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New consistency tests for high-accuracy measurements of X-ray mass attenuation coefficients by the X-ray extended-range technique

Authors :
Chanh Q. Tran
Jack L. Glover
Christopher T. Chantler
Zwi Barnea
Nicholas A. Rae
M. T. Islam
Source :
Acta crystallographica. Section A, Foundations of crystallography. 68(Pt 2)
Publication Year :
2011

Abstract

An extension of the X-ray extended-range technique is described for measuring X-ray mass attenuation coefficients by introducing absolute measurement of a number of foils - the multiple independent foil technique. Illustrating the technique with the results of measurements for gold in the 38-50 keV energy range, it is shown that its use enables selection of the most uniform and well defined of available foils, leading to more accurate measurements; it allows one to test the consistency of independently measured absolute values of the mass attenuation coefficient with those obtained by the thickness transfer method; and it tests the linearity of the response of the counter and counting chain throughout the range of X-ray intensities encountered in a given experiment. In light of the results for gold, the strategy to be ideally employed in measuring absolute X-ray mass attenuation coefficients, X-ray absorption fine structure and related quantities is discussed.

Details

ISSN :
16005724
Volume :
68
Issue :
Pt 2
Database :
OpenAIRE
Journal :
Acta crystallographica. Section A, Foundations of crystallography
Accession number :
edsair.doi.dedup.....ead5948d86f970385415921af708b726