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5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate

Authors :
Siyoung Jang
Sung Kwon Kang
Nam Sook Cho
Source :
Acta Crystallographica Section E, Vol 68, Iss 3, Pp o781-o781 (2012)
Publication Year :
2012
Publisher :
International Union of Crystallography, 2012.

Abstract

The asymmetric unit of the title compound, C12H10N4O2S4·2C2H6OS, contains one half of the p-xylene molecule and one dimethyl sulfoxide molecule. The p-xylene molecule is located about a crystallographic inversion centre. In the molecule, the thiadiazole and benzene rings are almost perpendicular to one another, with a dihedral angle of 88.95 (6)°. In the crystal, an N—H...O hydrogen bond is observed between the two components. The dimethyl sulfoxide molecule is disordered over two orientations with an occupancy ratio of 0.879 (1):0.121 (1).

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
68
Issue :
3
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.62a207dc62104a3bbcc1ac143b377086
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536812006289