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The human factor: results of a small-angle scattering data analysis Round Robin

Authors :
Pauw, Brian R.
Smales, Glen J.
Anker, Andy S.
Balazs, Daniel M.
Beyer, Frederick L.
Bienert, Ralf
Bouwman, Wim G.
Breßler, Ingo
Breternitz, Joachim
Brok, Erik S
Bryant, Gary
Clulow, Andrew J.
Crater, Erin R.
De Geuser, Frédéric
Del Giudice, Alessandra
Deumer, Jérôme
Disch, Sabrina
Dutt, Shankar
Frank, Kilian
Fratini, Emiliano
Gilbert, Elliot P.
Hahn, Marc Benjamin
Hallett, James
Hohenschutz, Max
Hollamby, Martin
Huband, Steven
Ilavsky, Jan
Jochum, Johanna K.
Juelsholt, Mikkel
Mansel, Bradley W.
Penttilä, Paavo
Pittkowski, Rebecca K.
Portale, Giuseppe
Pozzo, Lilo D.
Garcia, Paulo Ricardo de Abreu Furtado
Rochels, Leonhard
Rosalie, Julian M.
Saloga, Patrick E. J.
Seibt, Susanne
Smith, Andrew J.
Smith, Gregory N.
Annadurai, Venkatasamy
Spiering, Glenn A.
Stawski, Tomasz M.
Taché, Olivier
Thünemann, Andreas F.
Toth, Kristof
Whitten, Andrew E.
Wuttke, Joachim
Publication Year :
2023

Abstract

A Round Robin study has been carried out to estimate the impact of the human element in small-angle scattering data analysis. Four corrected datasets were provided to participants ready for analysis. All datasets were measured on samples containing spherical scatterers, with two datasets in dilute dispersions, and two from powders. Most of the 46 participants correctly identified the number of populations in the dilute dispersions, with half of the population mean entries within 1.5% and half of the population width entries within 40%, respectively. Due to the added complexity of the structure factor, much fewer people submitted answers on the powder datasets. For those that did, half of the entries for the means and widths were within 44% and 86% respectively. This Round Robin experiment highlights several causes for the discrepancies, for which solutions are proposed.<br />Comment: 23 pages, 10 figures. For the original information sent to RR participants, see https://zenodo.org/record/7506365 . For the anonymized results and Jupyter notebook for analysis, see https://zenodo.org/record/7509710

Details

Database :
arXiv
Publication Type :
Report
Accession number :
edsarx.2303.03772
Document Type :
Working Paper