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Asymmetric deprotonation using s-BuLi or i-PrLi and chiral diamines in THF: the diamine matters

Authors :
Carbone, Giorgio
O'rien, Peter
Hilmersson, Goran
Source :
Journal of the American Chemical Society. Nov 3, 2010, Vol. 132 Issue 43, 15445-15450
Publication Year :
2010

Abstract

The NMR spectroscopic analysis has shown that it is possible to perform highly enantioselective asymmetric deprotonation reaction by using i-PrLi or s-BuLi/(+)-sparteine surrogate in THF. The studies have shown that these are the first examples of highly enantioselective asymmetric deprotonation reactions by using organolithium/diamine complexes in THF.

Details

Language :
English
ISSN :
00027863
Volume :
132
Issue :
43
Database :
Gale General OneFile
Journal :
Journal of the American Chemical Society
Publication Type :
Academic Journal
Accession number :
edsgcl.242132110