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Synthesis of fluorinated 1,2,3-butatrienes from alpha-halovinyl organometallic reagents

Authors :
Morken, Peter A.
Bachand, Patrick C.
Swenson, Dale C.
Burton, Donald J.
Source :
Journal of the American Chemical Society. June 30, 1993, Vol. 115 Issue 13, p5430, 10 p.
Publication Year :
1993

Abstract

The dimerization reaction of fluorinated alpha-halovinyl zinc and copper reagents and their thermal stability was explored. The structures of each of the isomeric members of butatrienes were characterized by X-ray crystallography. Dimerization of these vinyl carbenoids to butatrienes occurs when R is an aromatic C6H5 or C6F5 and R' is a perfluoroalkyl group CF3, C2F5, C3F7.

Details

ISSN :
00027863
Volume :
115
Issue :
13
Database :
Gale General OneFile
Journal :
Journal of the American Chemical Society
Publication Type :
Academic Journal
Accession number :
edsgcl.14184634