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6-Bromo-3-{2-[2-(diphenylmethylene)hydrazinyl]-1,3-thiazol-5-yl}-2H-chromen-2-one chloroform monosolvate
- Source :
- Acta Crystallographica Section E, Vol 67, Iss 5, Pp o1079-o1080 (2011)
- Publication Year :
- 2011
- Publisher :
- International Union of Crystallography, 2011.
-
Abstract
- In the title compound, C25H16BrN3O2S·CHCl3, the thiazole ring is approximately planar [maximum deviation = 0.002 (3) Å] and makes dihedral angles of 10.75 (14) and 87.75 (15)/2.80 (14)° with the pyran ring system and the two terminal phenyl rings, respectively. The solvent molecule is disordered over two sets of sites, with refined occupancies of 0.639 (7) and 0.361 (7). In the crystal, molecules are connected via pairs of weak C—H...O interactions, forming centrosymmetric dimers. An intramolecular C—H...O hydrogen bond generates an S(6) ring motif.
- Subjects :
- Crystallography
QD901-999
Subjects
Details
- Language :
- English
- ISSN :
- 16005368
- Volume :
- 67
- Issue :
- 5
- Database :
- Directory of Open Access Journals
- Journal :
- Acta Crystallographica Section E
- Publication Type :
- Academic Journal
- Accession number :
- edsdoj.7534e41a3b0142ff90cee70c92263be1
- Document Type :
- article
- Full Text :
- https://doi.org/10.1107/S1600536811012335