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Fully automated measurement system for temperature-dependent X-ray total scattering at beamline BL04B2 at SPring-8

Authors :
Hiroki Yamada
Kengo Nakada
Michitaka Takemoto
Koji Ohara
Source :
Journal of Synchrotron Radiation, Vol 29, Iss 2, Pp 549-554 (2022)
Publication Year :
2022
Publisher :
International Union of Crystallography, 2022.

Abstract

Data-driven approaches in materials science demand the collection of large amounts of data on the target materials at synchrotron beamlines. To accurately gather suitable experimental data, it is essential to establish fully automated measurement systems to reduce the workload of the beamline staff. Moreover, the recent COVID-19 pandemic has further emphasized the necessity of automated and/or remote measurements at synchrotron beamlines. Here, the installation of a new sample changer combined with a high-temperature furnace and a fully automated alignment system on beamline BL04B2 at SPring-8 is reported. The system allows X-ray total scattering measurements of up to 21 samples at different temperatures (from room temperature to 1200°C) to be conducted without any human assistance.

Details

Language :
English
ISSN :
16005775
Volume :
29
Issue :
2
Database :
Directory of Open Access Journals
Journal :
Journal of Synchrotron Radiation
Publication Type :
Academic Journal
Accession number :
edsdoj.5f336f9f6bea4a4f8517cb5066e4bc83
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600577521013527