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NMR studies of 1H NOEs in glycogen

Authors :
Wei Chen
Avison, Malcolm J.
Xiao-Hong Zhu
Shulman, Robert G.
Source :
Biochemistry. Nov 2, 1993, Vol. 32 Issue 43, p11483, 5 p.
Publication Year :
1993

Abstract

Nuclear Overhauser enhancement, used to investigate the cross-relaxation activity of the oyster glycogen protons, revealed a 74% decrease of glycogen H1 following saturation of the H2+H4' resonances of glycogen in D2O. A 60% optimum decrease in H1 intensity occurred after selective reversion of the H2+H4' area and a correct delay for cross-relaxation. These are in agreement with a model in which powerful H1+H2 and H1-H4' dipolar reactions exist.

Details

ISSN :
00062960
Volume :
32
Issue :
43
Database :
Gale General OneFile
Journal :
Biochemistry
Publication Type :
Academic Journal
Accession number :
edsgcl.14832225