Back to Search Start Over

Microreactor-Based TG–TEM Synchronous Analysis

Authors :
Fanglan Yao
Pengcheng Xu
Ming Li
Xuefeng Wang
Hao Jia
Ying Chen
Xinxin Li
Source :
Analytical Chemistry. 94:9009-9017
Publication Year :
2022
Publisher :
American Chemical Society (ACS), 2022.

Abstract

It is challenging to measure the heating-induced mass change of the material during its morphological/structural evolution process. Herein, a silicon microreactor is developed for thermogravimetric-transmission electron microscopy synchronous analysis (TG-TEM synchronous analysis). A self-heating resonant microcantilever for mass-change detection and a dummy microcantilever with electron-beam transparent SiN

Subjects

Subjects :
Analytical Chemistry

Details

ISSN :
15206882 and 00032700
Volume :
94
Database :
OpenAIRE
Journal :
Analytical Chemistry
Accession number :
edsair.doi.dedup.....fb5d640a25b6d1268353127c9af1f008
Full Text :
https://doi.org/10.1021/acs.analchem.2c01051