(5-Methyl-3-phenyl-1 H-pyrazol-1-yl)-[5-( p-tolylamino)-2 H-1,2,3-triazol-4-yl]methanone was synthesized and characterized by 1H NMR, MS and IR spectra data. The structure of title compound was identified by X-ray diffraction. Compound, C 20H 18N 6O, Mr = 358.40, crystallizes in the triclinic space group P- 1 with unit cell parameters a = 10.303(6), b = 12.489(7), c = 15.305(9) Å, α = 108.489(12), β = 101.920(11), γ = 96.971(13)°, V = 1790.0(17) Å 3, Z = 4, Dx = 1.330 mg/cm 3. The final R was 0.0520. Graphical Abstract: (5-Methyl-3-phenyl-1H-pyrazol-1-yl)-[5-(p-tolylamino)-2H-1,2,3-triazol-4-yl]methanone was synthesized. [Figure not available: see fulltext.] [ABSTRACT FROM AUTHOR]