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The Dresden in-situ (S)TEM special with a continuous-flow liquid-helium cryostat

Authors :
Börrnert, Felix
Kern, Felix
Seifert, Franziska
Riedel, Thomas
Müller, Heiko
Büchner, Bernd
Lubk, Axel
Source :
Ultramicroscopy 203, 12-20 (2019)
Publication Year :
2019

Abstract

Fundamental solid state physics phenomena typically occur at very low temperatures, requiring liquid helium cooling in experimental studies. Transmission electron microscopy is a well-established characterization method, which allows probing crucial materials properties down to nanometer and even atomic resolution. Due to the limited space in the object plane, however, suitable liquid-helium cooling is very challenging. To overcome this limitation, resolving power was sacrificed in our Dresden in-situ (S)TEM special, resulting in more than 60 mm usable experimental space in all directions with the specimen in the center. With the installation of a continuous-flow liquid-helium cryostat, any temperature between 6.5 K and 400 K can be set precisely and kept for days. The information limit of the Dresden in-situ (S)TEM special is about 5 nm. It is shown that the resolution of the Dresden in-situ (S)TEM special is currently not limited by aberrations, but by external instabilities, that are currently addressed.<br />Comment: 9 Pages, 10 Figures

Details

Database :
arXiv
Journal :
Ultramicroscopy 203, 12-20 (2019)
Publication Type :
Report
Accession number :
edsarx.1910.00480
Document Type :
Working Paper
Full Text :
https://doi.org/10.1016/j.ultramic.2019.01.005