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2-Propyl 3,3-dibromo-2-hydroxypyrrolidine-1-carboxylate

Authors :
Christopher Hulme
Justin Dietrich
Zhigang Xu
Steven Gunawan
Gary S. Nichol
Source :
Acta Crystallographica Section E, Vol 66, Iss 3, Pp o597-o597 (2010)
Publication Year :
2010
Publisher :
International Union of Crystallography, 2010.

Abstract

The title compound, C8H13Br2NO3, crystallizes as a non-merohedral twin with twin law −0.6 0 0.4/0 − 1 0 /1.6 0 0.6, and the structure has a refined twin domain ratio of 0.546 (5). The structure shows a compact conformation, with the ester unit roughly coplanar with a mean plane fitted through the non-H atoms of the pyrrolidine ring [dihedral angle = 8.23 (9)°]. In the crystal, inversion dimers linked by pairs of O—H...O hydrogen bonds generate an R22(12) motif.

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
66
Issue :
3
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.06e49877bbb149119fda93c6fbe76853
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536810005106