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1. Assembly of Indoline-2-carboxylate-Embodied Dipeptidesvia Pd-Catalyzed C(sp2)–H Bond Direct Functionalization.

Author

He, Yu-Peng, Zhang, Chao, Fan, Mengyang, Wu, Zhijie, and Ma, Dawei

Subjects
*INDOLINE, *CARBOXYLATES, *DIPEPTIDES, *PALLADIUM catalysts, *CARBON-hydrogen bonds, *DEHYDROGENATION
Abstract

Intramolecular dehydrogenative cyclizationof 2-methoxyiminoacyl-protectedphenylalanine derivatives proceeded at 110 °C under catalysisof Pd(OAc)2in the presence of 1-fluoro-2,4,6-trimethylpyridiniumtetrafluoroborate to afford substituted indoline-2-carboxylates thatwere converted into indoline-2-carboxylate-embodied dipeptides viaRaney Ni-catalyzed hydrogenation. [ABSTRACT FROM AUTHOR]

Published
2015
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