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Synthesis of $c$-axis textured CaKFe$_4$As$_4$ superconducting bulk via spark plasma texturing technique

Authors :
Ishida, Shigeyuki
Kamiya, Yoshihisa
Tsuchiya, Yoshinori
Sugali, Pavan Kumar Naik
Mawatari, Yasunori
Iyo, Akira
Yoshida, Yoshiyuki
Eisaki, Hiroshi
Kawashima, Kenji
Ogino, Hiraku
Source :
Journal of Alloys and Compounds 961, 171093 (2023)
Publication Year :
2024

Abstract

Grain alignment is a key factor that determines the performance of a superconducting bulk. In this study, the spark plasma texturing (SPT) technique was used to fabricate a CaKFe$_4$As$_4$ superconducting bulk. X-ray diffraction and electron backscatter diffraction revealed that the $c$-axes of the CaKFe$_4$As$_4$ grains in the SPT bulk are aligned, demonstrating that the SPT technique is effective in achieving $c$-axis texture. In addition, chemical composition analysis showed that oxide impurities, which affect the grain boundary characteristics that determine the inter-grain critical current density ($J_c$), are randomly distributed in the SPT bulk. Magnetization measurements showed high $J_c$ values of the SPT bulk, reaching 127 kA cm$^{-2}$ and 26 kA cm$^{-2}$ at 4.2 K under a self-field and magnetic field of 5 T, respectively. These results suggest that the SPT technique is a promising approach for obtaining a high-performance superconducting bulk material for high-field applications.

Details

Database :
arXiv
Journal :
Journal of Alloys and Compounds 961, 171093 (2023)
Publication Type :
Report
Accession number :
edsarx.2403.19984
Document Type :
Working Paper
Full Text :
https://doi.org/10.1016/j.jallcom.2023.171093