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Assignments of NMR Spectral Data of a Novel Carbazole-Triazinoindole Based N-Acylhydrazone Derivative

Authors :
LI Ying-jun
YANG Hong-jing
LIU Ji-hong
JIN Kun
LIN Le-di
LIU Xue-jie
Source :
Chinese Journal of Magnetic Resonance, Vol 37, Iss 04, Pp 496-504 (2020)
Publication Year :
2020
Publisher :
Science Press, 2020.

Abstract

N-acylhydrazone compounds have two isomers, E/cis and E/trans, in polar solvents. In this work, 1H and 13C nuclear magnetic resonance (NMR) signals, coupling constants (J), and the spatial structures of the two isomers (E/cis and E/trans) of a novel carbazole-triazinoindole based N-acylhydrazone derivative 3, 2-(5H-[1,2,4] triazine[5,6-b]indol-3-ylthio)-N'-(9-ethylcarbazol-3-ylmethylene)acetylhydrazine, were obtained by one-dimensional and two-dimensional NMR techniques, infrared spectroscopy (IR) and elemental analysis. The ratios of the two isomers were determined.

Details

Language :
Chinese
ISSN :
10004556
Volume :
37
Issue :
04
Database :
Directory of Open Access Journals
Journal :
Chinese Journal of Magnetic Resonance
Publication Type :
Academic Journal
Accession number :
edsdoj.38dbd9bcf374bcbb89f62674e22261f
Document Type :
article
Full Text :
https://doi.org/10.11938/cjmr20202803