25 results on '"Wu, K."'
Search Results
2. Processing, Microstructure and Mechanical Properties of Ti6Al4V Particles-Reinforced Mg Matrix Composites
- Author
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Wang, X. M., Wang, X. J., Hu, X. S., Wu, K., and Zheng, M. Y.
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- 2016
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3. The Development of Steel Band Feeding for HSLA Heavy Plates
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Isayev, O., Hress, O., Hu, C. Y., Xin, R., and Wu, K. M.
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- 2016
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4. Magnesium matrix composite reinforced by nanoparticles – A review.
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Nie, K.B., Wang, X.J., Deng, K.K., Hu, X.S., and Wu, K.
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MAGNESIUM ,METAL nanoparticles ,NANOPARTICLES ,NANOPARTICLE size - Abstract
Significant progress has been made in magnesium-based composites during recent decades, especially for the appearance of magnesium matrix composite reinforced by nanoparticles. The nanoparticles added not only exhibit a good strengthening effect, but also maintain the initial toughness of the matrix, effectively balancing the contradiction between the strength and plasticity in the traditional magnesium matrix composites. The magnesium matrix nanocomposites with excellent mechanical properties have pushed the development of magnesium matrix composites to a new stage. However, it is very difficult to disperse the nanoparticles in metal melt especially in magnesium melt which is different from other metal melts and dangerous during the cast processing. This means that the preparation of magnesium matrix nanocomposite is extremely challenging. Further, the magnesium matrix nanocomposites possess a distinctive characteristic in deformation behavior, strengthening and toughening mechanism due to their special size effect of nanoparticles. Accordingly, this review will focus on the new preparation technologies, deformation behavior, mechanical properties and strengthening and toughening mechanisms. The potential applications, development trends and future research ideas of magnesium matrix nanocomposite are also prospected. [ABSTRACT FROM AUTHOR]
- Published
- 2021
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5. Microstructure and mechanical properties of spark plasma sintered titanium‐added copper/reduced graphene oxide composites.
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Zhang, X., Wu, K., Liu, X., Ge, X., and Yang, W.
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GRAPHENE oxide , *TITANIUM powder , *COPPER , *MICROSTRUCTURE , *SOLID solutions , *COMPRESSIVE strength - Abstract
Copper matrix composites were fabricated through mixing fixed amount of reduced graphene oxide and the different amounts of titanium. The dried copper/titanium/reduced graphene oxide mixture powders were firstly obtained by the wet‐mixing process, and then the spark plasma sintering process realized their faster densification. In the as‐sintered bulk composites, the layered reduced graphene oxide network, uniform titanium particles and copper‐titanium solid solution are observed in copper matrix. Investigations on mechanical properties show that the as‐prepared bulk composites exhibit the hardness and compressive yield strength compared with single reduced graphene oxide added composites. Increased titanium addition resulted into higher hardness and strength. The relevant formation and failure mechanisms of the composites and their influence on mechanical properties were discussed. [ABSTRACT FROM AUTHOR]
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- 2019
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6. Development of High Performance Magnesium Matrix Nanocomposites Using Nano-SiC Particulates as Reinforcement.
- Author
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Shen, M., Ying, W., Wang, X., Zhang, M., and Wu, K.
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MAGNETISM -- Experiments ,MAGNESIUM group ,LIGHT metals ,METAL extrusion ,MICROSTRUCTURE - Abstract
In the present study, magnesium-based composites with three different volume percentages of nano-sized SiC particulates (SiCp) reinforcement were fabricated using a simple and inexpensive technique followed by hot extrusion. Microstructural characterization of the materials revealed uniform distribution of nano-size SiCp and obvious grain refinement. The tensile test result indicates a remarkable improvement on the strength for the as-extruded SiCp/AZ31B nanocomposite, while the elongation to fracture was decreased by comparing with the AZ31B alloy. Although, compared with the as-extruded AZ31B alloy, the ductility of the SiCp-reinforced AZ31B nanocomposite is decreased, but the ductility of the present SiCp-reinforced AZ31B nanocomposite is far higher than that of the conventional micron or submicron SiCp-reinforced magnesium matrix composites. It is concluded that, compared with the larger sized (micron or submicron) particles, the addition of nano SiCp in the AZ31B alloy resulted in the best combination of the strength and ductility. An attempt is made in the present study to correlate the effect of presence of nano-SiCp as reinforcement and its increasing amount with the microstructural and mechanical properties of magnesium. [ABSTRACT FROM AUTHOR]
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- 2015
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7. Microstructure and room temperature tensile properties of 1 μm-SiCp/AZ31B magnesium matrix composite.
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Shen, M.J., Wang, X.J., Zhang, M.F., Zhang, B.H., Zheng, M.Y., and Wu, K.
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MICROSTRUCTURE ,TEMPERATURE ,TENSILE strength ,MAGNESIUM compounds ,TRANSMISSION electron microscopes - Abstract
In the present study, AZ31B magnesium matrix composites reinforced with two volume fractions (3 and 5 vol.%) of micron-SiC particles(1 μm) were fabricated by semisolid stirring assisted ultrasonic vibration method. The as-cast ingots were extruded at 350 °C with the extrusion ratio of 15:1 at a constant ram speed of 15 mm/s. The microstructure of the composites was investigated by optical microscopy, scanning electron microscope and transmission electron microscope. Microstructure characterization of the composites showed relative uniform reinforcement distribution and significant grain refinement. The presence of 1 μm-SiC particles assisted in improving the elastic modulus and tensile strength. The ultimate tensile strength and yield strength of the 5 vol.% SiCp/AZ31B composites were simultaneously improved. [ABSTRACT FROM AUTHOR]
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- 2015
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8. The Comparison in the Microstructure and Mechanical Properties between AZ91 Alloy and Nano-SiCp/AZ91 Composite Processed by Multi-Pass Forging Under Varying Passes and Temperatures.
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Nie, K.B., Han, J.G., Deng, K.K., Wang, X.J., Xu, C., and Wu, K.
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ALLOYS ,GRAIN size ,CRYSTALLIZATION ,MICROSTRUCTURE ,COMPOSITE materials ,MECHANICAL behavior of materials ,YIELD strength (Engineering) - Abstract
In this study, both AZ91 alloy and nano-SiCp/AZ91 composite were subjected to multi-pass forging under varying passes and temperatures. The microstructure and mechanical properties of the alloy were compared with its composite. After six passes of multi-pass forging at a constant temperature of 400 ℃, complete recrystallization occurred in both the AZ91 alloy and composite. The decrease of temperature and the increase of passes for the multi-pass forging led to further refinement of dynamic recrystallized grains and dynamic precipitation of second phases. The grain size of the nano-SiCp/AZ91 composite was smaller than that of the AZ91 alloy under the same multi-pass forging condition, which indicated that the addition of SiC nanoparticles were beneficial to grain refinement by pinning the grain boundaries. The texture intensity for the 12 passes of multi-pass forging with varying temperatures was increased compared with that after nine passes. The ultimate tensile strength is slightly decreased while the yield strength was increased unobviously for the AZ91 alloy with the decrease of temperature and the increase of the passes for the multi-pass forging. Under the same condition of multi-pass forging, the yield strength of the composite was higher than that of the AZ91 alloy due to the Orowan strengthening effect and grain refinement strengthening resulting from externally applied SiC nanoparticles and internally precipitated second phases. By comparing the microstructure and mechanical properties between the AZ91 alloy and nano-SiCp/AZ91 composite, the strength-toughness properties of the composites at room temperature were affected by the matrix grain size, texture evolution, SiC nanoparticles distribution and the precipitated second phases. [ABSTRACT FROM AUTHOR]
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- 2019
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9. Annealing hardening/softening of nanocrystalline Ta films mediated by grain boundary evolution and phase transformation.
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Zuo, J.D., Wang, Y.Q., Wu, K., Zhang, J.Y., Liu, G., and Sun, J.
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PHASE transitions , *CRYSTAL grain boundaries , *GRAIN , *LOW temperatures , *COMPARATIVE method , *RESEARCH personnel , *WATER softening - Abstract
Due to its service background, the thermal behavior of Ta films is substantially concerning to researchers, especially the heat-induced β-Ta to α-Ta phase transformation. In this work, the nanocrystalline Ta films with varying β/α phase ratios (0.85–0) were deposited and vacuum annealed at 200–800 °C to study the phase transformation behavior and mechanical properties. Partial phase transformation of β-Ta to α-Ta occurred at low temperature (200 °C) and complete transformation when the annealing temperature was raised to 800 °C. Moreover, an orientation relationship of β-<110>//α-<111> and β-{330}//α-{110} was concluded, and a hypothesis theory about the low-temperature phase transformation was proposed. Annealing hardening took place at 200–600 °C and softening at 800 °C in all the samples. The hardening is mostly due to the ordering of intergranular amorphous phases with the temperature increased, simultaneously bringing the increase of modulus. The annealing softening is governed by both grain coarsening and phase transformation, where the latter is dominated in high β fraction samples. • High-temperature induced grain boundary structure ordering promotes the hardening of Ta films at 200 °C–600 °C. • β-Ta to α-Ta phase transformation was found at a wide temperature range, which partially governs the softening of Ta at 800 °C. • A preferred orientation relationship of β-<110>{330}//α-<111>{110} was concluded • The influence of phase transformation on mechanical properties was independently quantified using a simple comparative method. [ABSTRACT FROM AUTHOR]
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- 2024
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10. Tuning the microstructure and mechanical properties of magnetron sputtered Cu-Cr thin films: The optimal Cr addition.
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Li, X.G., Cao, L.F., Zhang, J.Y., Li, J., Zhao, J.T., Feng, X.B., Wang, Y.Q., Wu, K., Zhang, P., Liu, G., and Sun, J.
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THIN films , *MICROSTRUCTURE , *MECHANICAL properties of metals , *SOLID state electronics , *MORPHOLOGY - Abstract
Grain boundary (GB) engineering via alloying opens a pathway to design the interfaces in alloys for tuning their mechanical properties, thus it is quite critical to determine the optimum addition of alloying element. Here, we prepared immiscible Cu-Cr alloyed thin films by non-equilibrium magnetron sputtering deposition to study Cr alloying effects on the microstructure and mechanical properties of Cu thin films. It is found that Cr doping can notably refine the grains and promote the formation of fully nanotwinned columnar grains at low Cr volume concentrations (≤∼3.7 at.%) associated with the average GB Cr concentrations ≤ ∼15 at.%, beyond which the formation of nanotwins is significantly suppressed. The role of Cr atoms/clusters played in the twinning process is rationalized in terms of dislocation rebound-promotion mechanism. Importantly, a maximum hardness is discovered at the optimum Cr addition of ∼2.0 at.%. The Cr concentration-dependent hardness of Cu-Cr alloyed films was quantified by a combined strengthening model. The achievement of the maximum hardness was related to the greatest GB solute segregation-induced strength contribution. It is further uncovered that the Cu-Cr system exhibits strain rate sensitivity (SRS, m ) monotonically reduced with increasing the Cr concentration, ranging from a positive m of 0.0314 (for pure Cu) to a negative m of −0.0245, which is attributed to a competition between the dislocation-boundary interactions (increasing m ) and the dislocation-solute atoms interactions (decreasing m ). These findings provide valuable insights into tuning the composition of alloyed thin films to achieve optimized mechanical performance. [ABSTRACT FROM AUTHOR]
- Published
- 2018
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11. Precipitate characteristics and synergistic strengthening realization of graphene nanoplatelets reinforced bimodal structural magnesium matrix composites.
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Xiang, S.L., Hu, X.S., Wang, X.J., Wang, L.D., and Wu, K.
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GRAPHENE , *MICROSTRUCTURE , *MAGNESIUM alloys , *COMPOSITE materials , *METAL extrusion - Abstract
This study investigates the precipitation behavior in the graphene nanoplatelets (GNPs) reinforced bimodal structural Mg-6Zn (wt%) matrix composite. The GNPs with an increasing content progressively accelerate the age-hardening response in the local regions of the composite. The composite takes only half the time that the Mg-6Zn alloy needs to reach the peak strength when aging at 200 °C. The observation reveals that the planar and wrinkled GNPs in the composite act as the effective trigger of dislocations and collector of solute atoms to accelerate the precipitation. It is concluded that GNPs have a pronounced effect on the development of matrix microstructure. Moreover, the orientation relationship between the aligned GNPs towards the extrusion direction and the matrix grains with a fiber type texture makes the GNPs and [0001] Mg precipitate rods constitute a hybrid strengthening architecture in the composite. As a result, the synergistic strengthening effect of the GNPs and the precipitates is realized. [ABSTRACT FROM AUTHOR]
- Published
- 2018
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12. Alloying effects on the microstructure and mechanical properties of nanocrystalline Cu-based alloyed thin films: Miscible Cu-Ti vs immiscible Cu-Mo.
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Zhang, J.Y., Zhao, J.T., Li, X.G., Wang, Y.Q., Wu, K., Liu, G., and Sun, J.
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MICROSTRUCTURE , *MECHANICAL properties of metals , *THIN films , *NANOCRYSTALS , *SOLID solutions - Abstract
Tuning the microstructure to optimize the mechanical performance of nanocrystalline Cu thin films via the alloying strategy is quite important for their application in microdevices. In this work, we prepared nanocrystalline miscible Cu-Ti and immiscible Cu-Mo alloyed thin films to investigate alloying effects on the microstructure and mechanical properties of Cu thin films in terms of mixing enthalpies. It is found that the dopants of both Ti and Mo can notably refine the grains, and in particular promote the formation of nanotwins below a critical content of solute, beyond which the formation of nanotwins is notably suppressed. The nonmonotonic solute concentration-dependent twinning behavior observed in Cu-Ti and Cu-Mo alloyed thin films is explained by the coupling effects between grain size and grain boundary segregated dopants that affects the stimulated slip process of partials. The increased hardness of both Cu-Ti and Cu-Mo systems with increasing the solute contents are quantitatively explained by combining several strengthening mechanisms, including solid solution strengthening, grain/twin boundary (GB/TB) strengthening, solute segregation-induced strengthening. It unexpectedly appears that with increasing the solute contents, the Cu-Ti system exhibits monotonically reduced positive strain rate sensitivity (SRS, m ), whereas the Cu-Mo system manifests almost constant negative SRS. The fundamental difference in SRS m between Cu-Ti and Cu-Mo is rationalized in terms of the interactions between solute atomic clusters and dislocations based on the cross-core diffusion mechanism. [ABSTRACT FROM AUTHOR]
- Published
- 2018
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13. The partial substitution of Y with Gd on microstructures and mechanical properties of as-cast and as-extruded Mg-10Zn-6Y-0.5Zr alloy.
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Jiang, H.S., Qiao, X.G., Zheng, M.Y., Wu, K., Xu, C., and Kamado, S.
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MAGNESIUM-yttrium alloys , *MECHANICAL behavior of materials , *MICROSTRUCTURE , *RECRYSTALLIZATION (Metallurgy) , *GRAIN size , *TENSILE strength - Abstract
Mg-10Zn-6Y-0.5Zr (wt%) alloy and Mg-10Zn-3Y-3Gd-0.5Zr (wt%) alloy with medium RE content have been fabricated by conventional casting and indirect extrusion. The as-extruded Mg-10Zn-6Y-0.5Zr (wt%) alloy shows a bimodal microstructure containing dynamic recrystallized (DRXed) grains with average grain size of 2 μm and deformed regions. In addition to the fragmented W phase particle bands distributing along the extrusion direction, large amount of nano W phase and small amount of nano β 2 ′ phase are precipitated in the matrix. While the as-extruded Mg-10Zn-3Y-3Gd-0.5Zr (wt%) alloy exhibits completely dynamic recrystallized microstructure with average grain size of 3 μm. The broken W phase particles are distributed homogeneously in the matrix. Icosahedral quasicrystal phase layer is observed at the surface of some W phase particles in the as-extruded Mg-10Zn-3Y-3Gd-0.5Zr alloy. The as-extruded Mg-10Zn-6Y-0.5Zr (wt%) alloy exhibits yield strength of 341 MPa, ultimate tensile strength of 368 MPa and elongation to failure of 6.8%. While the as-extruded Mg-10Zn-3Y-3Gd-0.5Zr (wt%) alloy shows lower yield strength of 247 MPa, ultimate tensile strength of 330 MPa and higher elongation to failure of 19.8%. The higher strength in the as-extruded Mg-10Zn-6Y-0.5Zr (wt%) alloy is mainly attributed to higher area fraction of unDRXed regions with strong texture and the precipitation of nano W and β 2 ′ phase. The fully recrystallized microstructure with weak texture and the formation of icosahedral quasicrystal phases with good coherent bond with α-Mg contribute to the good ductility of the as-extruded Mg-10Zn-3Y-3Gd-0.5Zr alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2018
- Full Text
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14. Low cycle fatigue behaviors of pure Mo and Mo-La2O3 alloys.
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Cheng, P.M., Zhang, Z.J., Zhang, G.J., Zhang, J.Y., Wu, K., Liu, G., Fu, W., and Sun, J.
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METAL fatigue , *MOLYBDENUM alloys , *STRENGTH of materials , *POWDER metallurgy , *MIXING , *TENSILE strength - Abstract
Pure molybdenum (PM) and La 2 O 3 dispersion strengthened Mo alloy (ODS-Mo) were prepared by powder metallurgy through two different mixing method (solid-solid or SS mixing and solid-liquid or SL mixing). After annealed at 1050 °C for 1 h, the PM, SS-Mo and SL-Mo were compared in microstructure and mechanical properties. The microstructural examinations showed that the PM was mostly recrystallized with rather coarse grains, but the ODS-Mo alloys remained fine elongated grains. This discrepancy is due to a higher recrystallization temperature held in the ODS-Mo alloys. The uniaxial testing results showed that the ODS-Mo had higher tensile mechanical properties compared to the PM, which are attributed to the remarkable strengthening and ductilizing effect induced by the La 2 O 3 particles. The low cycle fatigue (LCF) testing results revealed that the PM experienced cyclic hardening behaviors, while the ODS-Mo alloys exhibited cyclic softening behaviors. The Basquin-Manson-Coffin analyses results demonstrated that the ODS-Mo possessed a higher fatigue ductility and longer fatigue life than the PM. Two kinds of cracks, i.e., cleavage cracks and intergranular cracks, were experimentally observed to coexist on the fracture surface. In particular in the SL-Mo alloy, the two crack interacted and propagated forward until final fracture, leading to a step-like crack growth path and concomitantly enhanced fatigue ductility. In addition, different cycling dislocation structures were revealed between the PM and ODS-Mo alloys. Cycle fatigue mechanisms responsible for the fatigue behaviors and microstructure evolution during LCF testing were discussed. The best LCF resistance combined with superior uniaxial tensile mechanical properties found in the SL-Mo alloy were rationalized. [ABSTRACT FROM AUTHOR]
- Published
- 2017
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15. Influence of SiC nanoparticles addition on the microstructural evolution and mechanical properties of AZ91 alloy during isothermal multidirectional forging.
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Nie, K.B., Deng, K.K., Wang, X.J., Wang, T., and Wu, K.
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SILICON carbide , *MICROSTRUCTURE , *MECHANICAL behavior of materials , *MAGNESIUM alloys , *VIBRATION (Mechanics) - Abstract
In this study, low volume fraction SiCp/AZ91 magnesium matrix nanocomposites billets intended for structural applications were synthesized using semisolid stirring assisted ultrasonic vibration, leading to the dispersion of SiC nanoparticles. Both the AZ91 alloy and nanocomposite billets were then subjected to isothermal multidirectional forging (IMDF). Micrographic observations illustrated that the mean grain size of the developed nanocomposite showed an initial increase after 3 IMDF passes, followed by a decrease after 6 IMDF passes compared to the AZ91 alloy. This indicated that the effect of dispersed SiC nanoparticles on the inhibition of the dynamic recrystallization grains growth was impaired due to the present high IMDF temperature. The improved yield strength of the nanocomposite could be attributed to Orowan strengthening effect related to the dispersed SiC nanoparticles as well as the second phases precipitated far from the dynamic recrystallization grains. [ABSTRACT FROM AUTHOR]
- Published
- 2017
- Full Text
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16. Microstructure and mechanical properties of WE43 magnesium alloy fabricated by direct-chill casting.
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Jiang, H.S., Zheng, M.Y., Qiao, X.G., Wu, K., Peng, Q.Y., Yang, S.H., Yuan, Y.H., and Luo, J.H.
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MAGNESIUM alloys , *INGOTS , *METAL microstructure , *MECHANICAL properties of metals , *METAL castings , *GRAIN size - Abstract
High quality WE43 magnesium alloy ingots with diameter of 500 mm are successfully fabricated by direct-chill (DC) casting. The alloying elements distributed almost homogeneously across the large ingot. With the average grain size decreasing from the center to the edge of the ingot, the mechanical properties are improved gradually. After solution treatment at 525 °C for 8 h, the Mg 14 Nd 2 Y phases distributing along the grain boundaries are well dissolved into matrix. The direct-chill (DC) casting ingot exhibits remarkable age-hardening response from 85 Hv to 117 Hv after T6 treatment at 250 °C. The T6 peak-aged sample exhibits ultimate tensile strength of 274 MPa, yield strength of 215 MPa and elongation to failure of 3.4%, which are higher than those of sand-cast and permanent mold cast WE43 alloys. The large amount of nano prismatic β ′ and β 1 phases precipitated during T6 treatment contribute to improved strength of the WE43 alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2017
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17. Effect of Ca/Al ratio on microstructure and mechanical properties of Mg-Al-Ca-Mn alloys.
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Li, Z.T., Zhang, X.D., Zheng, M.Y., Qiao, X.G., Wu, K., Xu, C., and Kamado, S.
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MAGNESIUM alloys , *CALCIUM , *MECHANICAL properties of metals , *METAL microstructure , *METAL extrusion , *STRENGTH of materials - Abstract
The effect of Ca/Al ratio on microstructure and mechanical properties of the as-cast and as-extruded Mg-Al-Ca-Mn alloys were investigated. The as-cast Mg-Al-Ca-Mn alloys with Ca/Al mass ratios less than 0.50 contain divorced and lamellar eutectic (Mg,Al) 2 Ca. When Ca/Al ratio is greater than 0.90, fine lamellar Mg 2 Ca phase is formed in the as-cast Mg-Al-Ca-Mn alloys. After extrusion, the second phases are broken and dispersed along the extrusion direction. The area fraction of DRXed regions decrease with increasing Ca/Al ratio, the microstructure changes from an almost fully recrystallized structure to a bimodal structure consisting of fine dynamically recrystallized (DRXed) grains and coarse deformed regions. With increasing Ca/Al ratio, the DRXed grains and dispersed second phases are refined. The as-extruded alloys exhibit a strong basal fiber texture, the intensity of which is increased with increasing Ca/Al ratio. With increasing Ca/Al ratio, the {0002}<11-20> texture component in the DRXed regions is suppressed, and shifted to a {0002}<10-10> texture component. The strength of the as-extruded Mg-Al-Ca-Mn alloys increases significantly with increasing Ca/Al ratio. The as-extruded Mg-2.7Al-3.5Ca-0.4Mn (wt%) alloy exhibits a tensile proof strength of 438 MPa and an ultimate tensile strength of 457 MPa. The extraordinary high strengths are attributed to the ultrafine DRXed grains pinned by fragmented secondary phases, strong basal texture and dense nano-scale precipitates. The present research indicates that the Mg-Al-Ca-Mn alloys have a great potential as next generation low-cost ultrahigh-strength wrought Mg alloys. [ABSTRACT FROM AUTHOR]
- Published
- 2017
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18. Size-dependent microstructural evolution and mechanical properties of crystalline/amorphous high-entropy alloy nanostructured multilayers: Cu/FeCoCrNiBSi vs Ni/FeCoCrNiBSi.
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Zhao, Y.F., Chen, B., Wang, Y.Q., Zhang, J.Y., Li, S.Z., Wu, K., Liu, G., and Sun, J.
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AMORPHOUS alloys , *COPPER , *MULTILAYERS , *MAGNETRON sputtering , *DEVITRIFICATION , *PSEUDOPLASTIC fluids - Abstract
Magnetron sputtering technique was employed to synthesize crystalline/amorphous high-entropy alloy (AHEA) X/AHEA (X = Cu and Ni, AHEA = Fe 20 Co 20 Cr 20 Ni 20 B 10 Si 10) nanostructured multilayers (CANMs) with equal layer thickness h ranging from 5 to 150 nm, aiming at systematically investigating their plastic deformation and microstructural evolution. Unlike traditional crystalline/crystalline multilayers often with shear banding at small h , the present X/AHEA CANMs exhibit h -independent homogeneous deformation via the thinning of both constituent layers, while associated with h -dependent deformation-induced devitrification in AHEA layers with thickness below 25 nm. This homogeneous plasticity of AHEA layers with the large incubation size for mature shear bands can be ascribed to the coupling between dislocations in X layers and shear transformation zones in AHEA layers. Meanwhile, the absorption of abundant dislocations emitted from X layers by AHEA layers with small thickness facilitates the occurrence of devitrification behavior, implying the microstructural instability under strong constraint conditions. Moreover, both of Cu/AHEA and Ni/AHEA CANMs manifest size-dependent hardness with the fashion that "smaller is stronger", which is captured well by the rule-of-mixture, based on the size-dependent strength of X nanolayers and size-independent homogenous flow of AHEA nanolayers. [Display omitted] [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
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19. Characteristics and mechanical properties of magnesium matrix composites reinforced with micron/submicron/nano SiC particles.
- Author
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Shen, M.J., Wang, X.J., Ying, T., Wu, K., and Song, W.J.
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MAGNESIUM compounds , *MECHANICAL properties of metals , *METALLIC composites , *SILICON carbide , *PARTICLE size distribution , *MICROFABRICATION - Abstract
The (micron[m]+submicron[s]+nano[n]) SiC particles (SiCp) reinforced AZ31B magnesium matrix composites (AZ31B/SiCp/m + s + n composites) were fabricated by stirring casting technology followed by hot extrusion. This method has successfully solved the homodisperse problem of SiCp/m + s + n in the magnesium matrix composites. The influence of SiCp/m + s + n on the dynamic recrystallization (DRX) behavior of the magnesium matrix was investigated by researching the TEM microstructures of composites. The results indicated that the addition of SiCp/m + s + n was helpful to increase the ratio of DRXed nucleation and reduce the average grain size of matrix. The particle deformation zone (PDZ) can be formed in the vicinity of micron SiCp, while the region with high dislocation density can be created around submicron SiCp owing to pin dislocation and deformation mismatch between matrix and particles. These regions are ideal sites for the formation of recrystallization nucleus. Meanwhile, the addition of fine SiCp(nano and submicron) may delay or hinder the growth of matrix grain through the pinning effect on the grain boundaries during hot extrusion. The tensile test indicates that the strength of the AZ31B/SiCp/m + s + n composites has a significant improvement. Compared with the single sized or bimodal sized particles reinforced magnesium matrix composites, the tensile strength of the AZ31B/SiCp/m + s + n composites were highlighted. [ABSTRACT FROM AUTHOR]
- Published
- 2016
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20. Ultrahigh strength as-extruded Mg–10.3Zn–6.4Y–0.4Zr–0.5Ca alloy containing W phase.
- Author
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Jiang, H.S., Qiao, X.G., Xu, C., Zheng, M.Y., Wu, K., and Kamado, S.
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MAGNESIUM alloys , *METAL extrusion , *TUNGSTEN , *METAL castings , *TENSILE strength , *YIELD stress , *CRYSTAL grain boundaries - Abstract
A new ultrahigh-strength W phase (Mg 3 Y 2 Zn 3 ) containing Mg–10.3Zn–6.4Y–0.4Zr–0.5Ca (wt.%) alloy with medium RE content has been fabricated through conventional casting and indirect extrusion. The as-extruded alloy exhibits ultimate tensile strength of 466 MPa, tensile yield stress of 447 MPa and elongation to failure of 4.7%. The as-cast Mg–10.3Zn–6.4Y–0.4Zr–0.5Ca (wt.%) alloy is mainly composed of α-Mg and lamellar eutectic α-Mg and W phase distributed at grain boundaries. After extrusion, the coarse lamellar W phases in the as-cast alloy are broken into fine particles of about 0.5 μm, dispersing in the particle bands along the extrusion direction. The as-extruded alloy exhibits a bimodal microstructure consisting of ultrafine dynamic recrystallized (DRXed) grains with fine broken W phase particles at the DRXed grain boundaries and coarse un-DRXed regions. Large number of nano W phase and small amount of nano β 2 ′ phase are dynamically precipitated in the coarse unDRXed regions during extrusion, which contribute to the ultrahigh strength of the as-extruded alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2016
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21. Effect of microalloying with Ca on the microstructure and mechanical properties of Mg-6 mass%Zn alloys.
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Du, Y.Z., Qiao, X.G., Zheng, M.Y., Wang, D.B., Wu, K., and Golovin, I.S.
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ZINC alloys , *MICROALLOYING , *METAL microstructure , *MECHANICAL properties of metals , *PHASE transitions , *METAL castings - Abstract
The Mg-6 mass%Zn alloys microalloyed with different amounts of Ca were cast and extruded. The second phase in the as-cast Mg-6Zn alloy is Mg 4 Zn 7 , which is replaced by Ca 2 Mg 6 Zn 3 with an increase of Ca addition. Microalloying by Ca affects the grain size, dynamic recrystallization, and dynamic precipitation of Mg-6Zn alloys during extrusion. The Ca addition inhibits dynamic recrystallization and grain growth due to the pinning effect of fine precipitates, giving rise to fine dynamic recrystallized grains. A large amount of precipitates is observed in the Ca containing alloys after extrusion. Ca effectively improves strength of the as-extruded Mg-6Zn alloy, which is mainly attributed to refined dynamic recrystallized grains, dense precipitates, and deformed regions with high-density dislocations and strong basal texture. [ABSTRACT FROM AUTHOR]
- Published
- 2016
- Full Text
- View/download PDF
22. Significantly improved strength and ductility in bimodal-size grained microstructural magnesium matrix composites reinforced by bimodal sized SiCp over traditional magnesium matrix composites.
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Shen, M.J., Wang, X.J., Zhang, M.F., Zheng, M.Y., and Wu, K.
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COMPOSITE materials , *DUCTILITY , *GRAIN size , *MICROSTRUCTURE , *MAGNESIUM , *MATERIAL plasticity - Abstract
High strong magnesium matrix composites can be obtained by refining grain size, heat treatment and severe plastic deformation methods. However, most of the composite enhancing approaches result in the disappointingly poor tensile ductility. Thus, the designing and fabricating of composites with simultaneously good ductility and high strength have become burning issues for the application of light metals/alloys. Simply adding particles or changing particle parameters can not solve the problem of combination of high strength and good ductility. A new method has been developed, wherein the bimodal size grained microstructure formed by adding the bimodal sized SiC particles (SiCp) was selected as favorable microstructure for achieving good ductility and high strength in present work. The fine grains (grain size: <1 μm) were obtained through the particle stimulate of nucleation (PSN) and pin grain boundary effect. However, the coarse grains (grain size: ∼4 μm) were obtained through forming SiCp free zones in the present magnesium matrix composites. The tensile test indicates a significant improvement in the ductility (∼8.3%) and strength (UTS: ∼402 MPa, YS: ∼323 MPa) of the composites. Compared with the conventional single-sized particles (micron or nano) reinforced magnesium matrix composites, the tensile ductility and strength of present composite (AZ31B/SiCp/1n + 9m composite) were highlighted in the current literature. [ABSTRACT FROM AUTHOR]
- Published
- 2015
- Full Text
- View/download PDF
23. Microstructures and mechanical properties of SiCp/AZ91 magnesium matrix nanocomposites processed by multidirectional forging.
- Author
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Nie, K.B., Deng, K.K., Wang, X.J., Gan, W.M., Xu, F.J., Wu, K., and Zheng, M.Y.
- Subjects
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MAGNESIUM alloys , *METAL microstructure , *MECHANICAL properties of metals , *SILICON compounds , *NANOCOMPOSITE materials , *FORGING - Abstract
A particulate reinforced magnesium matrix nanocomposite was subjected to multidirectional forging (MDF). The results showed that the microstructure of the nanocomposite mainly consisted of some large initial grains and fine recrystallized grains along initial grain boundaries after 1 MDF pass. With increasing the MDF passes, the degree of dynamic recrystallization increased and ultrafine grains with average size of about 20 nm were observed in the nanocomposites after 6 MDF passes. The distribution of SiC nanoparticles in the nanocomposite was homogeneous outside some SiC nanoparticle dense zones after different MDF passes. Compared with typical basal texture obtained for 1 MDF pass, the basal pole intensity decreased firstly for 3 MDF pass and then increased for 6 MDF passes. Both ultimate tensile strength and elongation to fracture of the nanocomposite were enhanced with increasing the MDF passes, while yield strength decreased after 3 MDF passes and then increased slightly after 6 MDF passes. [ABSTRACT FROM AUTHOR]
- Published
- 2015
- Full Text
- View/download PDF
24. Multidirectional forging of AZ91 magnesium alloy and its effects on microstructures and mechanical properties.
- Author
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Nie, K.B., Deng, K.K., Wang, X.J., Xu, F.J., Wu, K., and Zheng, M.Y.
- Subjects
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FORGING , *MAGNESIUM alloys , *MECHANICAL behavior of materials , *RECRYSTALLIZATION (Metallurgy) , *CRYSTAL grain boundaries - Abstract
AZ91 alloy was subjected to multidirectional forging (MDF) and the relationship between microstructures and mechanical properties generated by MDF were investigated. The results showed that after 1 MDF pass grain size of the alloy decreased compared with as-cast alloy, and the amount of recrystallization grains increased when the MDF temperature increased from 250 °C to 400 °C. With increasing the MDF passes at 350 °C, grains of the alloy were gradually refined. A typical basal texture was obtained after 1 MDF pass, and then the basal pole scattered with the increase of MDF passes. Mg 17 Al 12 phases were precipitated along grain boundaries during MDF, which could hinder the growth of recrystallization grains. Both tensile strength and elongation to failure of the alloy were significantly enhanced till 3 MDF passes with increasing the MDF passes. [ABSTRACT FROM AUTHOR]
- Published
- 2015
- Full Text
- View/download PDF
25. Microstructures and mechanical properties of AZ91 magnesium alloy processed by multidirectional forging under decreasing temperature conditions.
- Author
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Nie, K.B., Wang, X.J., Deng, K.K., Xu, F.J., Wu, K., and Zheng, M.Y.
- Subjects
- *
MAGNESIUM alloys , *MICROSTRUCTURE , *MECHANICAL behavior of materials , *PRECIPITATION (Chemistry) , *CRYSTAL grain boundaries , *TENSILE strength , *GRAIN refinement - Abstract
The present study dealt with the AZ91 alloy subjected to multidirectional forging (MDF) under decreasing temperature conditions with emphasizing on relationship between microstructures and mechanical properties generated by MDF. The obtained results showed that grains of the alloy were gradually refined while the amount of the second phase precipitated along the grain boundaries was increased with increasing the MDF passes and decreasing the MDF temperature. Compared with the as-cast alloy, yield strength, ultimate tensile strength and elongation of the AZ91 alloy after MDF under decreasing temperature conditions were simultaneously increased. As the numbers of MDF passes were gradually increased and the MDF temperature was gradually decreased, the yield strength was gradually decreased, suggesting that texture softening may overwhelm the strengthening due to the grain refinement as well as the homogeneous distribution of precipitates. [ABSTRACT FROM AUTHOR]
- Published
- 2014
- Full Text
- View/download PDF
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