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In situ study of the sintering of a lead phosphovanadate in an Environmental Scanning Electron Microscope
- Source :
- Solid State Ionics, Solid State Ionics, 2011, 186 (1), pp.53-58. 〈10.1016/j.ssi.2011.01.004〉, Solid State Ionics, Elsevier, 2011, 186 (1), pp.53-58. ⟨10.1016/j.ssi.2011.01.004⟩
- Publication Year :
- 2011
- Publisher :
- HAL CCSD, 2011.
-
Abstract
- cited By 3; International audience; The in situ sintering of a powder of Pb3(VO4) 1.6(PO4)0.4 composition was performed in an Environmental Scanning Electron Microscope. The electric current induced by the electron beam was found to reduce the effective temperature of sintering as well as to accelerate the kinetics of shrinkage of a cluster composed of sub-micrometric grains of material. The presence of the residual current flow in the cluster during observation for in situ experiments helps to reduce the apparent sintering temperatures from 50 to 150 °C compared to conventional heating conditions without current. © 2011 Elsevier B.V. All rights reserved.
- Subjects :
- In situ
In-situ experiments
Materials science
Kinetics
Current
[ SPI.MAT ] Engineering Sciences [physics]/Materials
Analytical chemistry
Electron microscopes
Sintering
02 engineering and technology
Environmental scanning electron microscopes
01 natural sciences
[SPI.MAT]Engineering Sciences [physics]/Materials
Effective temperature
0103 physical sciences
General Materials Science
Electron beam-induced deposition
Composite material
Environmental scanning electron microscope
Shrinkage
010302 applied physics
Conventional heating
In-situ
Electron beams
General Chemistry
Residual current
Sintering temperatures
021001 nanoscience & nanotechnology
Condensed Matter Physics
ESEM
In-Situ Study
Cathode ray
Electric current
0210 nano-technology
Scanning electron microscopy
Subjects
Details
- Language :
- English
- ISSN :
- 01672738
- Database :
- OpenAIRE
- Journal :
- Solid State Ionics, Solid State Ionics, 2011, 186 (1), pp.53-58. 〈10.1016/j.ssi.2011.01.004〉, Solid State Ionics, Elsevier, 2011, 186 (1), pp.53-58. ⟨10.1016/j.ssi.2011.01.004⟩
- Accession number :
- edsair.doi.dedup.....ac480c6b9607d9eb125c0daa3d317a81