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Simple and one-pot multicomponent benzothiazole-based reaction: Synthesis of novel spiro compounds with 1,3-dicarbonyl skeleton
- Source :
- Results in Chemistry, Vol 9, Iss , Pp 101676- (2024)
- Publication Year :
- 2024
- Publisher :
- Elsevier, 2024.
-
Abstract
- In this work, a new series of 1,2-diphenyl-3aH-spiro[benzo[d]pyrrolo[2,1-b]thaizol-3,5ʹ-pyrimidine (4) or 3,2ʹ-indendion (6) derivatives were efficiently designed and prepared using a novel and easy route in excellent yields by multicomponent-reactions between benzothiazoles, 2-chloro-2-phenylacetophenone, and 1,3-dicarbonyl compounds. These reactions were carried out in CH2Cl2 at ambient temperature under catalyst-free conditions for 3 h. The structure all of the synthesized compounds were established by NMR, IR, EI-MS and elemental analyses.
Details
- Language :
- English
- ISSN :
- 22117156
- Volume :
- 9
- Issue :
- 101676-
- Database :
- Directory of Open Access Journals
- Journal :
- Results in Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- edsdoj.8c9ff8a1daf04bb1a9942d2a599d751e
- Document Type :
- article
- Full Text :
- https://doi.org/10.1016/j.rechem.2024.101676