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Synthesis of New Pentacyclo[5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCU) Cyanosilylated Derivatives Using Sulphated Zirconia and Hydrotalcite as Catalysts in Microwave-Assisted Reactions under Solvent Free Conditions
- Source :
- Molecules, Molecules; Volume 16; Issue 8; Pages: 6561-6576, Molecules, Vol 16, Iss 8, Pp 6561-6576 (2011)
- Publication Year :
- 2011
- Publisher :
- MDPI, 2011.
-
Abstract
- A comparison was made of the effectiveness of the functionalization reactions of pentacyclo[5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCU) using sulphated zirconia in protection-deprotection reactions and Mg/Al hydrotalcite in a cyanosilylation reaction, under classical thermal conditions and imposing microwave radiation; improved yields and reaction times were considered.
- Subjects :
- Silicon
Materials science
Magnesium Hydroxide
Chemistry, Organic
Pharmaceutical Science
Aluminum Hydroxide
Microwave assisted
Article
catalysts
microwaves
Catalysis
Analytical Chemistry
lcsh:QD241-441
chemistry.chemical_compound
lcsh:Organic chemistry
X-Ray Diffraction
hydrotalcite
Drug Discovery
Alkanes
Spectroscopy, Fourier Transform Infrared
Organic chemistry
Cubic zirconia
Physical and Theoretical Chemistry
Cyanates
Solvent free
Hydrotalcite
Sulfates
Organic Chemistry
sulphated zirconia
PCU
chemistry
Chemistry (miscellaneous)
Molecular Medicine
Surface modification
Zirconium
Undecane
Microwave
Subjects
Details
- Language :
- English
- ISSN :
- 14203049
- Volume :
- 16
- Issue :
- 8
- Database :
- OpenAIRE
- Journal :
- Molecules
- Accession number :
- edsair.doi.dedup.....f238f68d7f2047262723a2966b3fd9fa