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2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one

Authors :
De-Yong Ye
Yong Chu
Zhao-Hui Huang
Source :
Acta Crystallographica Section E, Vol 67, Iss 1, Pp o168-o168 (2011)
Publication Year :
2011
Publisher :
International Union of Crystallography, 2011.

Abstract

The title compound, C20H16N2O4S, was prepared by introduction of a 2-nitrobenzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one via an alkaline-catalysed reaction. The thiazepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.75 (14) and 10.82 (14)° with respect to the two benzene rings, while the two benzene rings make a dihedral angle of 62.96 (10)°. Weak intermolecular C—H...O hydrogen bonds occur in the crystal structure.

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
67
Issue :
1
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.2354c6d91dc45b0bd157899c71d9ed0
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536810052098