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Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative
- Source :
- Chinese Journal of Magnetic Resonance, Vol 37, Iss 04, Pp 496-504 (2020)
- Publication Year :
- 2020
- Publisher :
- Science Press, 2020.
-
Abstract
- N-acylhydrazone compounds have two isomers, E/cis and E/trans, in polar solvents. In this work, 1H and 13C nuclear magnetic resonance (NMR) signals, coupling constants (J), and the spatial structures of the two isomers (E/cis and E/trans) of a novel carbazole-triazinoindole based N-acylhydrazone derivative 3, 2-(5H-[1,2,4] triazine[5,6-b]indol-3-ylthio)-N'-(9-ethylcarbazol-3-ylmethylene)acetylhydrazine, were obtained by one-dimensional and two-dimensional NMR techniques, infrared spectroscopy (IR) and elemental analysis. The ratios of the two isomers were determined.
Details
- Language :
- Chinese
- ISSN :
- 10004556
- Volume :
- 37
- Issue :
- 04
- Database :
- Directory of Open Access Journals
- Journal :
- Chinese Journal of Magnetic Resonance
- Publication Type :
- Academic Journal
- Accession number :
- edsdoj.38dbd9bcf374bcbb89f62674e22261f
- Document Type :
- article
- Full Text :
- https://doi.org/10.11938/cjmr20202803