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Line narrowing in methyl-TROSY using zero quantum (super 1)H- (super 13)C NMR spectroscopy

Authors :
Tugarinov, Vitali
Sprangers, Remco
Kay, Lewis K.
Source :
Journal of the American Chemical Society. April 21, 2004, Vol. 126 Issue 15, 4921-4925
Publication Year :
2004

Abstract

A zero-quantum correlation experiment for recording (super 1)H-(super 13)C correlations of methyl groups in highly deuterated, a methyl protonated large protein is presented. These zero-quantum spectra benefit from the TROY- effects, in which both intra- and inter -methyl dipolar relaxation interactions are minimized.

Details

Language :
English
ISSN :
00027863
Volume :
126
Issue :
15
Database :
Gale General OneFile
Journal :
Journal of the American Chemical Society
Publication Type :
Academic Journal
Accession number :
edsgcl.119817765