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Note: A quartz cell with Pt single crystal bead electrode for electrochemical scanning tunneling microscope measurements

Authors :
Zhigang Xia
Yubin Hou
Jihao Wang
Qingyou Lu
Source :
The Review of scientific instruments. 85(9)
Publication Year :
2014

Abstract

In this paper, we provide and demonstrate a design of a unique cell with Pt single crystal bead electrode for electrochemical scanning tunneling microscope (ECSTM) measurements. The active metal Pt electrode can be protected from air contamination during the preparation process. The transparency of the cell allows the tip and bead to be aligned by direct observation. Based on this, a new and effective alignment method is introduced. The high-quality bead preparations through this new cell have been confirmed by the ECSTM images of Pt (111).

Details

ISSN :
10897623
Volume :
85
Issue :
9
Database :
OpenAIRE
Journal :
The Review of scientific instruments
Accession number :
edsair.doi.dedup.....f0b35c63e1308e1e5b059ed4125c5f8b