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1. Concise construction of novel bridged bicyclic lactams by sequenced Ugi/RCM/Heck reactions.

Author

Ribelin TP, Judd AS, Akritopoulou-Zanze I, Henry RF, Cross JL, Whittern DN, and Djuric SW

Subjects
Crystallography, X-Ray, Cyclization, Lactams chemistry, Models, Molecular, Molecular Structure, Stereoisomerism, Lactams chemical synthesis
Abstract

Herein we report a concise protocol for the diastereoselective synthesis of novel bridged bicyclic lactams from commercially available components by the sequence of Ugi, ring-closing metathesis (RCM), and Heck reactions. X-ray diffraction studies revealed that the bicyclic products contain varying degrees of pyramidalization of the bridgehead nitrogen atom.

Published
2007
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