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syn-6,15-Dihydroxy-2,11-dithia[3.3]metacyclophane ethyl acetate monosolvate

Authors :
Tetsuji Moriguchi
Daisuke Miyamoto
Ventakaprasad Jalli
Kenji Yoza
Akihiko Tsuge
Source :
IUCrData, Vol 1, Iss 1, p x160082 (2016)
Publication Year :
2016
Publisher :
International Union of Crystallography, 2016.

Abstract

The title compound, C16H16O2S2·C4H8O2, is a cyclophane derivative, which was crystallized from an ethylacetate/methanol solvent system. The metacyclophane moiety exists with the benzene rings in the syn orientation, and with a pseudo chair–chair conformation for the dithia 12-membered ring. Both hydroxy groups are positioned on same side of this ring. In the crystal, the cyclophane and the lattice solvent are linked by O—H...O hydrogen bonds.

Details

Language :
English
ISSN :
24143146
Volume :
1
Issue :
1
Database :
Directory of Open Access Journals
Journal :
IUCrData
Publication Type :
Academic Journal
Accession number :
edsdoj.843dba82f89549d28886a53b85b477bf
Document Type :
article
Full Text :
https://doi.org/10.1107/S2414314616000821