Back to Search Start Over

[Determination of fifteen metal elements in Cynomorium songaricum by flame atomic absorption spectrophotometry (FAAS)]

Authors :
Guo-qing, Xue
Qing, Liu
Xue-feng, Ren
Yu-qi, Han
Source :
Guang pu xue yu guang pu fen xi = Guang pu. 24(11)
Publication Year :
2005

Abstract

A FAAS method was established for the determination of Na, K, Mg, Ca, Cu, Zn, Fe, Mn, Ni, Co, Pb, Cr, Cd, Ag and Au in Cynomorium songaricum after digestion with HNO3-HClO4 (phi 4:1) at 90-95 degrees C and at normal pressure. In this paper, the parameters in FAAS were studied. The analytical results of Na, K, Mg, Ca, Fe, Zn, Cu, Mn, Pb, Ni and Ag were 13,572.0, 14,260.0, 358.3, 168.3, 238.5, 19.4, 5.9, 3.4, 2.6, 1.3 and 0.4 microg x g(-1) respectively and Co, Cr, Cd and Au were not found in the samples. The results showed that the recovery of standard addition was 97.8%-104.5%, and the relative standard deviation (n = 9) was 0.2%-5.0%. The method is fast, simple and convenient. The results were satisfactory.

Details

ISSN :
10000593
Volume :
24
Issue :
11
Database :
OpenAIRE
Journal :
Guang pu xue yu guang pu fen xi = Guang pu
Accession number :
edsair.pmid..........29b480e3952466119a17f268839c0ae2