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ChemPhotoChem / The Right Light: De Novo Design of a Robust Modular Photochemical Reactor for Optimum Batch and Flow Chemistry
- Publication Year :
- 2020
-
Abstract
- Having identified inconsistencies when repeating literatureexamples of photochemical transformations and difficultiesrecreating experimental setups, we devised several criteria thatan ideal lab-scale reactor should achieve. Herein, we introducea versatile photoreactor for high-throughput screening, prepa-rative-scale batch reactions and continuous processing, all witha single light source. The reactor utilizes interchangeable arraysof pseudo-monochromatic high-power LEDs in a range ofsynthetically useful wavelengths, combined with excellenttemperature control. Moreover, light intensity can be modu-lated in an accurate and straightforward manner. This systemhas subsequently been tested on a range of literature method-ologies.<br />Europäische Kommission 764920<br />Engineering and Physical Sciences Research Council (EPSRC)(DE-588)5164381-9 EP/S035990/1<br />Accepted version
Details
- Database :
- OAIster
- Notes :
- text/html, German
- Publication Type :
- Electronic Resource
- Accession number :
- edsoai.on1156959911
- Document Type :
- Electronic Resource
- Full Text :
- https://doi.org/10.1002.cptc.201900203