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Carbon fibre-reinforced ultra-high temperature ceramics (UHTCs) are considered a class of promising materials for several applications, the most appealing ones being in the aerospace sector. Reinforcement is necessary to overcome the brittleness and low thermal shock resistance of ceramics and is often provided through the addition of carbon fibres or other carbon-based phases, such as nanotubes, graphene, and graphite. The present work is focused on the toughening of UHTCs through incorporation of 30−50 vol% thin, ordered graphite layers from conventional filter paper followed by hot pressing sintering. Cellulose filter paper was selected because it undergoes thermolysis with no melting stage forming a strong carbonaceous residue that can be used as toughener. Microstructure and mechanical properties of toughened composites were compared to those of other materials reinforced with short carbon fibres and the effect of different distribution of graphite was studied. Addition of graphite allowed toughness to be increased from 3−4 MPa·m1/2 (for un-reinforced materials) to 5.1−5.5 MPa·m1/2, similar to results obtained with short fibre reinforcement. The high-temperature properties, such as strength and toughness as well as oxidation resistance at 1500 ℃, were also examined.

Traditionally, cellulose nanofiber (CNF) production has primarily relied on virgin cellulose sources. Yet, the shift to using paper mill sludge (PMS) as a source for CNF underscores the significance of reusing and recycling industrial byproducts. PMS contains significant amounts of cellulose that can be extracted as a raw material. The purpose of present study is to provide a sustainable approach to PMS utilization as a paper coating additive in the cellulose nanofibrils (CNFPMS) form via simply scalable wire-wound rod coating method. The effect of CNFPMS additive amounts at two coating layers on microstructure and surface properties of coatings such as porosity, air permeability surface roughness and optical properties such as brightness, gloss and CIE L*a*b* is studied, which they can also provide insight for the eventual print performance. Results indicated that the obtained CNFPMS in paper coating shows 52% decrease in porosity, presenting significant improvement in the coating microstructure. The marginal increase in permeability coefficient and surface roughness, 54% and 10%, respectively, suggests improving color reproduction and preventing color density losses. Optical analysis showed slight decrease in brightness and gloss, as was expected. Notably, the lightness was improved, which also indicates increasing color gamut volume in printing applications. As a result, the current work offers a sustainable approach to manage PMS for use in paper coatings as a high-value-added material. [ABSTRACT FROM AUTHOR]

At present, the friendly recycling of paper industry effluent sludge has gained great prominence due to the ecological and economic benefits. The aim of this work is to evaluate the influence of the incorporation of paper industry effluent sludge into a red wall tile formulation (BIII group), replacing natural limestone material by up to 10 wt.%. For this purpose, five red wall tile formulations were developed by the dry process, pressed at 47 MPa, and fired at 1170 ºC by using a fast-firing cycle. The wall tile formulations were characterized in terms of chemical analysis, thermal analysis (DTA-TG), and dilatometric analysis. The influence of paper industry effluent sludge on the technical properties (apparent density, water absorption, and flexural strength) and sintered microstructure was investigated. The results showed that red wall tiles containing up to 10 wt.% of paper industry effluent sludge have very good usable final properties, indicating their suitability for the wall tile industrial production (BIII group - ABNT NBR ISO 13006). Such results emphasize the feasibility of ecological and economic recycling of paper industry effluent sludge for the production of red wall tiles.

The microstructure of fibrous paper plays an important role in its property investigation. In this study, an approach is proposed to extrapolate a 2D image into a virtual 3D microstructure. Five types of handsheets made of different pulps were prepared. Then, a hybrid function of two-point correlation and lineal-path function (S2&L2) and co-occurrence correlation functions (CCFs) was used in the simulated annealing reconstruction method. Thus, microstructures of two-phase fiber-pore handsheets were reconstructed using 2D scanning electron microscopy images. Finally, penetration simulations and calculations of the absolute permeability of handsheets were conducted. The statistical values of two-point correlation function (S2) and lineal-path function (L2) extracted from the reconstructed images were used to characterize the reconstruction accuracy, and the comparisons of reconstruction accuracy and time were made. The study results showed that the 3D microstructures of fibrous handsheets could be reconstructed effectively by S2&L2 and CCFs, identifying with the targets. The accuracies were around 10−5, and the reconstruction times by CCFs were shortened by 30–60% compared with S2&L2. Moreover, the visual permeability simulation results could reflect the structural difference of handsheets, according to the calculated absolute permeability. These findings provide a guidance for 3D reconstruction of natural fiber paper.

In this work, stacked SiC fibers paper‐reinforced SiC ceramic matrix composites (SiCnf/SiC CMCs) were prepared by nanoimpregnation and transient eutectic (NITE) process using ultra‐long single‐crystal SiC nanofibers. The effect of the SiCnf surface modification via boron nitride (BN) interphase deposition as well as the sintering additive (Al2O3–Y2O3) content on the density, microstructure, and mechanical properties of SiCnf/SiC CMCs has been investigated systematically. The results revealed that the laminated SiCnf/SiC CMCs feature a significant saw‐tooth‐like curve on the load–displacement test, which indicates that the obtained laminated structure with the weak interlayer binding owning to the BN coating treatment possesses significant toughening to the SiC ceramics. Specifically, the SiCnf/SiC CMCs with the sintering additive content of 12 wt% revealed a fracture toughness of over 10 MPa m1/2 after 60 min of BN interface deposition, which is 104.31% higher than that of the composites prepared without BN coating. [ABSTRACT FROM AUTHOR]

Expansive soil exhibits significant swellings and shrinkages, which may result in severe damage or the collapse of structures built upon it. Calcium-based admixtures, such as lime, are commonly used to improve this problematic soil. However, traditional chemical additions can increase significant environmental stress. This paper proposes a sustainable solution, namely, the use of lignin fiber (LF) from the paper industry to partially replace lime as an amendment for expansive soils. Both the macroscopic and microscopic characteristics of the lignin fiber-treated expansive soil are extensively studied. The results show that the mechanical properties of expansive soil are improved by using lignin fiber alone. Under the condition of an optimal dosage of 8%, the compressive strength of lignin fiber-modified soil can reach 193 kPa, the shear strength is increased by 40% compared with the untreated soil, and the water conductivity is also improved with the increase in dosage. In addition, compared with 2% lime-modified soil, the compressive strength of 8% lignin fiber- and 2% lime composite-treated expansive soil increased by 50%, the cohesion increased by 12%, and the water conductivity decreased significantly. The microstructure analysis shows that at an 8% lignin fiber content, lignin fibers interweave into a network in the soil, which effectively enhances the strength and stability of the improved soil. Simultaneously, the fibers can form bridges across the adjacent micropores, leading to the merging of pores and transforming fine, dispersed micropores into larger, connected macropores. Lime promotes the flocculation of soil particles, forming larger aggregates and thus resulting in larger pores. The addition of fibers exerts an inhibitory effect on the flocculation reaction in the composite-improved soil. In conclusion, lignin fibers are an effective addition used to partially replace calcium admixture for the treatment of expansive soil, which provides a sustainable and environmentally friendly treatment scheme for reducing industrial waste. [ABSTRACT FROM AUTHOR]

Expansive soil exhibits significant swellings and shrinkages, which may result in severe damage or the collapse of structures built upon it. Calcium-based admixtures, such as lime, are commonly used to improve this problematic soil. However, traditional chemical additions can increase significant environmental stress. This paper proposes a sustainable solution, namely, the use of lignin fiber (LF) from the paper industry to partially replace lime as an amendment for expansive soils. Both the macroscopic and microscopic characteristics of the lignin fiber-treated expansive soil are extensively studied. The results show that the mechanical properties of expansive soil are improved by using lignin fiber alone. Under the condition of an optimal dosage of 8%, the compressive strength of lignin fiber-modified soil can reach 193 kPa, the shear strength is increased by 40% compared with the untreated soil, and the water conductivity is also improved with the increase in dosage. In addition, compared with 2% lime-modified soil, the compressive strength of 8% lignin fiber- and 2% lime composite-treated expansive soil increased by 50%, the cohesion increased by 12%, and the water conductivity decreased significantly. The microstructure analysis shows that at an 8% lignin fiber content, lignin fibers interweave into a network in the soil, which effectively enhances the strength and stability of the improved soil. Simultaneously, the fibers can form bridges across the adjacent micropores, leading to the merging of pores and transforming fine, dispersed micropores into larger, connected macropores. Lime promotes the flocculation of soil particles, forming larger aggregates and thus resulting in larger pores. The addition of fibers exerts an inhibitory effect on the flocculation reaction in the composite-improved soil. In conclusion, lignin fibers are an effective addition used to partially replace calcium admixture for the treatment of expansive soil, which provides a sustainable and environmentally friendly treatment scheme for reducing industrial waste.

This paper describes the fabrication and characterization of porous SiC ceramics derived from highly-filled preceramic papers. The SiC ceramics were obtained by spark plasma sintering of stacked preceramic papers at temperatures of 2100 and 2200 °C under pressures of 5–60 MPa for 10 min. The microstructure and phase composition were analyzed by scanning electron microscopy and X-ray diffraction, respectively. Gas permeation tests were performed using hydrogen permeation cell at room temperature. It is revealed that the porosity of sintered SiC can be varied from 9 to 45 % depending on the sintering parameters. The shrinkage of the materials during spark plasma sintering occurs in four stages. The linear shrinkage value of the material increases from 7 to 47 % at 2100 °C and from 20 to 50 % for the samples sintered at 2100 and 2200 °C, respectively. Correlation dependencies between porosity and mechanical properties of the fabricated SiC were established. The obtained porous SiC ceramics exhibit high bending strength of 165 MPa and gas permeation flux of 78 molH 2 /m2/s at the porosity of 36 % that make it suitable for ceramic-based membranes. [ABSTRACT FROM AUTHOR]

Multi-walled carbon nanotubes (MWCNTs) are a high-quality interlamination reinforcement material, but the high viscosity of polyetheretherketone (PEEK) prevents good fusion between MWCNTs and PEEK. This study proposes a method to achieve the complete integration of MWCNTs and PEEK through the preparation of a composite film using the vacuum suction filtration (VSF) method and optimizes the process parameters. An orthogonal experiment with three factors (filter paper pore size, ultrasonic dispersion time, and PEEK content) at three levels is designed, and mechanical performance testing and microscopic morphology observation are conducted. The influence of the three factors of filter paper pore size, ultrasonic time, and PEEK content on the elastic modulus and tensile strength of the film is investigated. The results are a filter paper pore size of 0.45 μm, ultrasonic time of 8.3 h, and PEEK content of 336.524 mg. The mechanical performance obtained under the optimal process parameters are an elastic modulus of 2437.5723 MPa and a tensile strength of 46.5196 MPa. This optimal process increases the elastic modulus by 12.3152% while maintaining a high tensile strength. [ABSTRACT FROM AUTHOR]

Collect screen paperboard of mine power transformer and ordinary power transformer in practical lifetime cycle to make insulation test samples, and according to the standard of power, use test means such as viscosity tester, scanning electron microscopy to compare and analyze microstructures of insulation paper such as polymerization degree, surface morphology of mine power transformer and ordinary power transformer, as well as electrical properties such as partial discharge and electrical strength; at the same time, effect of microstructure changes on electrical performances during aging was discussed. The analysis results show that the insulation defects gradually form and expand in the insulation paper during the aging process; compared with the insulation paper of ordinary power transformers, the surface morphology changes of the insulation paper of mine power transformers are more obvious, and the formed defects are more significant.In the aging process, the polymerization degree of insulation paper of ordinary power transformer and mine power transformer presents a gradual decline trend, but the decline speed of polymerization degree of mine power transformer insulation paper is faster.The operating environment of mining area is the main reason that the aging of insulation paper of mine power transformer is more serious than that of ordinary power transformer.In the process of operation, the insulation paper of mine power transformer will produce more discharge quantity, more discharge times and wider discharge phase than ordinary power transformer.In the aging process, the electrical strength of insulation paper of both ordinary power transformer and mine power transformer decreases gradually, but the electrical strength of insulation paper of mine power transformer is lower than that of ordinary power transformer.The microstructural defects of insulation paper of mine power transformers are the direct causes of the more significant changes in their electrical properties.In the process of state monitoring and maintenance of power equipment, it is suggested that the insulation state monitoring of mine power transformers should be carried out strictly according to the power standards,electrical property parameters are more suitable for insulation status monitoring and fault diagnosis of mine power transformer.

In this work, we report a unique and facile approach to the manufacture of fluorine-free superamphiphobic paper. Based on the principle that Fe3O4 nanoparticles (NPs) arranged along the direction of a magnetic field, the mixture of Fe3O4 NPs and polydimethylsiloxane (PDMS) was coated on kraft paper through self-assembly and thermal-curing at a high temperature in a magnetic field, fabricating a mushroom-like microstructure on the paper. At an Fe3O4 NPs content of 75%, the radius of the mushroom-like pillar caps (RCAP) and center-to-center spacing between two pillars (S) obtained the optimal size of 37 ± 18 μm and 237 ± 38 μm, respectively. The oil-contact angle and water-contact angle of the fabricated paper were up to 156° and 160.4°, respectively. It also showed excellent oleophobic stability; the oil-contact angle was still maintained at 141.9° after 1 h. In addition, the contact angles of milk, ethylene glycol and castor oil were all above 150°, and the contact angle of diiodomethane was 134.2°. Moreover, the sample showed great oil resistance with a kit rating value of 12/12 and permeability of 1800+ s. [ABSTRACT FROM AUTHOR]

This study evaluates the potential use of discarded plasterboard paper as fibers from buildings to reinforce concrete. Various concentrations of wastepaper fibers (0.5%, 1%, 1.5%, 2%, and 2.5% by weight of the binder) were investigated in this research. To mitigate the water absorption effect of the paper fibers, metakaolin was employed as a partial cement replacement. The results demonstrate that the inclusion of the wastepaper fiber enhances the mechanical and durability performance of the concrete. The optimal fiber proportion was identified as 1%, leading to a 29% increase in the compressive strength, a 38% increase in the splitting tensile strength, a 12% decrease in the water absorption, and a 23% decrease in the drying shrinkage with respect to the concrete containing 20% metakaolin. However, exceeding this optimal fiber content results in decreased mechanical and durability properties due to the fiber agglomeration and non-uniform fiber distribution within the concrete matrix. Based on the microstructural analysis, the improved performance of the concrete is ascribed to decreased porosity, more refined pore structure, and reduced propagation of microcracks within the concrete matrix in the presence of wastepaper fiber. According to the results, concrete containing 20% metakaolin and 1% wastepaper fiber exhibits durability and mechanical properties comparable to those of the traditional concrete. This finding highlights the significant promise of reducing dependency on conventional cement and incorporating suitable recycled materials, such as discarded plasterboard, and secondary by-products like metakaolin. Such a strategy encourages the preservation of resources, reduction in carbon dioxide emissions, and a decrease in the ecological footprint resulting from concrete production. [ABSTRACT FROM AUTHOR]

Abstract Building bricks were produced by utilizing deinking paper mill sludge (DPMS) and alluvial soil by varying percentage of sludge at different firing temperatures. Different mix proportions were prepared with 0%, 5%, 10%, 15%, 20%, 25% and 30% of DPMS incorporation in alluvial soil by weight. Three firing temperatures of 900 °C, 950 °C and 1000 °C were investigated to simulate the typical condition of kiln. The density, firing shrinkage, water absorption, efflorescence, apparent porosity, compressive strength and thermal conductivity of the bricks were determined. The XRD and microstructural analysis of brick specimens were also studied. The optimum firing temperature was 950 °C. The thermal conductivity decreases with increase in percentage of deinking paper mill sludge. It was found that 15% deinking paper mill sludge gives optimum strength at firing temperature of 950 °C. Developed bricks satisfy the requirements of class 10 of Bureau of Indian Standards (BIS), in terms of efflorescence, compressive strength and water absorption. Thermal conductivity results show that the developed brick was thermally more insulated than the conventional bricks and can be used as alternative to conventional bricks. This will address the issue of waste management through cleaner production and show the ways towards sustainable, economical and energy efficient construction. Highlights • Building bricks were developed utilizing deinking paper mill sludge (DPMS) & soil. • Maximum level of DPMS in production brick is 15% at firing temperature of 950 °C. • The developed bricks satisfies the requirement of class 10 bricks of BIS. • Developed bricks are sustainable and thermally insulated. [ABSTRACT FROM AUTHOR]

This paper identifies physical properties of an interesterified palm‐based fat (EIEPO) that predict oil binding capacity (OBC). A 100% EIEPO sample, 50% EIEPO sample diluted with 50% soybean oil (SBO), and a 20% EIEPO sample diluted with 80% SBO were used to test how saturation level impacts OBC. All samples were crystallized using either a fast (6.4°C/min) or slow (0.1°C/min) cooling rate as well as with or without the application of high‐intensity ultrasound (HIU; 20 kHz) to generate a wide range of physical properties. Immediately after crystallization, the sample's physical properties, including crystal microstructure, solid fat content (SFC), viscoelasticity (G′, G″, and δ), melting behavior, hardness, and OBC (centrifuge method) were quantified. The samples were then stored for 48 h at 22 and 5°C and the aforementioned physical properties were measured again, with one additional measurement for the samples stored at 5°C—OBC using a filter paper method (OBCp). The results indicate that OBC can be optimized in a palm‐based fat by modifying the physical properties which was achieved via the processing conditions. Both measurements of OBC were significantly correlated with SFC, hardness, δ, and enthalpy. A model was developed to predict a sample's OBCc using the following dominant variables—SFC, hardness, peak temperature, enthalpy, and the number of crystals. These results suggest that OBC can be predicted using a sample's SFC, hardness, peak temperature, enthalpy, and number of crystals and that SFC, hardness, and enthalpy are main drivers of OBC. [ABSTRACT FROM AUTHOR]

As two important industrial manufacturing materials, ceramics and metals have their own advantages and disadvantages in terms of physical, chemical, and mechanical properties. The field of material manufacturing has witnessed efforts to develop technical processes that can properly combine these two alloys, aiming to effectively use their respective advantages. The welding technology for ceramics and metals, as a research topic with broad prospects, is comprehensively and deeply analyzed in this review. The current research progress in this field is analyzed from different process perspectives such as fusion welding, brazing welding, diffusion welding. By using appropriate intermediate materials between these two materials, the residual stress and brittle intermetallics near the interface of the transition joint can be minimised by solving the thermal expansion mismatch, reducing the bonding temperature and pressure.

Ceramic matrix composites (CMCs) based on silicon carbide (SiC) are promising materials for applications as structural components used under high irradiation flux and high temperature conditions. The addition of SiC fibers (SiCf) may improve both the physical and mechanical properties of CMCs and lead to an increase in their tolerance to failure. This work describes the fabrication and characterization of novel preceramic paper-derived SiCf/SiCp composites fabricated by spark plasma sintering (SPS). The sintering temperature and pressure were 2100 °C and 20−60 MPa, respectively. The content of fibers in the composites was approx. 10 wt.%. The matrix densification and fiber distribution were examined by X-ray computed tomography and scanning electron microscopy. Short processing time avoided the destruction of SiC fibers during SPS. The flexural strength of the fabricated SiCf/SiCp composites at room temperature varies between 300 and 430 MPa depending on the processing parameters and microstructure of the fabricated composites. A quasi-ductile fracture behavior of the fabricated composites was observed.

In this study, continuous carbon reinforced C f /(Ti 0.2 Zr 0.2 Hf 0.2 Nb 0.2 Ta 0.2)C–SiC high entropy ceramic matrix composites were additively manufactured through paper laminating (PL), direct slurry writing (DSW), and precursor infiltration and pyrolysis (PIP). (Ti 0.2 Zr 0.2 Hf 0.2 Nb 0.2 Ta 0.2)C high entropy ceramic (HEC) powders were synthesized by pressureless sintering and ball milling. A certain proportion of HEC powder, SiC powder, water, binder, and dispersant were mixed to prepare the HEC-SiC slurry. Meanwhile, BN coating was prepared on the 2D fiber cloth surface by the boric acid-urea method and then the cloth was cut into required shape. Additive manufacturing were conducted subsequently. Firstly, one piece of the as-treated carbon fiber cloth was auto-placed on the workbench by paper laminating (PL). Then, the HEC-SiC slurry was extruded onto the surface of the cloth by direct slurry writing (DSW). PL and DSW process were repeated, and a C f /HEC-SiC preform was obtained after 3 cycles. At last, the preform was densified by precursor infiltration and pyrolysis (PIP) and the final C f /HEC-SiC composite was prepared. The open porosity of the C f /HEC-SiC composites, with the HEC volume fractions of 15, 30 and 45%, were 7.7, 10.6, and 11.3%, respectively. And the density of the C f /HEC-SiC composites, with the HEC volume fractions of 15, 30 and 45%, were 2.9, 2.7 and 2.3 g/cm3, respectively. The mechanical properties of the C f /HEC-SiC composites increased firstly and then decreased with the HEC content increase, reaching the maximum value when the HEC volume fraction was 30%. The mechanical properties of the C f /HEC-SiC composites containing 45, 30 and 15% HEC were as follows: flexural strength (180.4 ± 14 MPa, 183.7 ± 4 MPa, and 173.9 ± 4 MPa), fracture toughness (11.9 ± 0.17 MPa m1/2, 14.6 ± 2.89 MPa m1/2, and 11.3 ± 1.88 MPa m1/2), and tensile strength (71.5 ± 4.9 MPa, 98.4 ± 12.2 MPa, and 73.4 ± 8.5 MPa). From this study, the additive manufacturing of continuous carbon fiber reinforced high entropy ceramic matrix composites was achieved, opening a new insight into the manufacturing of ceramic matrix composites. [ABSTRACT FROM AUTHOR]

The paper production is developed throughout the world, therefore, more paper sludge waste (PSw) is accumulating. The aim of this work was to determine the properties of PSw burned at 900 °C and its impact on physical−mechanical properties of cementitious matrix and evaluate its usage/utilization possibilities in cementitious materials. For the implementation of the aim, cement-based specimens were prepared and their −mechanical properties were determined. Specimens from five compositions were formed, with 2.5%, 5%, 7.5%, and 10% of the cement by weight replaced with PSw. When 5% of the cement was replaced with PSw, the compressive strength increased by approximately 7%, although density and ultrasound velocity slightly decreased (up to 1.5%). When 7.5% PSw was added, the compressive strength of the specimens decreased. To summarize, it can be stated that up to 5% PSw may be utilized/used for the preparation of cementitious mixtures. The usage of the waste allows environment conservation, reduced amount of cement in mixtures, and improvement of properties of cementitious materials.

Cellulose‐based paper samples were surface‐modified by a polymeric single‐source precursor prepared from perhydropolysilazane (PHPS) and iron(III)acetylacetonate (Fe(acac)3) and ammonolyzed at 500°C, 700°C, 900°C, and 1000°C, leading to C/SiFe(N,C)O‐based ceramic papers with in situ‐generated hierarchical micro/nano‐morphology. As reference, cellulose‐free samples were prepared under the same conditions. Upon thermal treatment, the microstructure evolutions of the resulting ceramic paper and the reference sample were comparatively investigated. Scanning electron microscopy (SEM) showed that for all temperatures, the ceramic papers exhibit the same morphology as the template, however, with noticeable shrinkage and curling, particularly evident at higher temperatures. X‐ray diffraction (XRD) measurements of the reference samples and the ceramic papers showed a similar crystallization behavior and phase evolution in both materials. In the ceramic paper, the crystallization process seems to occur at a later time. The results provide a comprehensive understanding of the investigated C/SiFe(N,C)O‐based ceramic system. It was shown that use of the cellulose‐based paper template has the benefit of retaining the microstructure and furthermore, apart from transforming the cellulose fibers into turbostratic carbon, does not change the phase evolution during the polymer‐to‐ceramic transformation, allowing at the same time the manufacturing of novel morphologically complex parts by a convenient one‐pot synthesis approach. [ABSTRACT FROM AUTHOR]

This study investigated ink penetration through imaging technology, first by gray and contour mapping and then calculating the ink penetration depth by programing. Next, a series of further analyses were carried out, including average ink permeability, ink distributions, and printability of different uncoated inkjet paper with different parameters. The impact on ink penetration of the microstructure and hydrophilicity of the uncoated paper was also studied. The experimental results indicated that paper specimens with sizing agent were resistant to the ink, resulting in a slow and shallow ink penetration. Paper containing filler had a more hydrophilic surface and porous structure, leading to a faster and deeper ink penetration. However, the calendering operation could make the paper structure more compact and reduce the porosity and penetration depth. When an appropriate combination of sizing agent, filler content, and the calendering process was utilized, a more stable hue could be produced with improvements in optical density, saturation, and color. [ABSTRACT FROM AUTHOR]

This is a review of studies on various types of paper-based epoxy composites currently being designed and developed for technological use. The concept of designing composite materials is very significant for small to large industry and it is important where initiation of repairing work is now being considered for engineering applications. This composite material is of interest due to its advantages compared with others, including low environmental effects and low cost for a wide range of works. This review aims to provide an overview of morphological, physical and mechanical properties of various paper sheetsbased epoxy composites and details of achievements made. From this approach, this paper also presents the preliminary study of SEM results of paper sheets-based epoxy composites designed for repairing work applications. It has been found that a well-arranged laminated paper sheet layers could help the bond strength with epoxy matrix. Thus, this paper sheet-based epoxy composite can be considered as an easiest way, cheap and biodegradable that can be used for various small repairing works in structural and automotive applications. [ABSTRACT FROM AUTHOR]

This study investigated the influence of the main metal materials of transformers on the oil-paper insulation performance. Ten types of insulating specimens were subjected to accelerated thermal aging at 120°C. Some aging parameters, including oil acid number, furfural content and degree of polymerization (DP) of insulating paper, were measured and compared. At the same time, we conducted frequency domain spectroscopy, X-ray diffraction, scanning electron microscopy and energy dispersive spectrometry on the insulating paper. The following conclusions were drawn: silicon lamination slightly deteriorates the insulating oil, copper increases the acidity and accelerates the production of furfural, metal materials can decrease DP of insulating paper and the effect of copper is greater than that of silicon lamination. During thermal aging, the dielectric dissipation factor of insulating paper increases and the carbon content of insulating paper increases. Metal materials can significantly increase the dielectric dissipation factor and carbon content of insulating paper and the effect of copper is greater than that of silicon lamination. [ABSTRACT FROM AUTHOR]

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For the first time the feasibility of using an alkaline wastewater coming from the pulp and paper industry as an activator, partially (50 vol%) replacing commercial sodium hydroxide, in the production of cork-based activated carbons was evaluated. The activated carbons showed the highest value of specific surface area ever reported for cork-based activated carbons (1670 m 2 /g), surpassing several other commercial and waste-based ones. These eco-friendly cork and paper waste-based activated carbons were then evaluated as methylene blue adsorbent materials. The influence of contact time, methylene blue initial concentration and adsorbent amount on the methylene blue removal efficiency by the activated carbons was studied. Extremely fast (>99.9% removal in 5 min) and efficient methylene blue adsorption (uptake of 350 mg/g) by the cork and paper waste-based adsorbents was achieved, which demonstrates the huge potential of these innovative adsorbents. These activated carbons were produced using two unexplored industrial by-products (alkaline wastewater and cork) and, therefore, may be an inexpensive source of activated carbons, which can be used for the effective removal of dyes from wastewaters. Furthermore, despite the very large surface area and high removal efficiency this is not a nano material (being around 30–50 μm in size), its capabilities being due to its unique cork-derived microstructure, and hence it can be handled and removed/filtered much more easily than nanocarbons, and without any associated health or environmental risks. [ABSTRACT FROM AUTHOR]

Biodegradable paper mulch has the advantages of being easily degradable and environmentally benign, but its own performance and adaptability to harsh environments have not been tested. This paper uses scanning electron microscopy and three-dimensional morphometry to microscopically characterize biodegradable paper mulch and white plastic mulch. To analyze and compare their mechanical and hydrophobic properties, and weather resistance, the two mulches were measured through tensile tear load and static contact angle. A comparative analysis of the effect of mulching in the dry crop area of the Hexi Corridor was conducted by comparing the growth index, farm water heat, soil oxygen content, and yield using maize and flax. The test results show that biodegradable paper mulch films were slightly inferior to traditional white mulch films in terms of mechanical and hydrophobic properties, with inadequate insulation and moisture retention, but better in terms of aging resistance, soil oxygen content, and crop insulation and water storage capacity in the middle and growth stages. White mulch film had a better yield enhancement effect on maize, while with biodegradable paper mulch film, this was more significant with flax. [ABSTRACT FROM AUTHOR]

The paper describes the structure and properties of preceramic paper-derived Ti 3 Al(Si)C 2 -based composites fabricated by spark plasma sintering. The effect of sintering temperature and pressure on microstructure and mechanical properties of the composites was studied. The microstructure and phase composition were analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. It was found that at 1150 °C the sintering of materials with the MAX-phase content above 84 vol% leads to nearly dense composites. The partial decomposition of the Ti 3 Al(Si)C 2 phase becomes stronger with the temperature increase from 1150 to 1350 °C. In this case, composite materials with more than 20 vol% of TiC were obtained. The paper-derived Ti 3 Al(Si)C 2 -based composites with the flexural strength > 900 MPa and fracture toughness of >5 MPa m1/2 were sintered at 1150 °C. The high values of flexural strength were attributed to fine microstructure and strengthening effect by secondary TiC and Al 2 O 3 phases. The flexural strength and fracture toughness decrease with increase of the sintering temperature that is caused by phase composition and porosity of the composites. The hardness of composites increases from ~9.7 GPa (at 1150 °C) to ~11.2 GPa (at 1350 °C) due to higher content of TiC and Al 2 O 3 phases. [ABSTRACT FROM AUTHOR]

Highlights • The applicability of the continuum hypothesis to transport in carbon-fiber papers is analyzed. • The LBM is combined with X-ray tomograms to simulate diffusion, convection and conduction. • A representative elementary volume cannot be defined due to the thin nature of these materials. • The anisotropic microstructure strongly reduces through-plane compared to in-plane transport. • The reduction is critical for solid-phase conductivity due to the bottleneck effect of the surface region. Abstract Understanding the transport processes that occur in carbon-fiber papers (CFPs) used in fuel cells, electrolyzers, and metal-air/redox flow batteries is necessary to help predict cell performance and durability, optimize materials and diagnose problems. The most common technique used to model these thin, heterogeneous, anisotropic porous media is the volume-averaged approximation based on the existence of a representative elementary volume (REV). However, the applicability of the continuum hypothesis to these materials has been questioned many times, and the error incurred in the predictions is yet to be quantified. In this work, the existence of a REV in CFPs is assessed in terms of dry effective transport properties: mass diffusivity, permeability and electrical/thermal conductivity. Multiple sub-samples with different widths and thicknesses are examined by combining the lattice Boltzmann method with X-ray tomography images of four uncompressed CFPs. The results show that a meaningful length scale can be defined in the material plane in the order of 1–2 mm, which is comparable to the rib/channel width used in the aforementioned devices. As for the through-plane direction, no distinctive length scale smaller than the thickness can be identified due to the lack of a well-defined separation between pore and volume-averaged scales in these inherently thin heterogeneous materials. The results also show that the highly porous surface region (amounting up to 20% of the thickness) significantly reduces the through-plane electrical/thermal conductivity. Overall, good agreement is found with previous experimental data of virtually uncompressed CFPs when approximately the full thickness is considered. [ABSTRACT FROM AUTHOR]