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Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory

Authors :
Kenichi Ozawa
Yoshihiro Aiura
Daisuke Wakabayashi
Hirokazu Tanaka
Takashi Kikuchi
Akio Toyoshima
Kazuhiko Mase
Source :
Journal of Synchrotron Radiation, Vol 29, Iss 2, Pp 400-408 (2022)
Publication Year :
2022
Publisher :
International Union of Crystallography, 2022.

Abstract

Beamline 13 of the Photon Factory has been in operation since 2010 as a vacuum ultraviolet and soft X-ray undulator beamline for X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy (XAS), and angle-resolved photoelectron spectroscopy (ARPES) experiments. The beamline and the end-station at branch B have been recently upgraded, enabling microscopic XPS, XAS, and ARPES measurements to be performed. In 2015, a planar undulator insertion device was replaced with an APPLE-II (advanced planar polarized light emitter II) undulator. This replacement allows use of linear, circular, and elliptical polarized light between 48 and 2000 eV with photon intensities of 109ā€“1013 photons sāˆ’1. For microscopic measurements, a toroidal post-mirror was renewed to have more focused beam with profile sizes of 78 µm (horizontal) × 15 µm (vertical) and 84 µm × 11 µm at photon energies of 100 and 400 eV, respectively. A high-precision sample manipulator composed of an XYZ translator, a rotary feedthrough, and a newly developed goniometer, which is essential for microscopic measurements, has been used to control a sample specimen in six degrees of freedom, i.e. translation in the X, Y, and Z directions and rotation in the polar, azimuthal, and tilt directions. To demonstrate the performance of the focused beams, one- and two-dimensional XPS and XAS scan measurements of a copper grid have been performed. It was indicated from analysis of XPS and XAS intensity maps that the actual spatial resolution can be determined by the beam size.

Details

Language :
English
ISSN :
16005775
Volume :
29
Issue :
2
Database :
Directory of Open Access Journals
Journal :
Journal of Synchrotron Radiation
Publication Type :
Academic Journal
Accession number :
edsdoj.9824e5f381ca4a778107298bc2fa7cdd
Document Type :
article
Full Text :
https://doi.org/10.1107/S160057752200090X