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Synthesis and Crystal Structure of (5-Methyl-3-phenyl-1H-pyrazol-1-yl)-[5-(p-tolylamino)-2H-1,2,3-triazol-4-yl]methanone.
- Source :
- Journal of Chemical Crystallography; Dec2010, Vol. 40 Issue 12, p1078-1081, 4p
- Publication Year :
- 2010
-
Abstract
- (5-Methyl-3-phenyl-1 H-pyrazol-1-yl)-[5-( p-tolylamino)-2 H-1,2,3-triazol-4-yl]methanone was synthesized and characterized by <superscript>1</superscript>H NMR, MS and IR spectra data. The structure of title compound was identified by X-ray diffraction. Compound, C <subscript>20</subscript>H <subscript>18</subscript>N <subscript>6</subscript>O, Mr = 358.40, crystallizes in the triclinic space group P- 1 with unit cell parameters a = 10.303(6), b = 12.489(7), c = 15.305(9) Å, α = 108.489(12), β = 101.920(11), γ = 96.971(13)°, V = 1790.0(17) Å <superscript>3</superscript>, Z = 4, Dx = 1.330 mg/cm <superscript>3</superscript>. The final R was 0.0520. Graphical Abstract: (5-Methyl-3-phenyl-1H-pyrazol-1-yl)-[5-(p-tolylamino)-2H-1,2,3-triazol-4-yl]methanone was synthesized. [Figure not available: see fulltext.] [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 10741542
- Volume :
- 40
- Issue :
- 12
- Database :
- Complementary Index
- Journal :
- Journal of Chemical Crystallography
- Publication Type :
- Academic Journal
- Accession number :
- 55241629
- Full Text :
- https://doi.org/10.1007/s10870-010-9798-3