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Start Over Author "Francis P. Gailliot" Journal cheminform
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1. ChemInform Abstract: Isolation and Characterization of the Major Equilibrium Product of FK- 520

Author

Robert A. Reamer, John M. Ballard, Dennis Kuczynski, Francis P. Gailliot, G. J. Mcmanemin, Theresa K. Natishan, Barry C. Buckland, and Richard S. Egan

Subjects
Preparative hplc, Chemistry, Computational chemistry, law, Component (thermodynamics), Product (mathematics), Yield (chemistry), Polar, General Medicine, Crystallization, law.invention, Characterization (materials science)
Abstract

The existence of an isomeric form in equilibrium with the major component of FK-520 in polar solutions has been demonstrated. This minor component has been isolated in high yield and purity by a novel crystallization strategy and preparative HPLC. The equilibrium product was characterized by NMR and MS.

Published
2010
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