTRACT FROM AUTHOR]
- Published
- 2020
- Full Text
- View/download PDF
19. Strain State in Metal Sheet Axisymmetric Stretching with Variable Initial Thickness: Numerical and Experimental Results
- Author
-
Gillo Giuliano and Wilma Polini
- Subjects
AA6060 aluminum alloy ,sheet metal stretching ,formability ,thickness uniformity ,Technology ,Engineering (General). Civil engineering (General) ,TA1-2040 ,Biology (General) ,QH301-705.5 ,Physics ,QC1-999 ,Chemistry ,QD1-999 - Abstract
This work presents a finite element model to analyze the distribution of the strains due to an axisymmetric stretching of a metal sheet. The sheet is characterized by a variable initial thickness. The resulting strain state is compared with that of a sheet with a constant initial thickness. The results of the present study allow asserting that the distribution of strains in the sheet can be controlled by setting opportunely the trend of the sheet initial thickness. In this way, it is possible to see that, starting from a sheet with variable initial thickness, a lighter final product is obtained, whose final thickness distribution is more uniform than that of the product obtained from a classic stretching process that requires a sheet with constant initial thickness. Encouraging results from an experimental activity carried out on an AA6060 aluminum alloy sheet, whose trend of initial thicknesses was prepared by removing material from a commercial sheet with a constant thickness, allow us to note the good agreement with what was theoretically highlighted.
- Published
- 2021
- Full Text
- View/download PDF
20. Effects of complex graphite-like carbon coating on gear vibration noise.
- Author
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Feng, Lajun, Wang, Zuoping, and Shen, Wenning
- Abstract
Highlights • Effect of substrate surface roughness on thickness uniformity of complex GLC coatings was studied. • Thickness uniformity of GLC coating was improved by the introduction of element Y. • The number of elements Y, Ce and Ta inserts were optimized to obtain uniform thickness distribution. • Vibration attenuation was obtained by depositing uniform complex GLC coating on the gear. Abstract In this paper, the effects of substrate surface roughness and the addition of yttrium, cerium and tantalum on thickness uniformity of graphite-like carbon (GLC) coatings on gears were studied by magnetron sputtering method using mosaic targets. And noise reduction effects of gear pump deposited with complex GLC coatings were evaluated at different rotate speeds. The results showed that target-substrate distance, sputtering angle and surface roughness had influences on thickness uniformity of GLC coatings on gear. The introduction of elements Y, Ce and Ta into GLC coatings could effectively improve their thickness uniformity. The complex GLC coating with optimal thickness uniformity on gear exhibited significantly reduction effect for gear noise and the reduction effect for axial vibration was better than that of radial vibrations. Compared with uncoated gears, the noise for the coated gears was decreased by 10 dB at 2000 rpm. Good high-frequency noise reduction was obtained, which could be decreased by 19 dB in the range of 4000–10,000 Hz. [ABSTRACT FROM AUTHOR]
- Published
- 2019
- Full Text
- View/download PDF
21. Thickness Uniformity Dependence on Polymer Viscosity in Silver-Nanowire-Embedded Flexible and Transparent Electrodes
- Author
-
Moonsoo Chae, Dongwook Ko, Yoohan Ma, Sungjin Jo, Dong Choon Hyun, Hyeon-Ju Oh, and Jongbok Kim
- Subjects
silver nanowire ,polymer viscosity ,embedding ,flexible electrode ,thickness uniformity ,Technology ,Engineering (General). Civil engineering (General) ,TA1-2040 ,Biology (General) ,QH301-705.5 ,Physics ,QC1-999 ,Chemistry ,QD1-999 - Abstract
We herein report the effect of the viscosity of a prepolymer solution on the thickness uniformity of silver-nanowire-embedded flexible transparent electrodes. We adopted a model system with all the prepolymer solutions possessing identical physical properties except for the viscosity and then explored the most common prepolymer solutions for silver-nanowire-embedded flexible electrodes. In all experiments, single-step spin coating was conducted to coat the prepolymer solution on silver nanowires. We found that the electrodes were thinner for lower viscosity. However, the thickness ratio between the center and edge was comparable (50−60%) and independent of the prepolymer solution viscosity. This indicates that the viscosity does not determine the thickness uniformity, and that the coating method itself is vital to obtain films with uniform thickness. The flexible electrodes were introduced into organic solar cells. Their device performance was comparable regardless of the position of the electrodes and their thickness. This is because the thickness difference of the flexible electrodes did not affect their transmittance significantly. Thus, we conclude that although different coating approaches are needed to obtain flexible electrodes with high uniformity, the performance of optoelectronic devices on silver-nanowire-embedded flexible electrodes is independent of them.
- Published
- 2020
- Full Text
- View/download PDF
22. Optimization of Tool Path Pitch of Spray Painting Robots for Automotive Painting Quality.
- Author
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Park, Kiyang and Jeon, Doyoung
- Abstract
The spray painting robots with mounted electrostatic rotating bell (ESRB) atomizers have been widely used to maintain high painting quality for various car models in rapid automotive production. The focus of this study is on developing the optimum coating path pitch while considering automobile painting quality. We define a deposition model optimized for the ESRB atomizer and introduce a method to optimize the path pitch with a cost function for painting thickness uniformity, which plays an important role in painting quality. In addition, experimental results are presented to verify the validity of the optimal path pitch simulation results. By using the results of this study, it is possible to improve the painting quality and thus the productivity of spray painting robots. [ABSTRACT FROM AUTHOR]
- Published
- 2018
- Full Text
- View/download PDF
23. Opening Through 200 mm Silicon Carbide Epitaxy
- Author
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Michaud, JF, Phung, LV, Alquier, D, Planson, D, Crippa, D, Azadmand, M, Mauceri, M, Preti, S, Puglisi, M, Vecchio, C, Crippa D., Azadmand M., Mauceri M., Preti S., Puglisi M., Vecchio C., Michaud, JF, Phung, LV, Alquier, D, Planson, D, Crippa, D, Azadmand, M, Mauceri, M, Preti, S, Puglisi, M, Vecchio, C, Crippa D., Azadmand M., Mauceri M., Preti S., Puglisi M., and Vecchio C.
- Abstract
In this paper, the performance of a new CVD reactor (called PE1O8) designed by LPE and developed in the European project REACTION to process uniform 4H-SiC homoepitaxy on 200 mm substrate is reported. Its tunable multi-zone injection system and new gas delivery configuration ensure the uniform gas distribution throughout the substrate. Excellent thickness and doping uniformity on 200 mm substrates are achieved with run-to-run variation less than 1.4% and 5.6% respectively.
- Published
- 2022
24. An effect of dummy cathode on thickness uniformity in electroforming process
- Author
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Chul-Woo Park and Kyoung-Yong Park
- Subjects
Electroforming ,Auxiliary electrode ,Current density ,Probe pin ,Thickness uniformity ,Physics ,QC1-999 - Abstract
This study examines the solution for one of the most difficult problems of electroforming process “thickness deviation”. As an effective solution, an auxiliary electrode (dummy cathode) is considered. Generally, the thickness of an edge plating area is almost twice the center area or greater. An auxiliary electrode (intentionally attached dummy cathode) has helped to achieve more uniform thickness of the electroformed-nickel layer by preventing excessive electric charge. In addition, computer-aided analysis was performed to determine the optimal condition of electroforming process and to confirm the experimental result.
- Published
- 2014
- Full Text
- View/download PDF
25. Synthesis and Characterization of Boron Thin Films Using Chemical and Physical Vapor Depositions
- Author
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Bart Schurink, Wesley T. E. van den Beld, Roald M. Tiggelaar, Robbert W. E. van de Kruijs, Fred Bijkerk, XUV Optics, and MESA+ Institute
- Subjects
inorganic chemicals ,Deposition rate ,UT-Gold-D ,technology, industry, and agriculture ,Thickness uniformity ,Intrinsic stress ,Surfaces and Interfaces ,CVD ,boron ,thin film ,PVD ,deposition rate ,thickness uniformity ,intrinsic stress ,chemical resistance ,Surfaces, Coatings and Films ,Materials Chemistry ,Thin film ,Chemical resistance ,Boron - Abstract
Boron as thin film material is of relevance for use in modern micro- and nano-fabrication technology. In this research boron thin films are realized by a number of physical and chemical deposition methods, including magnetron sputtering, electron-beam evaporation, plasma enhanced chemical vapor deposition (CVD), thermal/non-plasma CVD, remote plasma CVD and atmospheric pressure CVD. Various physical, mechanical and chemical characteristics of these boron thin films are investigated, i.e., deposition rate, uniformity, roughness, stress, composition, defectivity and chemical resistance. Boron films realized by plasma enhanced chemical vapor deposition (PECVD) are found to be inert for conventional wet chemical etchants and have the lowest amount of defects, which makes this the best candidate to be integrated into the micro-fabrication processes. By varying the deposition parameters in the PECVD process, the influences of plasma power, pressure and precursor inflow on the deposition rate and intrinsic stress are further explored. Utilization of PECVD boron films as hard mask for wet etching is demonstrated by means of patterning followed by selective structuring of the silicon substrate, which shows that PECVD boron thin films can be successfully applied for micro-fabrication.
- Published
- 2022
- Full Text
- View/download PDF
26. New precision electroforming process for the simultaneous improvement of thickness uniformity and microstructure homogeneity of wafer-scale nanotwinned copper arrays.
- Author
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Zhan, Xiaofei, Shen, Chunjian, Zhu, Zengwei, and Zhu, Di
- Subjects
- *
ELECTROFORMING , *COPPER , *HOMOGENEITY , *UNIFORMITY , *MICROSTRUCTURE - Abstract
Nanotwinned (nt) Cu has received much attention because of its superior mechanical and electrical properties, but only a few production processes can yield nt-Cu parts with uniform thickness and a homogeneous microstructure on the wafer scale. To solve this problem, a new precision electroforming process is proposed that combines auxiliary cathodes with pulse reverse current (PRC) electroforming, which provides a synergistic effect to increase the homogeneity of the thickness and a nanoscale twin structure. As a practical example of the proposed process, 4-inch nt-Cu lamina arrays were fabricated and numerically modeled to probe into the synergistic mechanisms. The intrinsic correlations among the array element spacing, current waveform, and main forms of thickness nonuniformity were determined. In addition, the effects of the processing parameters on the microstructural evolution and microhardness of the nt-Cu arrays were analyzed. The results indicated that such a significant improvement in thickness uniformity and microstructure homogeneity were due to the auxiliary-cathode/PRC combination, which enables maximization of the PRC leveling efficiency by inducing a uniform current distribution; this effectively ensures that the microstructures are uniform across all laminae on the wafer scale. Additionally, thick nt-Cu deposited on the current-crowding regions was preferentially stripped during the application of reverse current. This alleviates the adverse effects of the current redistribution resulting from the auxiliary cathode on the thickness uniformity of the laminae and offers additional possibilities for homogeneous growth of nt-Cu. The new precision electroforming process has significant potential to produce wafer-scale components with uniform thickness and specific microstructures. [Display omitted] • A new precision electroforming process based on the combination of auxiliary cathode and pulse reverse current is proposed. • The process can fabricate wafer-scale array components with uniform thickness and homogeneous microstructures. • Numerical simulation and experimental studies highlighted the synergistic mechanisms controlling the thickness and microstructure. • The process maximizes the leveling efficiency while minimizing the current-redistribution problems caused by the auxiliary cathode. • The relationship between processing parameters, thickness distribution, microstructure, and microhardness were established. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
27. A Study on Computational Fluid Dynamic Simulations to Improve the Thickness Uniformity of Porous Metal Films Deposited by Using Cluster Sputtering
- Author
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Kim, Jun Hyeong, Park, Se Yong, Lee, Hee Chul, Yun, Sung Ho, and Lee, Ho Nyun
- Published
- 2020
- Full Text
- View/download PDF
28. Towards Scalable Large-Area Pulsed Laser Deposition
- Author
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V. S. Klimin, Vladimir A. Smirnov, Z. E. Vakulov, Oleg A. Ageev, Alexander Mikhaylichenko, E. G. Zamburg, D. A. Khakhulin, and R. V. Tominov
- Subjects
Technology ,Fabrication ,Materials science ,Lithium niobate ,Substrate (electronics) ,ablation ,Article ,thickness uniformity ,Nanomaterials ,Pulsed laser deposition ,law.invention ,chemistry.chemical_compound ,law ,metal oxides ,computer simulation ,Deposition (phase transition) ,large-area deposition ,General Materials Science ,Thin film ,pulsed laser deposition ,nanomaterials ,Microscopy ,QC120-168.85 ,business.industry ,lithium niobate ,QH201-278.5 ,Laser ,Engineering (General). Civil engineering (General) ,TK1-9971 ,chemistry ,thin films ,Descriptive and experimental mechanics ,Optoelectronics ,Electrical engineering. Electronics. Nuclear engineering ,TA1-2040 ,business - Abstract
One of the significant limitations of the pulsed laser deposition method in the mass-production-technologies of micro- and nanoelectronic and molecular device electronic fabrication is the issue of ensuring deposition of films with uniform thickness on substrates with large diameter (more than 100 mm) since the area of the laser spot (1–5 mm2) on the surface of the ablated target is incommensurably smaller than the substrate area. This paper reports the methodology that allows to calculate the distribution profile of the film thickness over the surface substrate with a large diameter, taking into account the construction and technological parameters of the pulsed laser deposition equipment. Experimental verification of the proposed methodology showed that the discrepancy with the experiment does not exceed 8%. The modeling of various technological parameters influence on the thickness uniformity has been carried out. Based on the modeling results, recommendations and parameters are proposed for manufacturing uniform thickness films. The results allow for increasing the film thickness uniformity with the thickness distribution <, 5% accounts for ~ 31% of 300 mm diameter substrate.
- Published
- 2021
29. A technology to improve formability for rectangular cross section component hydroforming.
- Author
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Chu, G., Chen, G., Chen, B., and Yang, S.
- Subjects
- *
METAL fractures , *THICKNESS measurement , *METAL formability , *DEFORMATIONS (Mechanics) , *ELECTROMAGNETIC devices , *CROSS-sectional method - Abstract
In order to overcome difficulties in non-uniform thickness distribution and cracking failure during rectangular tube quasi-static hydroforming, a new forming technology, named as electromagnetically assisted hydroforming, is put forward. Both experiment and finite element method were conducted to investigate corner deformability and deformation pattern and its effect mechanisms. Results indicate that both corner deformability and thickness distribution are improved greatly under electromagnetic-assisted hydroforming. The reason is that deformation behavior changed after electromagnetic force application. As electromagnetic force is applied, tine petal cross sections are periodically produced and flattened. Thus, petal-like preform continues to generate and play a useful role in corner filling. Such deformation pattern overcomes friction holding back defect and results in stress state going over from tensile stress to compressive stress, which helps to avoid cracking failure and greatly improve thickness uniformity. At the same time, it also contributes to improve surface quality and decrease forming pressure simultaneously. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
30. Effects of Process Parameters on the Thickness Uniformity in Two-Point Incremental Forming (TPIF) with a Positive Die for an Irregular Stepped Part
- Author
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Zhiguo An, Lu Ou, Men Zhengxing, Shuqiang Zhou, and Zhengyuan Gao
- Subjects
0209 industrial biotechnology ,Materials science ,business.product_category ,formability ,two-point incremental forming ,chemistry.chemical_element ,02 engineering and technology ,Process variable ,process parameter ,lcsh:Technology ,Article ,thickness uniformity ,020901 industrial engineering & automation ,0203 mechanical engineering ,Aluminium ,Formability ,General Materials Science ,Point (geometry) ,Composite material ,lcsh:Microscopy ,lcsh:QC120-168.85 ,lcsh:QH201-278.5 ,lcsh:T ,Process (computing) ,irregular stepped part ,020303 mechanical engineering & transports ,chemistry ,lcsh:TA1-2040 ,Head (vessel) ,Die (manufacturing) ,lcsh:Descriptive and experimental mechanics ,lcsh:Electrical engineering. Electronics. Nuclear engineering ,business ,lcsh:Engineering (General). Civil engineering (General) ,lcsh:TK1-9971 ,Incremental sheet forming - Abstract
Incremental sheet forming (ISF) is a novel flexible forming technology with advantages, such as a low forming force, low-energy-consuming equipment, and good forming performance. The lack of available information about the formability of the two-point incremental forming (TPIF) process makes it limited for practical applications. Taking an irregular stepped part as the target part, the effects of process parameters on the thickness uniformity when using TPIF with a positive die for AA1060 aluminum alloy sheets were investigated. First, the set of optimal parameters regarding the diameter of the tool head, feed rate, and the step size were obtained through orthogonal experiments. Furthermore, the optimal parameter set of the number of forming passes, the direction of movement of the forming tool, and the forming angle was determined and the optimal forming result was numerically and experimentally verified. This demonstrated that the parameters affecting the thickness uniformity of the irregular stepped parts were, in descending order, the diameter of the forming tool, the feed rate, and the step size, with corresponding optimal values of 12 mm, 15,000 mm/min, and 0.4 mm, respectively. With an increase of the number of passes and a decrease of the forming angle between adjacent passes, and adopting an alternating clockwise and counterclockwise toolpath, the thickness uniformity of the formed parts was effectively improved.
- Published
- 2020
31. The Pamir Yaks of North Tajikistan: Specifics of Hide Formation
- Author
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Idiboy Sharipov, Ruslan Bobohojaev, Anvaridin Muhiddinov, Anatoly Popov, and Mikhail Sorochkin
- Subjects
0303 health sciences ,skin ,lcsh:TP368-456 ,030309 nutrition & dietetics ,Economics, Econometrics and Finance (miscellaneous) ,hide ,weight ,area ,04 agricultural and veterinary sciences ,thickness of skin ,040401 food science ,Industrial and Manufacturing Engineering ,thickness uniformity ,03 medical and health sciences ,lcsh:Food processing and manufacture ,0404 agricultural biotechnology ,yaks ,cattle ,chemical composition ,Food Science - Abstract
In all animals, the hide mass increases together with live body weight. At the age of 6 months and 3 years, the total weight of yak hide is almost two times higher than in other cattle. At 6 months, the thickness of yak hide in all topographical points exceeds that of cowhide by almost two times. By one and three years, the difference in the reference point disappears. However, the neck and the bellous hides of yak remain 25–40% thicker, and the skin area of other breeds of cattle exceeds that of yak at all ages by 35–40%. For the yaks of the Aininks Region, the optimal hide removal period is from birth to 3–4 years. For the animals over 4 years old, the hide yield by weight becomes relatively low. As far as thickness uniformity is concerned, the best skins for leather processing are those obtained from yaks under 3 years old, since they have the lowest degree of slackness. As for the chemical composition, the moisture of yak hide is 2.0–2.5% higher and the hide substance is 7.0–18.5% lower than in cowhide. This is, probably, connected with a certain reserve of water, or the so-called “depot moisture”, in the skin of the animal. For all age periods, the moisture of the bellous yak hides is lower and fat content is by 1.5–2.2% higher than in other topographical areas. Apparently, this is due to the thermal adaptation of animals to the habitat conditions.
- Published
- 2018
32. A correlation study of layer growth rate, thickness uniformity, stoichiometry, and hydrogen impurity level of ALD grown HfO2 thin films
- Author
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Blaschke, D., (0000-0003-2506-6869) Munnik, F., Grenzer, J., (0000-0002-8066-6392) Rebohle, L., (0000-0003-4756-5239) Zahn, P., Schmidt, H., (0000-0003-0455-1945) Gemming, S., Blaschke, D., (0000-0003-2506-6869) Munnik, F., Grenzer, J., (0000-0002-8066-6392) Rebohle, L., (0000-0003-4756-5239) Zahn, P., Schmidt, H., and (0000-0003-0455-1945) Gemming, S.
- Abstract
Hafnium oxide was deposited from tetrakis(dimethylamino)hafnium (TDMAHf) and water by atomic layer deposition (ALD) on heated 400 Si wafers covered with native oxide in the temperature range from 100 C to 350 C. Optimized self-limiting ALD reaction and smallest hydrogen impurity level have been realized for a substrate temperature of 300 C. The stoichiometry of deposited films and hydrogen impurity level were measured by elastic recoil detection analysis. The hafnium to oxygen ratio showed the expected 1:2 value. Besides hydrogen, no other impurities could be detected. Furthermore, a strong correlation between the growth rate per cycle (GPC), film uniformity and level of hydrogen impurities was observed. Based on this result, the easily accessible GPC can be used as a first indication for the hydrogen impurity level in ALD grown thin films. Furthermore, the characterization of the crystal structure showed the appearance of some crystallites in an amorphous matrix already for a growth temperature of 250 C and a pure crystalline layer at a growth temperature of 350 C. The increased crystallinity with increasing growth temperature was attributed to a higher seed concentration and a constant crystal size.
- Published
- 2020
33. An effect of dummy cathode on thickness uniformity in electroforming process.
- Author
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Park, Chul-Woo and Park, Kyoung-Yong
- Abstract
This study examines the solution for one of the most difficult problems of electroforming process “thickness deviation”. As an effective solution, an auxiliary electrode (dummy cathode) is considered. Generally, the thickness of an edge plating area is almost twice the center area or greater. An auxiliary electrode (intentionally attached dummy cathode) has helped to achieve more uniform thickness of the electroformed-nickel layer by preventing excessive electric charge. In addition, computer-aided analysis was performed to determine the optimal condition of electroforming process and to confirm the experimental result. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
34. Global variation and uniformity of eggshell thickness for chicken eggs.
- Author
-
Sun, C. J., Chen, S. R., Xu, G. Y., Liu, X. M., and Yang, N.
- Subjects
- *
EGG quality , *EGGSHELLS , *THICKNESS measurement , *AGRICULTURAL egg production , *STRENGTH of materials , *COEFFICIENTS (Statistics) - Abstract
Damaged eggshells result in losses of eggs. Numerous efforts have been carried out to improve eggshell quality, which may lead to increased eggshell thickness. The conventional way of enhancing eggshell strength with thicker eggshell on average may be replaced by a new strategy to improve eggshell uniformity without increasing eggshell thickness. To achieve this, it is necessary to investigate global variation of eggshell thickness. In this study, we used 100 fresh eggs from 52-wk-old layers of a commercial brown-egg variety. To determine the global variation of eggshell thickness, 42 points for each egg along both longitudinal and latitudinal axes were selected to measure thickness using an eggshell thickness gauge. The eggshell thickness from blunt to sharp end varied significantly (P < 0.05). The area surrounding the blunt end was the thinnest (0.341 ± 0.025 mm), whereas the area surrounding the sharp end was the thickest (0.367 ± 0.023 mm). It was found that the thickness of the sharp end was the closest to the average thickness of the whole eggshell and could be considered as a valid measurement of eggshell thickness. A new parameter, eggshell thickness uniformity, was defined as the reciprocal of the coefficient of variation (1/CV) of eggshell thickness from 42 points of each egg and can be used to evaluate the eggshell quality. Eggshell thickness uniformity was positively correlated with breaking strength (r = 0.341; P < 0.01), suggesting that the parameter may be used as a potential selection criterion in breeding program to improve eggshell quality without increasing eggshell thickness. [ABSTRACT FROM AUTHOR]
- Published
- 2012
- Full Text
- View/download PDF
35. Large-area uniform hydrogen-free diamond-like carbon films prepared by unbalanced magnetron sputtering for infrared anti-reflection coatings
- Author
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Xu, Junqi, Fan, Huiqing, Liu, Weiguo, and Hang, Lingxia
- Subjects
- *
COATING processes , *CARBON , *SPECTRUM analysis , *CORROSION & anti-corrosives - Abstract
Abstract: The hydrogen-free diamond-like carbon (DLC) films are potential materials to be used as infrared anti-reflection protective coatings if their optical absorption can be reduced to get relatively thick films needed. In this study, hydrogen-free DLC films were deposited by the physical vapor deposition (PVD) method in an unbalanced magnetron sputtering (UBMS) system with a rectangle graphite target of 440×80 mm in the argon atmosphere. The UBMS system was described in detail and the magnetron field distribution of the target was denoted in this work. The film thickness uniformity was investigated and the results showed that this system is capable of depositing uniform films larger than 150 mm in diameter. The infrared transmission spectra of DLC films were analyzed by a FTIR spectrometer, the results indicating that transparent films were obtained in the infrared region for the single side DLC coated on the silicon and germanium substrates, and about 68.83% and 63.05% transmittance were achieved respectively at the wave number of 2983 /cm, close to theoretical value for non-absorption carbon material. No obvious absorption peaks were found between 5000 and 800 /cm. The refractive index and extinction coefficient of the DLC films deposited under optimized conditions were about 2.08 and 0.067 respectively at the wavelength of 1600 nm. These important optical characteristics showed that the hydrogen-free DLC films prepared in the UBMS system were suitable for infrared transmission enhancement applications. [Copyright &y& Elsevier]
- Published
- 2008
- Full Text
- View/download PDF
36. Thickness uniformity measurements and damage threshold tests of large-area GaAs/AlGaAs crystalline coatings for precision interferometry
- Author
-
Koch, P., Cole, G.D., Deutsch, C., Follman, D., Heu, P., Kinley-Hanlon, M., Kirchhoff, R., Leavey, S., Lehmann, J., Oppermann, P., Rai, A.K., Tornasi, Z., Wöhler, J., Wu, D.S., Zederbauer, T., Lück, H., Koch, P., Cole, G.D., Deutsch, C., Follman, D., Heu, P., Kinley-Hanlon, M., Kirchhoff, R., Leavey, S., Lehmann, J., Oppermann, P., Rai, A.K., Tornasi, Z., Wöhler, J., Wu, D.S., Zederbauer, T., and Lück, H.
- Abstract
Precision interferometry is the leading method for extremely sensitive measurements in gravitational wave astronomy. Thermal noise of dielectric coatings poses a limitation to the sensitivity of these interferometers. To decrease coating thermal noise, new crystalline GaAs/AlGaAs multilayer mirrors have been developed. To date, the surface figure and thickness uniformity of these alternative low-loss coatings has not been investigated. Surface figure errors, for example, cause small angle scattering and thereby limit the sensitivity of an interferometer. Here we measure the surface figure of highly reflective, substrate-transferred, crystalline GaAs/AlGaAs coatings with a custom scanning reflectance system. We exploit the fact that the reflectivity varies with the thickness of the coating. To increase penetration into the coating, we used a 1550 nm laser on a highly reflective coating designed for a center wavelength of 1064 nm. The RMS thickness variation of a two inch optic was measured to be 0.41 ± 0.05 nm. This result is within 10% of the thickness uniformity, of 0.37 nm RMS, achieved with ion-beam sputtered coatings for the aLIGO detector. We additionally measured a lower limit of the laser induced damage threshold of 64 MW/cm2 for GaAs/AlGaAs coatings at a wavelength of 1064 nm. © 2019 Optical Society of America under the terms of the OSA Open Access Publishing Agreement
- Published
- 2019
37. Towards Scalable Large-Area Pulsed Laser Deposition.
- Author
-
Vakulov, Zakhar, Khakhulin, Daniil, Zamburg, Evgeny, Mikhaylichenko, Alexander, Smirnov, Vladimir A., Tominov, Roman, Klimin, Viktor S., and Ageev, Oleg A.
- Subjects
- *
PULSED laser deposition , *PULSED lasers , *MOTION picture distribution , *ELECTRONIC equipment , *LITHIUM niobate , *UNIFORMITY - Abstract
One of the significant limitations of the pulsed laser deposition method in the mass-production-technologies of micro- and nanoelectronic and molecular device electronic fabrication is the issue of ensuring deposition of films with uniform thickness on substrates with large diameter (more than 100 mm) since the area of the laser spot (1–5 mm2) on the surface of the ablated target is incommensurably smaller than the substrate area. This paper reports the methodology that allows to calculate the distribution profile of the film thickness over the surface substrate with a large diameter, taking into account the construction and technological parameters of the pulsed laser deposition equipment. Experimental verification of the proposed methodology showed that the discrepancy with the experiment does not exceed 8%. The modeling of various technological parameters influence on the thickness uniformity has been carried out. Based on the modeling results, recommendations and parameters are proposed for manufacturing uniform thickness films. The results allow for increasing the film thickness uniformity with the thickness distribution < 5% accounts for ~ 31% of 300 mm diameter substrate. [ABSTRACT FROM AUTHOR]
- Published
- 2021
- Full Text
- View/download PDF
38. Thickness uniformity measurements and damage threshold tests of large-area GaAs/AlGaAs crystalline coatings for precision interferometry
- Author
-
David Follman, Tobias Zederbauer, R. Kirchhoff, Garrett D. Cole, Harald Lück, Z. Tornasi, P. Oppermann, Patrick M. Koch, Paula Heu, C. Deutsch, J. Wöhler, M. Kinley-Hanlon, J. Lehmann, A. K. Rai, D. S. Wu, and S. Leavey
- Subjects
III-V semiconductors ,Thermal noise ,Materials science ,Sensitive measurement ,Reflection ,Dielectric ,Gravity waves ,engineering.material ,law.invention ,Gallium arsenide ,chemistry.chemical_compound ,Optics ,Reflective coatings ,Coating ,law ,Crystalline coatings ,Astronomical interferometer ,ddc:530 ,Semiconducting gallium ,Reflection coefficient ,Interferometers ,business.industry ,Thickness uniformity ,Small angle scattering ,Laser ,Atomic and Molecular Physics, and Optics ,Wavelength ,Interferometry ,chemistry ,Surface figure error ,Ion beams ,Laser induced damage thresholds ,Thickness variation ,engineering ,Highly reflective coatings ,Dewey Decimal Classification::500 | Naturwissenschaften::530 | Physik ,business ,Laser damage - Abstract
Precision interferometry is the leading method for extremely sensitive measurements in gravitational wave astronomy. Thermal noise of dielectric coatings poses a limitation to the sensitivity of these interferometers. To decrease coating thermal noise, new crystalline GaAs/AlGaAs multilayer mirrors have been developed. To date, the surface figure and thickness uniformity of these alternative low-loss coatings has not been investigated. Surface figure errors, for example, cause small angle scattering and thereby limit the sensitivity of an interferometer. Here we measure the surface figure of highly reflective, substrate-transferred, crystalline GaAs/AlGaAs coatings with a custom scanning reflectance system. We exploit the fact that the reflectivity varies with the thickness of the coating. To increase penetration into the coating, we used a 1550 nm laser on a highly reflective coating designed for a center wavelength of 1064 nm. The RMS thickness variation of a two inch optic was measured to be 0.41 ± 0.05 nm. This result is within 10% of the thickness uniformity, of 0.37 nm RMS, achieved with ion-beam sputtered coatings for the aLIGO detector. We additionally measured a lower limit of the laser induced damage threshold of 64 MW/cm2 for GaAs/AlGaAs coatings at a wavelength of 1064 nm. © 2019 Optical Society of America under the terms of the OSA Open Access Publishing Agreement
- Published
- 2019
39. Broad band anti-reflection 2-16μm coatings on diamond and ZnSe
- Author
-
Hakim Khalili, Mohammad and Endrino Armenteros, Jose
- Subjects
yttrium ,RF PVD sputtering ,diamond prism ,ytterbia ,infrared ,zinc selenide optics ,thickness uniformity ,Anti-reflective coatings - Abstract
In this project, Thin Metal Films an optical coating company is requiring the upgrade of a desktop research type radio frequency magnetron sputtering machine which was custom made for a European funded project and was gifted to it after the project completion. As the machine had no usage history, it had to be investigated and its capabilities and characteristics identified. The first part of the project, focused on restoring the machine using a systematic approach by utilising a technique called Plan Do Check Act, where a continuous feedback loop is used to identify problems and finding solution to them. Within the restoration process the aim was to improve the coating uniformity and machine’s repeatability. The restoration of the machine consumed almost the entire project duration leaving a little time for second part of the project. The second part was to use the restored machine, to develop single and multilayer Broad Band Anti-Reflective Coatings for Zinc Selenide and diamond optics. The optics are to be used in Attenuated Total Reflectance accessory units for Infrared spectroscopy. Based on the literature review and multiple decision criteria, yttria and ytterbia were showing promising results in adhering very well to a diamond surface and improving its transmission. Therefore, using Macleod software, a single layer quarter wavelength coating was designed and theoretically examined. It was found that a quarter wavelength ytteria at 5000 nm and a quarter wavelength ytterbia at 3370 nm can increase the transmission on both ZnSe and diamond optics to maximum of 98% and 95% accordingly. The coatings have not actually been deposited on the optics due to both targets breaking before conducting the actual experiments. PhD in Manufacturing
- Published
- 2018
40. Comparative study of soft thermal printing and lamination of dry thick photoresist films for the uniform fabrication of polymer MOEMS on small-sized samples
- Author
-
Emmanuelle Daran, Véronique Bardinal, Rémi Courson, Laurène Salvi, Thierry Camps, Jean-Baptiste Doucet, Benjamin Reig, Sami Abada, Équipe MICrosystèmes d'Analyse ( LAAS-MICA ), Laboratoire d'analyse et d'architecture des systèmes [Toulouse] ( LAAS ), Institut National Polytechnique [Toulouse] ( INP ) -Institut National des Sciences Appliquées - Toulouse ( INSA Toulouse ), Institut National des Sciences Appliquées ( INSA ) -Institut National des Sciences Appliquées ( INSA ) -Université Paul Sabatier - Toulouse 3 ( UPS ) -Centre National de la Recherche Scientifique ( CNRS ) -Institut National Polytechnique [Toulouse] ( INP ) -Institut National des Sciences Appliquées - Toulouse ( INSA Toulouse ), Institut National des Sciences Appliquées ( INSA ) -Institut National des Sciences Appliquées ( INSA ) -Université Paul Sabatier - Toulouse 3 ( UPS ) -Centre National de la Recherche Scientifique ( CNRS ), Service Techniques et Équipements Appliqués à la Microélectronique ( LAAS-TEAM ), Équipe MICrosystèmes d'Analyse (LAAS-MICA), Laboratoire d'analyse et d'architecture des systèmes (LAAS), Université Toulouse - Jean Jaurès (UT2J)-Université Toulouse 1 Capitole (UT1), Université Fédérale Toulouse Midi-Pyrénées-Université Fédérale Toulouse Midi-Pyrénées-Centre National de la Recherche Scientifique (CNRS)-Université Toulouse III - Paul Sabatier (UT3), Université Fédérale Toulouse Midi-Pyrénées-Institut National des Sciences Appliquées - Toulouse (INSA Toulouse), Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA)-Institut National Polytechnique (Toulouse) (Toulouse INP), Université Fédérale Toulouse Midi-Pyrénées-Université Toulouse - Jean Jaurès (UT2J)-Université Toulouse 1 Capitole (UT1), Université Fédérale Toulouse Midi-Pyrénées, Service Techniques et Équipements Appliqués à la Microélectronique (LAAS-TEAM), Université Toulouse Capitole (UT Capitole), Université de Toulouse (UT)-Université de Toulouse (UT)-Institut National des Sciences Appliquées - Toulouse (INSA Toulouse), Institut National des Sciences Appliquées (INSA)-Université de Toulouse (UT)-Institut National des Sciences Appliquées (INSA)-Université Toulouse - Jean Jaurès (UT2J), Université de Toulouse (UT)-Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Centre National de la Recherche Scientifique (CNRS)-Institut National Polytechnique (Toulouse) (Toulouse INP), Université de Toulouse (UT)-Université Toulouse Capitole (UT Capitole), and Université de Toulouse (UT)
- Subjects
Materials science ,Fabrication ,[ SPI.MAT ] Engineering Sciences [physics]/Materials ,02 engineering and technology ,01 natural sciences ,thickness uniformity ,law.invention ,[SPI.MAT]Engineering Sciences [physics]/Materials ,law ,Lamination ,lamination ,Electrical and Electronic Engineering ,Composite material ,[SPI.NANO]Engineering Sciences [physics]/Micro and nanotechnologies/Microelectronics ,Deposition (law) ,Thermal printing ,chemistry.chemical_classification ,Mechanical Engineering ,010401 analytical chemistry ,Epoxy ,Polymer ,021001 nanoscience & nanotechnology ,0104 chemical sciences ,Electronic, Optical and Magnetic Materials ,[SPI.TRON]Engineering Sciences [physics]/Electronics ,SU-8 ,[ SPI.TRON ] Engineering Sciences [physics]/Electronics ,MOEMS ,micro-optics ,Surface coating ,Resist ,chemistry ,Mechanics of Materials ,visual_art ,visual_art.visual_art_medium ,[SPI.OPTI]Engineering Sciences [physics]/Optics / Photonic ,dry thick resist film ,[ SPI.NANO ] Engineering Sciences [physics]/Micro and nanotechnologies/Microelectronics ,wafer-scale fabrication ,[ SPI.OPTI ] Engineering Sciences [physics]/Optics / Photonic ,0210 nano-technology - Abstract
International audience; A method called " soft thermal printing " (STP) was developed to ensure the optimal transfer of 50-µm-thick dry epoxy resist films (DF-1050) on small-sized samples. The aim was the uniform fabrication of high aspect ratio polymer-based MOEMS (micro-optical-electrical-mechanical system) on small and/or fragile samples, such as GaAs. The printing conditions were optimized, and the resulting thickness uniformity profiles were compared to those obtained via lamination and SU-8 standard spin-coating. Under the best conditions tested, STP and lamination produced similar results, with a maximum deviation to the central thickness of 3% along the sample surface, compared to greater than 40% for SU-8 spin-coating. Both methods were successfully applied to the collective fabrication of DF1050-based MOEMS designed for the dynamic focusing of VCSELs (vertical-cavity surface-emitting lasers). Similar, efficient electro-thermo-mechanical behaviour was obtained in both cases. 2
- Published
- 2017
- Full Text
- View/download PDF
41. Study of the influence of the pressure and rotational motion of 3D substrates processed by magnetron sputtering: A comparative study between Monte Carlo modelling and experiments
- Author
-
Stéphane Lucas, Martin Evrard, Aurélien Besnard, Centre de Recherche en Physique de la Matière et du Rayonnement [Namur] (PMR), Université de Namur [Namur] (UNamur), Laboratoire Bourguignon des Matériaux et Procédés (LABOMAP), Arts et Métiers Sciences et Technologies, HESAM Université (HESAM)-HESAM Université (HESAM), and The authors M. Evrard and S. Lucas gratefully acknowledge the financial support of the Walloon region under the FEDER and 3DCOATER-5: Convention N° 1610258, project 3215. The author A. Besnard also thanks the 'Région Bourgogne Franche-Comté' for the concession of the grant (Rech-Mobi-000026).
- Subjects
matière Condensée: Science des matériaux [Physique] ,Work (thermodynamics) ,Matériaux [Sciences de l'ingénieur] ,Materials science ,Monte Carlo method ,Substrate (electronics) ,01 natural sciences ,thickness uniformity ,[SPI.MAT]Engineering Sciences [physics]/Materials ,010309 optics ,motion ,0103 physical sciences ,Monte-carlo simulation ,Materials Chemistry ,Deposition (phase transition) ,[SPI.GPROC]Engineering Sciences [physics]/Chemical and Process Engineering ,010306 general physics ,Génie des procédés [Sciences de l'ingénieur] ,Rotation around a fixed axis ,Surfaces and Interfaces ,General Chemistry ,Mechanics ,Sputter deposition ,Condensed Matter Physics ,Pressure vessel ,Surfaces, Coatings and Films ,3D complex substrate ,macroscopic shadowing ,PVD ,[PHYS.COND.CM-MS]Physics [physics]/Condensed Matter [cond-mat]/Materials Science [cond-mat.mtrl-sci] ,Particle - Abstract
Over the last ten years, low pressure plasma solutions for materials surface treatment have been remarkable. Nevertheless, the deposition of films with a uniform thickness on 3D complex shapes is still a challenge for various deposition systems. In several cases, concavities and different substrate orientations and motions lead to macroscopic shadowing and affect the thickness uniformity. The objective of this work is to describe a modelling method able to predict the layer thickness on any surface of 3D substrates in motion and subject to vapour transported in a low pressure vessel. The meshing of objects with Delaunay-triangulation enables the modelling of complex shapes. The deposition process consists of several Monte Carlo simulations involving first the computing of the angular and energy particles distribution from the source, second their transport through the chamber and last the deposition on a meshed substrate. The algorithm is optimised with a “cell-list-linked-like” method and differs from existing models by the computation speed. The benchmarking between simulation and experimental results for Cr, Ag and Ta deposition at various pressures and on moving complex substrates with several shadowed faces is presented. Moreover, particle energy distribution will be discussed for each sample surface, mode and pressure. The authors M. Evrard and S. Lucas gratefully acknowledge the financial support of the Walloon region under the FEDER and 3DCOATER-5: Convention N° 1610258, project 3215. The author A. Besnard also thanks the “Région Bourgogne Franche-Comté” for the concession of the grant (Rech-Mobi-000026).
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- 2019
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42. Elastomeric microfluidic valve for active resin flow control within composite structure.
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He, Yongxi, Li, Yingguang, Ju, Kai, Wen, Youyi, Hao, Xiaozhong, Zhou, Jing, and Liu, Shuting
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COMPOSITE structures , *VALVES , *COMPOSITE numbers , *GUMS & resins - Abstract
• A concept of microfluidic valve is proposed for composite thickness uniformity control. • A self-adjusting elastomeric microfluidic valve is designed based on its self-structure of FRP composite. • The effectiveness of microfluidic valve is fully confirmed by real-time micro-flow monitoring. • The microfluidic valve exhibits self-adjusting, low-cost and easy-fabrication. Due to the existence of curvature, non-uniform pressure field forms within fiber reinforced polymer (FRP) composite during processing. Complex resin flow induces significant thickness deviation and defects concentration at corners. In this study, a microfluidic valve based on self-structure was proposed to restrict the mutual flow between regions for thickness uniformity control. Besides, little resin was actively guided to flow towards microfluidic valve, which helped avoid ply wrinkling, evacuate bubbles and enhance the surface quality of composite. By introducing an isolation film with a certain number of micropores on composite surface, the microfluidic valve formed naturally. Its microstructure adjusted self-adaptively to deviate local flow directions, and finally reverted to its initial states. This method allowed composite parts to be manufactured with uniform thickness (Maximum deviation of thickness: 0.01 mm), and without the need for extra hardware. [ABSTRACT FROM AUTHOR]
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- 2020
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43. Effects of Process Parameters on the Thickness Uniformity in Two-Point Incremental Forming (TPIF) with a Positive Die for an Irregular Stepped Part.
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Ou, Lu, An, Zhiguo, Gao, Zhengyuan, Zhou, Shuqiang, and Men, Zhengxing
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UNIFORMITY , *ALUMINUM sheets , *ALUMINUM alloys - Abstract
Incremental sheet forming (ISF) is a novel flexible forming technology with advantages, such as a low forming force, low-energy-consuming equipment, and good forming performance. The lack of available information about the formability of the two-point incremental forming (TPIF) process makes it limited for practical applications. Taking an irregular stepped part as the target part, the effects of process parameters on the thickness uniformity when using TPIF with a positive die for AA1060 aluminum alloy sheets were investigated. First, the set of optimal parameters regarding the diameter of the tool head, feed rate, and the step size were obtained through orthogonal experiments. Furthermore, the optimal parameter set of the number of forming passes, the direction of movement of the forming tool, and the forming angle was determined and the optimal forming result was numerically and experimentally verified. This demonstrated that the parameters affecting the thickness uniformity of the irregular stepped parts were, in descending order, the diameter of the forming tool, the feed rate, and the step size, with corresponding optimal values of 12 mm, 15,000 mm/min, and 0.4 mm, respectively. With an increase of the number of passes and a decrease of the forming angle between adjacent passes, and adopting an alternating clockwise and counterclockwise toolpath, the thickness uniformity of the formed parts was effectively improved. [ABSTRACT FROM AUTHOR]
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- 2020
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44. Highly uniform growth of 2-inch GaN wafers with a multi-wafer HVPE system
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Nanliu Liu, Jiejun Wu, Guoyi Zhang, Li Wenhui, Tong Yuzhen, and Luo Ruihong
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Materials science ,business.industry ,Multi-wafer ,Thickness uniformity ,Mass production ,Nanotechnology ,Condensed Matter Physics ,Epitaxy ,A3. HVPE ,GaN ,Volumetric flow rate ,Inorganic Chemistry ,Crystal ,Full width at half maximum ,Materials Chemistry ,Surface roughness ,Optoelectronics ,Deposition (phase transition) ,Wafer ,business ,Layer (electronics) - Abstract
A new nozzle structure was developed in an improved multi-wafer hybrid vapor phase epitaxy (IHVPE) system by adding an inner dilution gas (ID) pipe between V and III groups gas channels. Experimental results showed that the thickness distribution of 2-inch GaN layer depended strongly on the flow rate of ID gas. The uniformity of film can arrive at ±3–4% by optimizing ID gas, which was better than that of ±30% grown in the old conventional multi-wafer hybrid vapor phase epitaxy (CHVPE) system. Meanwhile, the crystal quality and surface morphology were also greatly improved for GaN film by using the new reactor structure. The FWHM values of (002) and (102) were reduced from 342″ and 806″ to 207″ and 254″, respectively. AFM result of surface roughness (RMS, 10 μm×10 μm) of GaN layer was also lowered from 1.226 nm to 0.798 nm. It was partly because of the suppression of parasitic polycrystalline deposition due to the ID gas. This simple and economic method could provide an effective solution to simultaneously fabricate multiple GaN wafer with good thickness uniformity, high crystal quality and low cost.
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- 2014
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45. Double slot high-k waveguide grating couplers for silicon photonics
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Naiini, Maziar M., Henkel, Christoph, Malm, Gunnar B., Östling, Mikael, Naiini, Maziar M., Henkel, Christoph, Malm, Gunnar B., and Östling, Mikael
- Abstract
Novel on-chip double slot high-k waveguide grating couplers have been successfully fabricated, and characterized. Silicon cannot yet be directly used for light generation and modulation in photonic devices because of its weak nonlinear optical effects. Slot waveguide is a solution to this problem, this structure consists of silicon and low refractive index material layers as the active material[1, 2]. Previously, grating couplers were demonstrated for horizontal single slot SiO 2 waveguides [3, 4]. Double slot waveguide is of great interest since the confinement of the optical power in the active material is significantly larger. Atomic layer deposited (ALD) high-k aluminum oxide (Al 2O 3) was used as the slot layer because of a superior layer quality and thickness uniformity. The ultimate goal of this work is the demonstration of the highly reproducible on-chip photonic devices., QC 20121121
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- 2012
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46. The influence of conditions of forming composite coating polymer-magnetic powder on physico-mechanical properties of telecommunication optical fibers
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Milutinović-Nikolić, Aleksandra D., Aleksić, Radoslav, Jeremić, Katarina, Srećković, Milesa, Talijan, Nadežda, and Uskoković, Petar
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optical fiber ,magnetic detection ,SmCо5 ,mаgnеtnо lоcirаnjе ,Ba-ferrite ,coating ,kоmpоzitnа prеvlаkа ,composite coating ,mechanical properties ,thickness uniformity ,viskоznоst ,Bа-fеrit ,prеvlаčеnjе ,numеričkа simulаciја ,SmCo5 ,mеhаničkа svојstvа ,numerical simulation ,viscosity ,rаvnоmеrnоst dеblјinе ,optičkо vlаknо - Abstract
Fеrоmаgnеtskа kоmpоzitnа prеvlаkа nа оptičkоm vlаknu оmоgućаvа idеntifikаciјu i dеtеkciјu tеlеkоmunikаciоnih оptičkih vlаkаnа/kаblоvа nаkоn njihоvоg pоlаgаnjа, primеnоm stаndаrdnih mаgnеtskih mеtоdа. U оvоm rаdu su dоbiјаnа оptičkа vlаknа sа kоmpоzitnоm fеrоmаgnеtskоm prеvlаkоm. Dеfinisаn је i оptimizоvаn prоcеsа njihоvоg dоbiјаnjа i vršеnа njеgоvа numеričkа simulаciја. Kоmpоzitnа prеvlаkа fоrmirаnа је prеvlаčеnjеm оptičkih vlаkаnа dispеrziјоm prаhоvа Bа-fеritа i SmCo5 u rаstvоru ЕVA u tоluеnu. Rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе ispitivаnа је kоrišćеnjеm mikrоskоpа sа оdbiјеnоm svеtlоšću. Аnаlizа mikrоskоpskih slikа bilа је оmоgućеnа kоrišćеnjеm sistеmа: mikrоskоp- digitаlnа kаmеrа- pеrsоnаlni rаčunаr sа оdgоvаrајućim prоgrаmоm zа kvаntifikаciјu vizuеlnih infоrmаciја. Rеzultаti dоbiјеni аnаlizоm slikе оbrаđеni su mаtеmаtičkо-stаtističkоm mеtоdоm. Ispitаn је uticај brzinе prеvlаčеnjа, kоncеntrаciје pоlimеrа i mаgnеtnоg prаhа u dispеrziјi nа rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе pоlimеr mаgnеtni prаh. Kао kritеriјum zа dеfinisаnjе unifоrmnе dеblјinе kоmpоzitnе prеvlаkе usvојеnа је nајmаnjа vrеdnоst stаndаrdnе dеviјаciје nајvеrоvаtniје vrеdnоsti prеčnikа оptičkоg vlаknа sа kоmpоzitnоm prеvlаkоm. Nа оsnоvu еkspеrimеntаlnih rеzultаtа, utvrđеnо је dа sе uticај svih istrаživаnih prоcеsnih pаrаmеtаrа nа rаvnоmеrnоst prеvlаkе, mоžе svеsti nа uticај viskоznоsti dispеrziје kојоm sе vrši prеvlаčеnjе. Ustаnоvlјеnа је оptimаlnа vrеdnоst viskоznоsti dispеrziје оd 1,20-1,24 Pas, zа ispitаni sistеm, kоја оmоgućаvа fоrmirаnjе kоmpоzitnе prеvlаkе nајrаvnоmеrniје dеblјinе. Pоtvrđеnо је dа svе prоcеsnе pаrаmеtrе: kоncеntrаciјu pоlimеrа i mаgnеtnоg prаhа, brzinu i tеmpеrаturu prеvlаčеnjа trеbа usklаditi tаkо dа sе prеvlаčеnjе оdviја dispеrziјоm čiја је viskоznоst оptimаlnа. Nа оsnоvu еkspеrimеntаlnо utvrđеnih rеоlоških јеdnаčinа zа pоnаšаnjе dispеrznоg sistеmа (prаhоvi Bа-fеritа ili SmCo5 dispеrgоvаni u rаstvоru ЕVА u tоluеnu) i pоstојеćеg mаtеmаtičkоg mоdеlа zа prеvlаčеnjе оptičkih vlаkаnа pоlimеrnоm prеvlаkоm rаzviјеn је mаtеmаtički mоdеl fоrmirаnjа kоmpоzitnе prеvlаkе nа оptičkоm vlаknu kојi је оmоgućiо numеričku simulаciјu prоcеsа prеvlаčеnjа оptičkih vlаkаnа kоmpоzitnоm prеvlаkоm. Numеričkоm simulаciјоm оmоgućеnо је ispitivаnjе uticаја vеćеg brоја prоcеsnih pаrаmеtаrа i оnih kојi nisu bili еkspеrimеntаlnо ispitivаni. Utvrđеnо је dа dеblјinа prеvlаkе nајvišе zаvisi оd gеоmеtriјskih kаrаktеristikа sistеmа zа prеvlаčеnjе. Vаlidnоst mоdеlа pоtvrđеnа је dоbrim slаgаnjеm rеzultаtа numеričkе simulаciје sа еkspеrimеntаlnim. Dоbiјеnа оptičkа vlаkаnа sа kоmpоzitnоm prеvlаkоm zаdržаvајu trаnsmisiоnа i pоbоlјšаvајu mеhаničkа svојstvа. Pri dејstvu spоlјаšnjеg јеdnоsmеrnоg i nаizmеničnоg mаgnеtnоg pоlја nа оptičkо vlаknо sа fеrоmеgnеtskоm kоmpоzitnоm prеvlаkоm nе dоlаzi dо prоmеnе u snаzi prеnеsеnе svеtlоsti. Ispitаnа оptičkа vlаknа mоgućе је kоristiti kао tеlеkоmunikаciоnа оptičkа vlаknа kоја sе mоgu lоcirаti kоrišćеnjеm mаgnеtnih mеtоdа. The ferromagnetic composite coating on optical fiber enables identification and detection of telecommunication optical fibers/cables after they have been laid down, using standard magnetic methods. In this thesis the optical fibers with composite ferromagnetic coating were obtained. The process of their synthesis was defined and optimized and numerical simulation of this process was performed. The composite coating was formed by coating optical fibers with dispersion of Ba-ferrite and SmCo5 powders in EVA solution in toluene. The coating thickness uniformity was investigated using optical microscope with reflective light. The analysis of microscope images was performed using the system: microscope - digital camera- personal computer with appropriate software for quantification of visual information. These results were evaluated using mathematical-statistic methods. The influence of coating rate, concentration of polymer and magnetic powder in dispersion on polymer-magnetic powder composite coating thickness was investigated. As criteria for defining uniform thickness of composite coating the minimal value of standard deviation of mean value of diameter of optical fiber with composite coating was established. According to experimental results it was found out that the influence of all investigated process parameters on coating uniformity ends up as the influence of viscosity of coating dispersion. For investigated system, the optimal value of viscosity of dispersion that enables forming the composite coating of the most uniform thickness was established as 1.20-1.24 Pa s. It was confirmed that all process parameters: concentration of polymer and magnetic powder and coating rate and temperature should be established in that manner that coating is performed with the evaluated optimal viscosity of dispersion. According to the experimentally estimated rheological equation for behavior of dispersed system (powders of Ba-ferrite and SmCo5 dispersed in EVA solution in toluene) and existing mathematical model for coating optical fibers with polymer coating the mathematical model of forming composite coating on optical fiber was established and enabled the numerical simulation of process of coating optical fibers with composite coating. By using numerical simulation it was possible to investigate higher number of process parameters and those that were not experimentally investigated. It was established that the coating thickness mostly depends on geometrical properties of the coating system. Validity of model was confirmed by good agreement of results obtained with numerical simulation with experimental. The obtained optical fibers with composite coating keep their transmission properties and improve mechanical. No change in the power of the propagated laser beam through the fiber optic with composite ferromagnetic coating was observed when external DC and AC magnetic fields were applied. It is possible to use the developed optical fibers as telecommunication optical fibers detectable by magnetic methods.
- Published
- 2001
47. Uticaj uslova formiranja kompozitne prevlake polimer-magnetni prah na fizičko-mehanička svojstva telekomunikacionih optičkih vlakana
- Author
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Milutinović Nikolić, Aleksandra, Aleksić, Radoslav, Jeremić, Katarina B., Srećković, Milesa, Talijan, Nadežda M., and Uskoković, Petar S.
- Subjects
optical fiber ,magnetic detection ,SmCо5 ,mаgnеtnо lоcirаnjе ,Ba-ferrite ,coating ,kоmpоzitnа prеvlаkа ,composite coating ,mechanical properties ,thickness uniformity ,viskоznоst ,Bа-fеrit ,prеvlаčеnjе ,numеričkа simulаciја ,SmCo5 ,mеhаničkа svојstvа ,numerical simulation ,viscosity ,rаvnоmеrnоst dеblјinе ,optičkо vlаknо - Abstract
Fеrоmаgnеtskа kоmpоzitnа prеvlаkа nа оptičkоm vlаknu оmоgućаvа idеntifikаciјu i dеtеkciјu tеlеkоmunikаciоnih оptičkih vlаkаnа/kаblоvа nаkоn njihоvоg pоlаgаnjа, primеnоm stаndаrdnih mаgnеtskih mеtоdа. U оvоm rаdu su dоbiјаnа оptičkа vlаknа sа kоmpоzitnоm fеrоmаgnеtskоm prеvlаkоm. Dеfinisаn је i оptimizоvаn prоcеsа njihоvоg dоbiјаnjа i vršеnа njеgоvа numеričkа simulаciја. Kоmpоzitnа prеvlаkа fоrmirаnа је prеvlаčеnjеm оptičkih vlаkаnа dispеrziјоm prаhоvа Bа-fеritа i SmCo5 u rаstvоru ЕVA u tоluеnu. Rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе ispitivаnа је kоrišćеnjеm mikrоskоpа sа оdbiјеnоm svеtlоšću. Аnаlizа mikrоskоpskih slikа bilа је оmоgućеnа kоrišćеnjеm sistеmа: mikrоskоp- digitаlnа kаmеrа- pеrsоnаlni rаčunаr sа оdgоvаrајućim prоgrаmоm zа kvаntifikаciјu vizuеlnih infоrmаciја. Rеzultаti dоbiјеni аnаlizоm slikе оbrаđеni su mаtеmаtičkо-stаtističkоm mеtоdоm. Ispitаn је uticај brzinе prеvlаčеnjа, kоncеntrаciје pоlimеrа i mаgnеtnоg prаhа u dispеrziјi nа rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе pоlimеr mаgnеtni prаh. Kао kritеriјum zа dеfinisаnjе unifоrmnе dеblјinе kоmpоzitnе prеvlаkе usvојеnа је nајmаnjа vrеdnоst stаndаrdnе dеviјаciје nајvеrоvаtniје vrеdnоsti prеčnikа оptičkоg vlаknа sа kоmpоzitnоm prеvlаkоm. Nа оsnоvu еkspеrimеntаlnih rеzultаtа, utvrđеnо је dа sе uticај svih istrаživаnih prоcеsnih pаrаmеtаrа nа rаvnоmеrnоst prеvlаkе, mоžе svеsti nа uticај viskоznоsti dispеrziје kојоm sе vrši prеvlаčеnjе. Ustаnоvlјеnа је оptimаlnа vrеdnоst viskоznоsti dispеrziје оd 1,20-1,24 Pas, zа ispitаni sistеm, kоја оmоgućаvа fоrmirаnjе kоmpоzitnе prеvlаkе nајrаvnоmеrniје dеblјinе. Pоtvrđеnо је dа svе prоcеsnе pаrаmеtrе: kоncеntrаciјu pоlimеrа i mаgnеtnоg prаhа, brzinu i tеmpеrаturu prеvlаčеnjа trеbа usklаditi tаkо dа sе prеvlаčеnjе оdviја dispеrziјоm čiја је viskоznоst оptimаlnа. Nа оsnоvu еkspеrimеntаlnо utvrđеnih rеоlоških јеdnаčinа zа pоnаšаnjе dispеrznоg sistеmа (prаhоvi Bа-fеritа ili SmCo5 dispеrgоvаni u rаstvоru ЕVА u tоluеnu) i pоstојеćеg mаtеmаtičkоg mоdеlа zа prеvlаčеnjе оptičkih vlаkаnа pоlimеrnоm prеvlаkоm rаzviјеn је mаtеmаtički mоdеl fоrmirаnjа kоmpоzitnе prеvlаkе nа оptičkоm vlаknu kојi је оmоgućiо numеričku simulаciјu prоcеsа prеvlаčеnjа оptičkih vlаkаnа kоmpоzitnоm prеvlаkоm. Numеričkоm simulаciјоm оmоgućеnо је ispitivаnjе uticаја vеćеg brоја prоcеsnih pаrаmеtаrа i оnih kојi nisu bili еkspеrimеntаlnо ispitivаni. Utvrđеnо је dа dеblјinа prеvlаkе nајvišе zаvisi оd gеоmеtriјskih kаrаktеristikа sistеmа zа prеvlаčеnjе. Vаlidnоst mоdеlа pоtvrđеnа је dоbrim slаgаnjеm rеzultаtа numеričkе simulаciје sа еkspеrimеntаlnim. Dоbiјеnа оptičkа vlаkаnа sа kоmpоzitnоm prеvlаkоm zаdržаvајu trаnsmisiоnа i pоbоlјšаvајu mеhаničkа svојstvа. Pri dејstvu spоlјаšnjеg јеdnоsmеrnоg i nаizmеničnоg mаgnеtnоg pоlја nа оptičkо vlаknо sа fеrоmеgnеtskоm kоmpоzitnоm prеvlаkоm nе dоlаzi dо prоmеnе u snаzi prеnеsеnе svеtlоsti. Ispitаnа оptičkа vlаknа mоgućе је kоristiti kао tеlеkоmunikаciоnа оptičkа vlаknа kоја sе mоgu lоcirаti kоrišćеnjеm mаgnеtnih mеtоdа. The ferromagnetic composite coating on optical fiber enables identification and detection of telecommunication optical fibers/cables after they have been laid down, using standard magnetic methods. In this thesis the optical fibers with composite ferromagnetic coating were obtained. The process of their synthesis was defined and optimized and numerical simulation of this process was performed. The composite coating was formed by coating optical fibers with dispersion of Ba-ferrite and SmCo5 powders in EVA solution in toluene. The coating thickness uniformity was investigated using optical microscope with reflective light. The analysis of microscope images was performed using the system: microscope - digital camera- personal computer with appropriate software for quantification of visual information. These results were evaluated using mathematical-statistic methods. The influence of coating rate, concentration of polymer and magnetic powder in dispersion on polymer-magnetic powder composite coating thickness was investigated. As criteria for defining uniform thickness of composite coating the minimal value of standard deviation of mean value of diameter of optical fiber with composite coating was established. According to experimental results it was found out that the influence of all investigated process parameters on coating uniformity ends up as the influence of viscosity of coating dispersion. For investigated system, the optimal value of viscosity of dispersion that enables forming the composite coating of the most uniform thickness was established as 1.20-1.24 Pa s. It was confirmed that all process parameters: concentration of polymer and magnetic powder and coating rate and temperature should be established in that manner that coating is performed with the evaluated optimal viscosity of dispersion. According to the experimentally estimated rheological equation for behavior of dispersed system (powders of Ba-ferrite and SmCo5 dispersed in EVA solution in toluene) and existing mathematical model for coating optical fibers with polymer coating the mathematical model of forming composite coating on optical fiber was established and enabled the numerical simulation of process of coating optical fibers with composite coating. By using numerical simulation it was possible to investigate higher number of process parameters and those that were not experimentally investigated. It was established that the coating thickness mostly depends on geometrical properties of the coating system. Validity of model was confirmed by good agreement of results obtained with numerical simulation with experimental. The obtained optical fibers with composite coating keep their transmission properties and improve mechanical. No change in the power of the propagated laser beam through the fiber optic with composite ferromagnetic coating was observed when external DC and AC magnetic fields were applied. It is possible to use the developed optical fibers as telecommunication optical fibers detectable by magnetic methods.
- Published
- 2001
48. Uticaj uslova formiranja kompozitne prevlake polimer-magnetni prah na fizičko-mehanička svojstva telekomunikacionih optičkih vlakana
- Author
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Aleksić, Radoslav, Jeremić, Katarina B., Srećković, Milesa, Talijan, Nadežda M., Uskoković, Petar S., Milutinović Nikolić, Aleksandra, Aleksić, Radoslav, Jeremić, Katarina B., Srećković, Milesa, Talijan, Nadežda M., Uskoković, Petar S., and Milutinović Nikolić, Aleksandra
- Abstract
Fеrоmаgnеtskа kоmpоzitnа prеvlаkа nа оptičkоm vlаknu оmоgućаvа idеntifikаciјu i dеtеkciјu tеlеkоmunikаciоnih оptičkih vlаkаnа/kаblоvа nаkоn njihоvоg pоlаgаnjа, primеnоm stаndаrdnih mаgnеtskih mеtоdа. U оvоm rаdu su dоbiјаnа оptičkа vlаknа sа kоmpоzitnоm fеrоmаgnеtskоm prеvlаkоm. Dеfinisаn је i оptimizоvаn prоcеsа njihоvоg dоbiјаnjа i vršеnа njеgоvа numеričkа simulаciја. Kоmpоzitnа prеvlаkа fоrmirаnа је prеvlаčеnjеm оptičkih vlаkаnа dispеrziјоm prаhоvа Bа-fеritа i SmCo5 u rаstvоru ЕVA u tоluеnu. Rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе ispitivаnа је kоrišćеnjеm mikrоskоpа sа оdbiјеnоm svеtlоšću. Аnаlizа mikrоskоpskih slikа bilа је оmоgućеnа kоrišćеnjеm sistеmа: mikrоskоp- digitаlnа kаmеrа- pеrsоnаlni rаčunаr sа оdgоvаrајućim prоgrаmоm zа kvаntifikаciјu vizuеlnih infоrmаciја. Rеzultаti dоbiјеni аnаlizоm slikе оbrаđеni su mаtеmаtičkо-stаtističkоm mеtоdоm. Ispitаn је uticај brzinе prеvlаčеnjа, kоncеntrаciје pоlimеrа i mаgnеtnоg prаhа u dispеrziјi nа rаvnоmеrnоst dеblјinе kоmpоzitnе prеvlаkе pоlimеr mаgnеtni prаh. Kао kritеriјum zа dеfinisаnjе unifоrmnе dеblјinе kоmpоzitnе prеvlаkе usvојеnа је nајmаnjа vrеdnоst stаndаrdnе dеviјаciје nајvеrоvаtniје vrеdnоsti prеčnikа оptičkоg vlаknа sа kоmpоzitnоm prеvlаkоm. Nа оsnоvu еkspеrimеntаlnih rеzultаtа, utvrđеnо је dа sе uticај svih istrаživаnih prоcеsnih pаrаmеtаrа nа rаvnоmеrnоst prеvlаkе, mоžе svеsti nа uticај viskоznоsti dispеrziје kојоm sе vrši prеvlаčеnjе. Ustаnоvlјеnа је оptimаlnа vrеdnоst viskоznоsti dispеrziје оd 1,20-1,24 Pas, zа ispitаni sistеm, kоја оmоgućаvа fоrmirаnjе kоmpоzitnе prеvlаkе nајrаvnоmеrniје dеblјinе. Pоtvrđеnо је dа svе prоcеsnе pаrаmеtrе: kоncеntrаciјu pоlimеrа i mаgnеtnоg prаhа, brzinu i tеmpеrаturu prеvlаčеnjа trеbа usklаditi tаkо dа sе prеvlаčеnjе оdviја dispеrziјоm čiја је viskоznоst оptimаlnа. Nа оsnоvu еkspеrimеntаlnо utvrđеnih rеоlоških јеdnаčinа zа pоnаšаnjе dispеrznоg sistеmа (prаhоvi Bа-fеritа ili SmCo5 dispеrgоvаni u rаstvоru ЕVА u tоluеnu) i pоstојеćеg mаtеmаtičkоg mоdеlа zа prеvlаčеnjе оp, The ferromagnetic composite coating on optical fiber enables identification and detection of telecommunication optical fibers/cables after they have been laid down, using standard magnetic methods. In this thesis the optical fibers with composite ferromagnetic coating were obtained. The process of their synthesis was defined and optimized and numerical simulation of this process was performed. The composite coating was formed by coating optical fibers with dispersion of Ba-ferrite and SmCo5 powders in EVA solution in toluene. The coating thickness uniformity was investigated using optical microscope with reflective light. The analysis of microscope images was performed using the system: microscope - digital camera- personal computer with appropriate software for quantification of visual information. These results were evaluated using mathematical-statistic methods. The influence of coating rate, concentration of polymer and magnetic powder in dispersion on polymer-magnetic powder composite coating thickness was investigated. As criteria for defining uniform thickness of composite coating the minimal value of standard deviation of mean value of diameter of optical fiber with composite coating was established. According to experimental results it was found out that the influence of all investigated process parameters on coating uniformity ends up as the influence of viscosity of coating dispersion. For investigated system, the optimal value of viscosity of dispersion that enables forming the composite coating of the most uniform thickness was established as 1.20-1.24 Pa s. It was confirmed that all process parameters: concentration of polymer and magnetic powder and coating rate and temperature should be established in that manner that coating is performed with the evaluated optimal viscosity of dispersion. According to the experimentally estimated rheological equation for behavior of dispersed system (powders of Ba-ferrite and SmCo5 dispersed in EVA solution in tolue
- Published
- 2001
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