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1. A continuous flow investigation of sulfonyl chloride synthesis using N-chloroamides: optimization, kinetics and mechanism

Author

Dominik Polterauer, Dominique M. Roberge, Paul Hanselmann, Ryan Littich, Christopher A. Hone, and C. Oliver Kappe

Subjects
Fluid Flow and Transfer Processes, Chemistry (miscellaneous), Process Chemistry and Technology, Chemical Engineering (miscellaneous), Catalysis
Abstract

We develop a continuous flow protocol for the synthesis of sulfonyl chlorides from disulfides and thiols, using 1,3-dichloro-5,5-dimethylhydantoin (DCH) as a dual-function reagent for oxidative chlorination.

Published
2022
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