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Avoiding common errors in X-ray photoelectron spectroscopy data collection and analysis, and properly reporting instrument parameters

Authors :
Joshua W. Pinder
George H. Major
Donald R. Baer
Jeff Terry
James E. Whitten
Jan Čechal
Jacob D. Crossman
Alvaro J. Lizarbe
Samira Jafari
Christopher D. Easton
Jonas Baltrusaitis
Matthijs A. van Spronsen
Matthew R. Linford
Source :
Applied Surface Science Advances, Vol 19, Iss , Pp 100534- (2024)
Publication Year :
2024
Publisher :
Elsevier, 2024.

Abstract

Despite numerous tutorials and standards written to the technical community on X-ray photoelectron spectroscopy (XPS), difficulties with data acquisition, analysis, and reporting persist. This work focuses on common errors in XPS that are frequently observed in the scientific literature and their sources. Indeed, this work covers: (i) XPS data collection, initial data analysis, and data presentation, (ii) Handling XPS backgrounds, (iii) Common errors in XPS peak fitting, and (iv) XPS data presentation and reporting. Graphical examples of errors and appropriate ways of handling data and correcting errors are provided. Additional readings are listed for greater in-depth exploration of the subjects discussed.

Details

Language :
English
ISSN :
26665239
Volume :
19
Issue :
100534-
Database :
Directory of Open Access Journals
Journal :
Applied Surface Science Advances
Publication Type :
Academic Journal
Accession number :
edsdoj.043c0df989af4c78811d052c13777431
Document Type :
article
Full Text :
https://doi.org/10.1016/j.apsadv.2023.100534