1. XPS and NEXAFS characterisation of plasma deposited vertically aligned N-doped MWCNT
- Author
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Point, S., Minea, T., Bouchet-Fabre, B., Granier, A., and Turban, G.
- Subjects
- *
SPECTRUM analysis , *CARBON , *NANOTUBES , *FULLERENES - Abstract
Abstract: This paper is dedicated to carbon nanotubes grown by electron cyclotron resonance plasma-enhanced chemical vapour deposition. It has been shown that carbon nanotubes (CNTs) can be grown at temperature as low as 550 °C by this technique. X-ray photoelectron spectroscopy and near-edge X-ray absorption fine structure spectroscopy were used to analyse nitrogen-doped CNTs. Independently of the synthesis temperature, about 4 at.% nitrogen are incorporated in the CNTs. A good correlation was found between XPS and NEXAFS results. Four components (397.3, 398.5, 400.8 and 402.5 eV) compose N 1s XPS spectra related to different chemical environments of nitrogen. This interpretation can be used as a simple check method of the presence of CNTs on as-deposited PECVD samples. [Copyright &y& Elsevier]
- Published
- 2005
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