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Start Over Author "Andreas Stumpf" Journal advanced synthesis & catalysis
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1. Kilogram-Scale Asymmetric Ruthenium-Catalyzed Hydrogenation of a Tetrasubstituted Fluoroenamide

Author

Michael Welch, Erhard Bappert, Srinivasan Babu, Felix Spindler, Andreas Stumpf, Daniel P. Sutherlin, John Gaudino, and Mark Reynolds

Subjects
chemistry, Homogeneous, Fluorine, chemistry.chemical_element, Organic chemistry, Homogeneous catalysis, General Chemistry, Enantiomer, Catalysis, Ruthenium
Abstract

Ruthenium-catalyzed asymmetric homogeneous hydrogenation (AHH) is used as the key step of a multi-kilogram scale synthesis of an enantiomeric fluoropiperidine. The AHH of a tetrasubstituted β-fluoroenamide is carried out under mild conditions using a Ru/Josiphos catalyst with high ee (98%).

Published
2011
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