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1,3-Dipolar Addition Reactions of Some Bisdiazo Compounds with Mono and Diolefins

Authors :
STEVENS INST OF TECH HOBOKEN NJ DEPT OF CHEMISTRY AND CHEMICAL ENGINEERING
Kricks, R. J.
Volpe, A. A.
STEVENS INST OF TECH HOBOKEN NJ DEPT OF CHEMISTRY AND CHEMICAL ENGINEERING
Kricks, R. J.
Volpe, A. A.
Source :
DTIC AND NTIS
Publication Year :
1972

Abstract

Bisdiazoterephthalaldehyde, para-bisdiazobenzoylbenzene and meta-bis-diazobenzoylbenzene were synthesized as dicarbene precursors. Simultaneous dicarbene formation and olefinic insertion was attempted. However, what was observed was 1,3-dipolar addition of the bisdiazo compounds and strained olefinic systems such as norbornene and norbornadiene. Nuclear magnetic resonance spectroscopy indicates that the stereo-chemistry of the adducts formed lead to some large chemical shifts. Polymerization was also attempted between meta-bisdiazobenzoylbenzene and norbornadiene.

Details

Database :
OAIster
Journal :
DTIC AND NTIS
Notes :
text/html, English
Publication Type :
Electronic Resource
Accession number :
edsoai.ocn831992952
Document Type :
Electronic Resource