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A 30 nm-resolution hard X-ray microscope with X-ray fluorescence mapping capability at BSRF

Authors :
Kun Gao
Michael Feser
Youli Hong
Andrei Tkachuk
Wenbing Yun
Wanxia Huang
Kai Zhang
Jeff Gelb
Benjamin Hornberger
Ziyu Wu
Zhili Wang
Qingxi Yuan
Peiping Zhu
Source :
Journal of Synchrotron Radiation. 19:1021-1028
Publication Year :
2012
Publisher :
International Union of Crystallography (IUCr), 2012.

Abstract

A full-field transmission X-ray microscope (TXM) operating continuously from 5 keV to 12 keV with fluorescence mapping capability has been designed and constructed at the Beijing Synchrotron Radiation Facility, a first-generation synchrotron radiation facility operating at 2.5 GeV. Spatial resolution better than 30 nm has been demonstrated using a Siemens star pattern in both absorption mode and Zernike phase-contrast mode. A scanning-probe mode fluorescence mapping capability integrated with the TXM has been shown to provide 50 p. p. m. sensitivity for trace elements with a spatial resolution (limited by probing beam spot size) of 20 mm. The optics design, testing of spatial resolution and fluorescence sensitivity are presented here, including performance measurement results.

Details

ISSN :
16005775 and 09090495
Volume :
19
Database :
OpenAIRE
Journal :
Journal of Synchrotron Radiation
Accession number :
edsair.doi.dedup.....c3f9ef88694c63e45847da231098e03c