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Investigation of tetrahedral mixed-metal carbonyl clusters by two-dimensional (super 59)Co COSY and DQFCOSY NMR experiments

Authors :
Kempgens, Pierre
Elbayed, Karim
Raya, Jesus
Granger, Pierre
Rose, Jacky
Braunstein, Pierre
Source :
Inorganic Chemistry. April 17, 2006, Vol. 45 Issue 8, p3378, 6 p.
Publication Year :
2006

Abstract

Two-dimensional (2D) (Super 59)Co correlation spectroscopy (COSY)/Double-quantum-filtered (DQF)COSY experiments are reported for three tetrahedral mixed-metal clusters HFeCo3(CO)11L with L = PPh3, p(OMe)3, and PCy3 (Cy = cyclohexyl). The 2-D (Super 59)Co COSY and DQFCOSY NMR spectra of these clusters in solution prove the existence of a scalar coupling constant between the (super 59)Co nuclei.

Details

Language :
English
ISSN :
00201669
Volume :
45
Issue :
8
Database :
Gale General OneFile
Journal :
Inorganic Chemistry
Publication Type :
Academic Journal
Accession number :
edsgcl.146109058